Processing of Thermoelectric Fe2VAl Heusler-compounds by laser powder bed fusion: From single scan tracks to bulk material

In the present study, the n-type Fe2 VAl0.9 Si0.1 was printed by laser powder bed fusion (L-PBF) for the first time. This work highlights the complexity of processing non-metallic materials by L-PBF and the need for advanced optimization strategies. A Single Scan Tracks (SSTs) analysis was conducted...

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Main Authors: M. Delcroix, G. Roy, C. van der Rest, V. Marchal-Marchant, P.J. Jacques
Format: Article
Language:English
Published: Elsevier 2025-07-01
Series:Additive Manufacturing Letters
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Online Access:http://www.sciencedirect.com/science/article/pii/S2772369025000386
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author M. Delcroix
G. Roy
C. van der Rest
V. Marchal-Marchant
P.J. Jacques
author_facet M. Delcroix
G. Roy
C. van der Rest
V. Marchal-Marchant
P.J. Jacques
author_sort M. Delcroix
collection DOAJ
description In the present study, the n-type Fe2 VAl0.9 Si0.1 was printed by laser powder bed fusion (L-PBF) for the first time. This work highlights the complexity of processing non-metallic materials by L-PBF and the need for advanced optimization strategies. A Single Scan Tracks (SSTs) analysis was conducted as usually done for materials newly processed by L-PBF as well as a top-down approach based on printing parameters of stainless steel. Process parameter sets based on SST analysis led to overheating while the stainless-steel-based strategy successfully produced bulk samples. Printed samples transitioned rapidly from cold defects (i.e. lack-of-fusion) to overheating as the printing parameters were varied. Moreover, high density samples were printed with parameters that would produce insufficient melting in the case of SSTs. Successive parallel tracks were printed and revealed a transition from unmelting to balling to continuous densification, demonstrating the critical role of heat accumulation. The microstructure of printed samples was analyzed, and their thermoelectric properties were measured. Transverse cold cracks, perpendicular to the scanning direction were observed. Statistical analysis on SST demonstrated that these cracks were insensitive to laser parameter variations, significantly decreasing the thermoelectric performance of bulk samples.
format Article
id doaj-art-6fbd28dd253b45b89bd8fbd8f4bdfb2d
institution Kabale University
issn 2772-3690
language English
publishDate 2025-07-01
publisher Elsevier
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series Additive Manufacturing Letters
spelling doaj-art-6fbd28dd253b45b89bd8fbd8f4bdfb2d2025-08-21T04:17:55ZengElsevierAdditive Manufacturing Letters2772-36902025-07-011410030510.1016/j.addlet.2025.100305Processing of Thermoelectric Fe2VAl Heusler-compounds by laser powder bed fusion: From single scan tracks to bulk materialM. Delcroix0G. Roy1C. van der Rest2V. Marchal-Marchant3P.J. Jacques4Corresponding author.; UCLouvain, Institute of Mechanics, Materials and Civil Engineering (IMMC), Materials and Process Engineering (IMAP), Réaumur, Place Sainte Barbe 2, 1348 Louvain-la-Neuve, BelgiumUCLouvain, Institute of Mechanics, Materials and Civil Engineering (IMMC), Materials and Process Engineering (IMAP), Réaumur, Place Sainte Barbe 2, 1348 Louvain-la-Neuve, BelgiumUCLouvain, Institute of Mechanics, Materials and Civil Engineering (IMMC), Materials and Process Engineering (IMAP), Réaumur, Place Sainte Barbe 2, 1348 Louvain-la-Neuve, BelgiumUCLouvain, Institute of Mechanics, Materials and Civil Engineering (IMMC), Materials and Process Engineering (IMAP), Réaumur, Place Sainte Barbe 2, 1348 Louvain-la-Neuve, BelgiumUCLouvain, Institute of Mechanics, Materials and Civil Engineering (IMMC), Materials and Process Engineering (IMAP), Réaumur, Place Sainte Barbe 2, 1348 Louvain-la-Neuve, BelgiumIn the present study, the n-type Fe2 VAl0.9 Si0.1 was printed by laser powder bed fusion (L-PBF) for the first time. This work highlights the complexity of processing non-metallic materials by L-PBF and the need for advanced optimization strategies. A Single Scan Tracks (SSTs) analysis was conducted as usually done for materials newly processed by L-PBF as well as a top-down approach based on printing parameters of stainless steel. Process parameter sets based on SST analysis led to overheating while the stainless-steel-based strategy successfully produced bulk samples. Printed samples transitioned rapidly from cold defects (i.e. lack-of-fusion) to overheating as the printing parameters were varied. Moreover, high density samples were printed with parameters that would produce insufficient melting in the case of SSTs. Successive parallel tracks were printed and revealed a transition from unmelting to balling to continuous densification, demonstrating the critical role of heat accumulation. The microstructure of printed samples was analyzed, and their thermoelectric properties were measured. Transverse cold cracks, perpendicular to the scanning direction were observed. Statistical analysis on SST demonstrated that these cracks were insensitive to laser parameter variations, significantly decreasing the thermoelectric performance of bulk samples.http://www.sciencedirect.com/science/article/pii/S2772369025000386HeuslerThermoelectricAdditive manufacturingSingle scan trackCrack defects
spellingShingle M. Delcroix
G. Roy
C. van der Rest
V. Marchal-Marchant
P.J. Jacques
Processing of Thermoelectric Fe2VAl Heusler-compounds by laser powder bed fusion: From single scan tracks to bulk material
Additive Manufacturing Letters
Heusler
Thermoelectric
Additive manufacturing
Single scan track
Crack defects
title Processing of Thermoelectric Fe2VAl Heusler-compounds by laser powder bed fusion: From single scan tracks to bulk material
title_full Processing of Thermoelectric Fe2VAl Heusler-compounds by laser powder bed fusion: From single scan tracks to bulk material
title_fullStr Processing of Thermoelectric Fe2VAl Heusler-compounds by laser powder bed fusion: From single scan tracks to bulk material
title_full_unstemmed Processing of Thermoelectric Fe2VAl Heusler-compounds by laser powder bed fusion: From single scan tracks to bulk material
title_short Processing of Thermoelectric Fe2VAl Heusler-compounds by laser powder bed fusion: From single scan tracks to bulk material
title_sort processing of thermoelectric fe2val heusler compounds by laser powder bed fusion from single scan tracks to bulk material
topic Heusler
Thermoelectric
Additive manufacturing
Single scan track
Crack defects
url http://www.sciencedirect.com/science/article/pii/S2772369025000386
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