Development of a plant reference material for composition of a cement raw mixture

A plant reference material (RM) was developed, which was certified in the content of fluorine-ion (% wt) in the cement raw mixture (PRM - 1 CM). Its metrological characteristics were set on the basis of results ofpotentiometric, photometric and titrimetric methods of analysis. The substantiation of...

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Main Authors: A. N. Smagunova, I. S. Shirokolobova, V. A. Kozlov, E. N. Korzhova, O. S. Krivchenko, L. P. Shaulina, A. L. Finkelshtein
Format: Article
Language:Russian
Published: Ural Research Institute of Metrology 2017-05-01
Series:Стандартные образцы
Subjects:
Online Access:https://www.rmjournal.ru/jour/article/view/32
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author A. N. Smagunova
I. S. Shirokolobova
V. A. Kozlov
E. N. Korzhova
O. S. Krivchenko
L. P. Shaulina
A. L. Finkelshtein
author_facet A. N. Smagunova
I. S. Shirokolobova
V. A. Kozlov
E. N. Korzhova
O. S. Krivchenko
L. P. Shaulina
A. L. Finkelshtein
author_sort A. N. Smagunova
collection DOAJ
description A plant reference material (RM) was developed, which was certified in the content of fluorine-ion (% wt) in the cement raw mixture (PRM - 1 CM). Its metrological characteristics were set on the basis of results ofpotentiometric, photometric and titrimetric methods of analysis. The substantiation of the need for RM is given to increase the accuracy of results when determining fluorine in materials of cement production. The conditions are defined to use X-ray fluorescence method for estimating the material homogeneity in developing similar RMs. The interpretation of the error in residual heterogeneity in the results of analysis of powder materials and calculations of a smallest mass of representative sample is given when analyzing of such materials.
format Article
id doaj-art-727d93180dfc400fa9ada4fbb5d66761
institution DOAJ
issn 2077-1177
language Russian
publishDate 2017-05-01
publisher Ural Research Institute of Metrology
record_format Article
series Стандартные образцы
spelling doaj-art-727d93180dfc400fa9ada4fbb5d667612025-08-20T02:56:39ZrusUral Research Institute of MetrologyСтандартные образцы2077-11772017-05-0103929932Development of a plant reference material for composition of a cement raw mixtureA. N. Smagunova0I. S. Shirokolobova1V. A. Kozlov2E. N. Korzhova3O. S. Krivchenko4L. P. Shaulina5A. L. Finkelshtein6ФГБОУ ВПО «Иркутский государственный университет»ФГБОУ ВПО «Иркутский государственный университет»ФГБОУ ВПО «Иркутский государственный университет»ФГБОУ ВПО «Иркутский государственный университет»ОАО «Ангарскцемент»ФГБОУ ВПО «Иркутский государственный университет»ФГБУН «Институт геохимии им . А . П . Виноградова СО РАН»A plant reference material (RM) was developed, which was certified in the content of fluorine-ion (% wt) in the cement raw mixture (PRM - 1 CM). Its metrological characteristics were set on the basis of results ofpotentiometric, photometric and titrimetric methods of analysis. The substantiation of the need for RM is given to increase the accuracy of results when determining fluorine in materials of cement production. The conditions are defined to use X-ray fluorescence method for estimating the material homogeneity in developing similar RMs. The interpretation of the error in residual heterogeneity in the results of analysis of powder materials and calculations of a smallest mass of representative sample is given when analyzing of such materials.https://www.rmjournal.ru/jour/article/view/32стандартный образецаттестованное содержание и его погрешностьостаточная неоднородностьнаименьшая масса представительной навескимежлабораторный экспериментreference materialcertified content and its errorthe residual heterogeneitythe smallest mass of representative sampleinter-laboratory experiment
spellingShingle A. N. Smagunova
I. S. Shirokolobova
V. A. Kozlov
E. N. Korzhova
O. S. Krivchenko
L. P. Shaulina
A. L. Finkelshtein
Development of a plant reference material for composition of a cement raw mixture
Стандартные образцы
стандартный образец
аттестованное содержание и его погрешность
остаточная неоднородность
наименьшая масса представительной навески
межлабораторный эксперимент
reference material
certified content and its error
the residual heterogeneity
the smallest mass of representative sample
inter-laboratory experiment
title Development of a plant reference material for composition of a cement raw mixture
title_full Development of a plant reference material for composition of a cement raw mixture
title_fullStr Development of a plant reference material for composition of a cement raw mixture
title_full_unstemmed Development of a plant reference material for composition of a cement raw mixture
title_short Development of a plant reference material for composition of a cement raw mixture
title_sort development of a plant reference material for composition of a cement raw mixture
topic стандартный образец
аттестованное содержание и его погрешность
остаточная неоднородность
наименьшая масса представительной навески
межлабораторный эксперимент
reference material
certified content and its error
the residual heterogeneity
the smallest mass of representative sample
inter-laboratory experiment
url https://www.rmjournal.ru/jour/article/view/32
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AT enkorzhova developmentofaplantreferencematerialforcompositionofacementrawmixture
AT oskrivchenko developmentofaplantreferencematerialforcompositionofacementrawmixture
AT lpshaulina developmentofaplantreferencematerialforcompositionofacementrawmixture
AT alfinkelshtein developmentofaplantreferencematerialforcompositionofacementrawmixture