Synthesis of Some Salicylaldehyde-Based Schiff Bases in Aqueous Media
A new efficient and environmental friendly procedure for the synthesis of a series of salicylaldehyde-based schiff bases under microwave irradiation is described. The method is compared with the conventional method also. The present work involves condensation of salicylaldehyde with various aromatic...
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| Format: | Article |
| Language: | English |
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Wiley
2013-01-01
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| Series: | Journal of Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2013/909217 |
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| author | Sunita Bhagat Nutan Sharma Tejpal Singh Chundawat |
| author_facet | Sunita Bhagat Nutan Sharma Tejpal Singh Chundawat |
| author_sort | Sunita Bhagat |
| collection | DOAJ |
| description | A new efficient and environmental friendly procedure for the synthesis of a series of salicylaldehyde-based schiff bases under microwave irradiation is described. The method is compared with the conventional method also. The present work involves condensation of salicylaldehyde with various aromatic amines in water under microwave irradiation. A judicious choice of the solvent and reaction conditions allowed the final products to be generated in excellent yields in a one-step procedure, whereas experiments under thermal conditions led to lower yields with tedious work-up. Microwave irradiation method gives advantages like reduction in reaction time, increase in conversion, reduced wastes, and good yields. The structures of synthesized compounds were confirmed by IR, 1HNMR, and Mass Spectra data. |
| format | Article |
| id | doaj-art-6fddee708faf4db3a6fe950baf715fbc |
| institution | DOAJ |
| issn | 2090-9063 2090-9071 |
| language | English |
| publishDate | 2013-01-01 |
| publisher | Wiley |
| record_format | Article |
| series | Journal of Chemistry |
| spelling | doaj-art-6fddee708faf4db3a6fe950baf715fbc2025-08-20T03:19:15ZengWileyJournal of Chemistry2090-90632090-90712013-01-01201310.1155/2013/909217909217Synthesis of Some Salicylaldehyde-Based Schiff Bases in Aqueous MediaSunita Bhagat0Nutan Sharma1Tejpal Singh Chundawat2Organic Synthesis Research Laboratory, Department of Chemistry, A.R.S.D. College, University of Delhi, New Delhi 110021, IndiaOrganic Synthesis Research Laboratory, Department of Chemistry, A.R.S.D. College, University of Delhi, New Delhi 110021, IndiaOrganic Synthesis Research Laboratory, Department of Chemistry, A.R.S.D. College, University of Delhi, New Delhi 110021, IndiaA new efficient and environmental friendly procedure for the synthesis of a series of salicylaldehyde-based schiff bases under microwave irradiation is described. The method is compared with the conventional method also. The present work involves condensation of salicylaldehyde with various aromatic amines in water under microwave irradiation. A judicious choice of the solvent and reaction conditions allowed the final products to be generated in excellent yields in a one-step procedure, whereas experiments under thermal conditions led to lower yields with tedious work-up. Microwave irradiation method gives advantages like reduction in reaction time, increase in conversion, reduced wastes, and good yields. The structures of synthesized compounds were confirmed by IR, 1HNMR, and Mass Spectra data.http://dx.doi.org/10.1155/2013/909217 |
| spellingShingle | Sunita Bhagat Nutan Sharma Tejpal Singh Chundawat Synthesis of Some Salicylaldehyde-Based Schiff Bases in Aqueous Media Journal of Chemistry |
| title | Synthesis of Some Salicylaldehyde-Based Schiff Bases in Aqueous Media |
| title_full | Synthesis of Some Salicylaldehyde-Based Schiff Bases in Aqueous Media |
| title_fullStr | Synthesis of Some Salicylaldehyde-Based Schiff Bases in Aqueous Media |
| title_full_unstemmed | Synthesis of Some Salicylaldehyde-Based Schiff Bases in Aqueous Media |
| title_short | Synthesis of Some Salicylaldehyde-Based Schiff Bases in Aqueous Media |
| title_sort | synthesis of some salicylaldehyde based schiff bases in aqueous media |
| url | http://dx.doi.org/10.1155/2013/909217 |
| work_keys_str_mv | AT sunitabhagat synthesisofsomesalicylaldehydebasedschiffbasesinaqueousmedia AT nutansharma synthesisofsomesalicylaldehydebasedschiffbasesinaqueousmedia AT tejpalsinghchundawat synthesisofsomesalicylaldehydebasedschiffbasesinaqueousmedia |