Three-Dimensional Supramolecular Network Directed by Intermolecular Interactions in [Pb2(dmp)2(hfacac)4]

To investigate the interactions between noncovalent bond donor and acceptor giving rise to three dimensional networks, compound [Pb2(dmp)2(hfacac)2] (1) (dmp = 2,9-dimethyl-1,10-henanthroline and Hhfacac = hexafluoroacetylacetonate) has been prepared and characterized by elemental analysis, IR, 1H N...

Full description

Saved in:
Bibliographic Details
Main Authors: Farzin Marandi, Lotfali Saghatforoush, Hossein Farzaneh
Format: Article
Language:English
Published: Wiley 2009-01-01
Series:E-Journal of Chemistry
Online Access:http://dx.doi.org/10.1155/2009/673828
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849414480358801408
author Farzin Marandi
Lotfali Saghatforoush
Hossein Farzaneh
author_facet Farzin Marandi
Lotfali Saghatforoush
Hossein Farzaneh
author_sort Farzin Marandi
collection DOAJ
description To investigate the interactions between noncovalent bond donor and acceptor giving rise to three dimensional networks, compound [Pb2(dmp)2(hfacac)2] (1) (dmp = 2,9-dimethyl-1,10-henanthroline and Hhfacac = hexafluoroacetylacetonate) has been prepared and characterized by elemental analysis, IR, 1H NMR, and 13C NMR spectroscopy and its crystal structures was investigated. The single crystal structure show the coordination number of Pb(II) to be eight with two N-donor atoms from a “dmp” ligand and six O-donors from the anionic ligands. The supramolecular structure of 1 is realized by weak directional C–H∙∙∙O–C, C–F∙∙∙F–C and π–π stacking interactions.
format Article
id doaj-art-6dfec18932994337ac06024fcbc98ca1
institution Kabale University
issn 0973-4945
2090-9810
language English
publishDate 2009-01-01
publisher Wiley
record_format Article
series E-Journal of Chemistry
spelling doaj-art-6dfec18932994337ac06024fcbc98ca12025-08-20T03:33:50ZengWileyE-Journal of Chemistry0973-49452090-98102009-01-01641085109010.1155/2009/673828Three-Dimensional Supramolecular Network Directed by Intermolecular Interactions in [Pb2(dmp)2(hfacac)4]Farzin Marandi0Lotfali Saghatforoush1Hossein Farzaneh2Department of Science, Payame Noor University (PNU), Zanjan, IranDepartment of Science, Payame Noor University (PNU), Khoy, IranDepartment of Science, Zanjan University, Zanjan, IranTo investigate the interactions between noncovalent bond donor and acceptor giving rise to three dimensional networks, compound [Pb2(dmp)2(hfacac)2] (1) (dmp = 2,9-dimethyl-1,10-henanthroline and Hhfacac = hexafluoroacetylacetonate) has been prepared and characterized by elemental analysis, IR, 1H NMR, and 13C NMR spectroscopy and its crystal structures was investigated. The single crystal structure show the coordination number of Pb(II) to be eight with two N-donor atoms from a “dmp” ligand and six O-donors from the anionic ligands. The supramolecular structure of 1 is realized by weak directional C–H∙∙∙O–C, C–F∙∙∙F–C and π–π stacking interactions.http://dx.doi.org/10.1155/2009/673828
spellingShingle Farzin Marandi
Lotfali Saghatforoush
Hossein Farzaneh
Three-Dimensional Supramolecular Network Directed by Intermolecular Interactions in [Pb2(dmp)2(hfacac)4]
E-Journal of Chemistry
title Three-Dimensional Supramolecular Network Directed by Intermolecular Interactions in [Pb2(dmp)2(hfacac)4]
title_full Three-Dimensional Supramolecular Network Directed by Intermolecular Interactions in [Pb2(dmp)2(hfacac)4]
title_fullStr Three-Dimensional Supramolecular Network Directed by Intermolecular Interactions in [Pb2(dmp)2(hfacac)4]
title_full_unstemmed Three-Dimensional Supramolecular Network Directed by Intermolecular Interactions in [Pb2(dmp)2(hfacac)4]
title_short Three-Dimensional Supramolecular Network Directed by Intermolecular Interactions in [Pb2(dmp)2(hfacac)4]
title_sort three dimensional supramolecular network directed by intermolecular interactions in pb2 dmp 2 hfacac 4
url http://dx.doi.org/10.1155/2009/673828
work_keys_str_mv AT farzinmarandi threedimensionalsupramolecularnetworkdirectedbyintermolecularinteractionsinpb2dmp2hfacac4
AT lotfalisaghatforoush threedimensionalsupramolecularnetworkdirectedbyintermolecularinteractionsinpb2dmp2hfacac4
AT hosseinfarzaneh threedimensionalsupramolecularnetworkdirectedbyintermolecularinteractionsinpb2dmp2hfacac4