Multi-walled carbon nanotubes reinforced Inconel 718 superalloy fabricated by spark plasma sintering: Microstructure and mechanical property

To investigate the densification and strengthening mechanisms of MWCNT/Inconel 718 composites, samples with different MWCNTs content are fabricated by spark plasma sintering (SPS) at varying sintering temperatures. The densification process, the room-temperature flexural and compression properties,...

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Main Authors: Z.J. Han, L.Y. Ma, Q.S. Feng, B. Meng, M. Wan
Format: Article
Language:English
Published: Elsevier 2025-01-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785424028874
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author Z.J. Han
L.Y. Ma
Q.S. Feng
B. Meng
M. Wan
author_facet Z.J. Han
L.Y. Ma
Q.S. Feng
B. Meng
M. Wan
author_sort Z.J. Han
collection DOAJ
description To investigate the densification and strengthening mechanisms of MWCNT/Inconel 718 composites, samples with different MWCNTs content are fabricated by spark plasma sintering (SPS) at varying sintering temperatures. The densification process, the room-temperature flexural and compression properties, the mechanical properties at high temperatures, and microstructure evolution are discussed. Increasing the sintering temperature improves material densification by reducing the number of indented pores and gully defects in the heating and holding stage. The incorporation of MWCNTs, though impeding material density by affecting the bonding of powder particles, can enhance the mechanical properties of the composites through load transfer and Orowan strengthening mechanisms. The composites prepared at 1050 °C with 0.5% MWCNTs content show a high relative density of 97%, a flexural strength of 1090 MPa, a compressive strength of 1523 MPa, and a high-temperature (1200 K) compression strength of 138.5 MPa, which are all much higher than that of Inconel 718 alloy. Finally, turbine blades with complex curved areas are prepared at a temperature of 1050 °C and an MWCNTs content of 0.5%, providing a new idea for forming high-strength superalloy matrix composites that can withstand ultra-high temperatures.
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spelling doaj-art-6e9d40226d9940ebaeb55368b81c139d2025-01-19T06:25:22ZengElsevierJournal of Materials Research and Technology2238-78542025-01-0134972986Multi-walled carbon nanotubes reinforced Inconel 718 superalloy fabricated by spark plasma sintering: Microstructure and mechanical propertyZ.J. Han0L.Y. Ma1Q.S. Feng2B. Meng3M. Wan4School of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, PR China; Ningbo Institute of Technology, Beihang University, Ningbo, 315832, PR ChinaSchool of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, PR China; Ningbo Institute of Technology, Beihang University, Ningbo, 315832, PR China; School of Mechanical Engineering, Hebei University of Architecture, Zhangjiakou 075051, PR ChinaSchool of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, PR China; Ningbo Institute of Technology, Beihang University, Ningbo, 315832, PR ChinaSchool of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, PR China; Ningbo Institute of Technology, Beihang University, Ningbo, 315832, PR China; Corresponding author. School of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, PR China.School of Mechanical Engineering and Automation, Beihang University, Beijing, 100191, PR China; Ningbo Institute of Technology, Beihang University, Ningbo, 315832, PR ChinaTo investigate the densification and strengthening mechanisms of MWCNT/Inconel 718 composites, samples with different MWCNTs content are fabricated by spark plasma sintering (SPS) at varying sintering temperatures. The densification process, the room-temperature flexural and compression properties, the mechanical properties at high temperatures, and microstructure evolution are discussed. Increasing the sintering temperature improves material densification by reducing the number of indented pores and gully defects in the heating and holding stage. The incorporation of MWCNTs, though impeding material density by affecting the bonding of powder particles, can enhance the mechanical properties of the composites through load transfer and Orowan strengthening mechanisms. The composites prepared at 1050 °C with 0.5% MWCNTs content show a high relative density of 97%, a flexural strength of 1090 MPa, a compressive strength of 1523 MPa, and a high-temperature (1200 K) compression strength of 138.5 MPa, which are all much higher than that of Inconel 718 alloy. Finally, turbine blades with complex curved areas are prepared at a temperature of 1050 °C and an MWCNTs content of 0.5%, providing a new idea for forming high-strength superalloy matrix composites that can withstand ultra-high temperatures.http://www.sciencedirect.com/science/article/pii/S2238785424028874MWCNT/Inconel 718 compositesSpark plasma sinteringDensificationStrengthening mechanismMicrostructure
spellingShingle Z.J. Han
L.Y. Ma
Q.S. Feng
B. Meng
M. Wan
Multi-walled carbon nanotubes reinforced Inconel 718 superalloy fabricated by spark plasma sintering: Microstructure and mechanical property
Journal of Materials Research and Technology
MWCNT/Inconel 718 composites
Spark plasma sintering
Densification
Strengthening mechanism
Microstructure
title Multi-walled carbon nanotubes reinforced Inconel 718 superalloy fabricated by spark plasma sintering: Microstructure and mechanical property
title_full Multi-walled carbon nanotubes reinforced Inconel 718 superalloy fabricated by spark plasma sintering: Microstructure and mechanical property
title_fullStr Multi-walled carbon nanotubes reinforced Inconel 718 superalloy fabricated by spark plasma sintering: Microstructure and mechanical property
title_full_unstemmed Multi-walled carbon nanotubes reinforced Inconel 718 superalloy fabricated by spark plasma sintering: Microstructure and mechanical property
title_short Multi-walled carbon nanotubes reinforced Inconel 718 superalloy fabricated by spark plasma sintering: Microstructure and mechanical property
title_sort multi walled carbon nanotubes reinforced inconel 718 superalloy fabricated by spark plasma sintering microstructure and mechanical property
topic MWCNT/Inconel 718 composites
Spark plasma sintering
Densification
Strengthening mechanism
Microstructure
url http://www.sciencedirect.com/science/article/pii/S2238785424028874
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