Controllable synthesis of transition metal-modified molybdenum carbide crystalline phases and its application on hydrodeoxygenation of phenol

Biomass energy is a kind of energy that can play an important supporting role in the future. In-situ hydrogenation of biomass reduces the consumption of hydrogen and lowers the cost of production, so the focus on in-situ hydrogenation of bio-oils is of great green chemistry and practical significanc...

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Main Authors: Yang Ying, Li Yaru, Guo Aijun, Zhang Shuaixin, Xu Kunyu
Format: Article
Language:English
Published: EDP Sciences 2025-01-01
Series:E3S Web of Conferences
Online Access:https://www.e3s-conferences.org/articles/e3sconf/pdf/2025/25/e3sconf_iceree2025_01016.pdf
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author Yang Ying
Li Yaru
Guo Aijun
Zhang Shuaixin
Xu Kunyu
author_facet Yang Ying
Li Yaru
Guo Aijun
Zhang Shuaixin
Xu Kunyu
author_sort Yang Ying
collection DOAJ
description Biomass energy is a kind of energy that can play an important supporting role in the future. In-situ hydrogenation of biomass reduces the consumption of hydrogen and lowers the cost of production, so the focus on in-situ hydrogenation of bio-oils is of great green chemistry and practical significance, which can significantly reduce the cost of producing bio-oils with high combustion performance to replace fossil fuels. In this paper, a series of nickel-modified molybdenum carbide catalysts (Ni-MoxC) with two crystalline phase structures simultaneously were prepared by one-step pyrolysis based on organic-inorganic hybrid precursors. As-synthesized molybdenum carbide materials were characterized by XRD, XPS and so on. It was found that the synthesized molybdenum carbide catalysts exhibited good catalytic performance for the hydrodeoxygenation of phenol, with the conversion and selectivity of phenol and cyclohexanol being 95.1% and 93.4%, respectively, in which methanol and water were the most green hydrogen supply media.
format Article
id doaj-art-71860928df0443dc8bbdd764ba2f0b8b
institution Kabale University
issn 2267-1242
language English
publishDate 2025-01-01
publisher EDP Sciences
record_format Article
series E3S Web of Conferences
spelling doaj-art-71860928df0443dc8bbdd764ba2f0b8b2025-08-20T03:53:51ZengEDP SciencesE3S Web of Conferences2267-12422025-01-016250101610.1051/e3sconf/202562501016e3sconf_iceree2025_01016Controllable synthesis of transition metal-modified molybdenum carbide crystalline phases and its application on hydrodeoxygenation of phenolYang Ying0Li Yaru1Guo Aijun2Zhang Shuaixin3Xu Kunyu4College of Chemistry and Chemical Engineering, China University of Petroleum (East China)College of Chemistry and Chemical Engineering, China University of Petroleum (East China)College of Chemistry and Chemical Engineering, China University of Petroleum (East China)College of Chemistry and Chemical Engineering, China University of Petroleum (East China)College of Chemistry and Chemical Engineering, China University of Petroleum (East China)Biomass energy is a kind of energy that can play an important supporting role in the future. In-situ hydrogenation of biomass reduces the consumption of hydrogen and lowers the cost of production, so the focus on in-situ hydrogenation of bio-oils is of great green chemistry and practical significance, which can significantly reduce the cost of producing bio-oils with high combustion performance to replace fossil fuels. In this paper, a series of nickel-modified molybdenum carbide catalysts (Ni-MoxC) with two crystalline phase structures simultaneously were prepared by one-step pyrolysis based on organic-inorganic hybrid precursors. As-synthesized molybdenum carbide materials were characterized by XRD, XPS and so on. It was found that the synthesized molybdenum carbide catalysts exhibited good catalytic performance for the hydrodeoxygenation of phenol, with the conversion and selectivity of phenol and cyclohexanol being 95.1% and 93.4%, respectively, in which methanol and water were the most green hydrogen supply media.https://www.e3s-conferences.org/articles/e3sconf/pdf/2025/25/e3sconf_iceree2025_01016.pdf
spellingShingle Yang Ying
Li Yaru
Guo Aijun
Zhang Shuaixin
Xu Kunyu
Controllable synthesis of transition metal-modified molybdenum carbide crystalline phases and its application on hydrodeoxygenation of phenol
E3S Web of Conferences
title Controllable synthesis of transition metal-modified molybdenum carbide crystalline phases and its application on hydrodeoxygenation of phenol
title_full Controllable synthesis of transition metal-modified molybdenum carbide crystalline phases and its application on hydrodeoxygenation of phenol
title_fullStr Controllable synthesis of transition metal-modified molybdenum carbide crystalline phases and its application on hydrodeoxygenation of phenol
title_full_unstemmed Controllable synthesis of transition metal-modified molybdenum carbide crystalline phases and its application on hydrodeoxygenation of phenol
title_short Controllable synthesis of transition metal-modified molybdenum carbide crystalline phases and its application on hydrodeoxygenation of phenol
title_sort controllable synthesis of transition metal modified molybdenum carbide crystalline phases and its application on hydrodeoxygenation of phenol
url https://www.e3s-conferences.org/articles/e3sconf/pdf/2025/25/e3sconf_iceree2025_01016.pdf
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AT liyaru controllablesynthesisoftransitionmetalmodifiedmolybdenumcarbidecrystallinephasesanditsapplicationonhydrodeoxygenationofphenol
AT guoaijun controllablesynthesisoftransitionmetalmodifiedmolybdenumcarbidecrystallinephasesanditsapplicationonhydrodeoxygenationofphenol
AT zhangshuaixin controllablesynthesisoftransitionmetalmodifiedmolybdenumcarbidecrystallinephasesanditsapplicationonhydrodeoxygenationofphenol
AT xukunyu controllablesynthesisoftransitionmetalmodifiedmolybdenumcarbidecrystallinephasesanditsapplicationonhydrodeoxygenationofphenol