Improvements in manufacturability, bonding strength, and curing efficiency of a silicone adhesive

Two-component room temperature vulcanizing silicone adhesive RTV566 with a lower elastic modulus has been widely used in precision optomechanical products such as remote sensors and aerospace infrared cameras. However, the silicone adhesive is of poor manufacturability due to its extremely high visc...

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Main Authors: Ye Yang, Jinfeng Xu, Xusheng Chen, Wang Yang, Lina Si, Hongjuan Yan, Zhaoliang Dou, Fengbin Liu, Huanxiong Xia
Format: Article
Language:English
Published: Elsevier 2024-11-01
Series:Journal of Advanced Joining Processes
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2666330924000591
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author Ye Yang
Jinfeng Xu
Xusheng Chen
Wang Yang
Lina Si
Hongjuan Yan
Zhaoliang Dou
Fengbin Liu
Huanxiong Xia
author_facet Ye Yang
Jinfeng Xu
Xusheng Chen
Wang Yang
Lina Si
Hongjuan Yan
Zhaoliang Dou
Fengbin Liu
Huanxiong Xia
author_sort Ye Yang
collection DOAJ
description Two-component room temperature vulcanizing silicone adhesive RTV566 with a lower elastic modulus has been widely used in precision optomechanical products such as remote sensors and aerospace infrared cameras. However, the silicone adhesive is of poor manufacturability due to its extremely high viscosity, and the bonded joint usually exhibits low bonding strength and requires a long curing time. This paper investigates a way to improve both the adhesion strength and curing efficiency of Invar alloy and optical glass with RTV566 through single-lap experiments. It is found that adding small amounts of acetone and water can significantly reduce the viscosity, enhance the bonding strength, and shorten the curing time. The viscosity can be reduced by 63.4 % and the bonding strength can be improved by 136.4 % with the weight ratio of adhesive to acetone being 20:2. Moreover, a little amount of water in the weight ratio of 100:10:0.1 (adhesive: acetone: water) can shorten the curing time from 7 days to 4 days without harms to the bonding strength and elastic modulus. As to the mechanism, the silicone adhesive can be dissolved by acetone and its sulfuration reaction can be enhanced by water, resulting in good manufacturability and high curing efficiency. This work contributes a novel and easy-to-use method to greatly improve the performances of the bonding process of precision optical structures.
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spelling doaj-art-6bfbe984d10544dba8317685d76534862025-08-20T01:59:35ZengElsevierJournal of Advanced Joining Processes2666-33092024-11-011010024310.1016/j.jajp.2024.100243Improvements in manufacturability, bonding strength, and curing efficiency of a silicone adhesiveYe Yang0Jinfeng Xu1Xusheng Chen2Wang Yang3Lina Si4Hongjuan Yan5Zhaoliang Dou6Fengbin Liu7Huanxiong Xia8School of Mechanical and Material Engineering, North China University of Technology, Beijing 100144, PR ChinaSchool of Mechanical and Material Engineering, North China University of Technology, Beijing 100144, PR ChinaSchool of Mechanical and Material Engineering, North China University of Technology, Beijing 100144, PR ChinaGalaxy Space, Beijing 100089, PR ChinaSchool of Mechanical and Material Engineering, North China University of Technology, Beijing 100144, PR ChinaSchool of Mechanical and Material Engineering, North China University of Technology, Beijing 100144, PR ChinaSchool of Mechanical and Material Engineering, North China University of Technology, Beijing 100144, PR ChinaSchool of Mechanical and Material Engineering, North China University of Technology, Beijing 100144, PR ChinaSchool of Mechanical Engineering, Beijing Institute of Technology, Beijing 100081, PR China; Corresponding author.Two-component room temperature vulcanizing silicone adhesive RTV566 with a lower elastic modulus has been widely used in precision optomechanical products such as remote sensors and aerospace infrared cameras. However, the silicone adhesive is of poor manufacturability due to its extremely high viscosity, and the bonded joint usually exhibits low bonding strength and requires a long curing time. This paper investigates a way to improve both the adhesion strength and curing efficiency of Invar alloy and optical glass with RTV566 through single-lap experiments. It is found that adding small amounts of acetone and water can significantly reduce the viscosity, enhance the bonding strength, and shorten the curing time. The viscosity can be reduced by 63.4 % and the bonding strength can be improved by 136.4 % with the weight ratio of adhesive to acetone being 20:2. Moreover, a little amount of water in the weight ratio of 100:10:0.1 (adhesive: acetone: water) can shorten the curing time from 7 days to 4 days without harms to the bonding strength and elastic modulus. As to the mechanism, the silicone adhesive can be dissolved by acetone and its sulfuration reaction can be enhanced by water, resulting in good manufacturability and high curing efficiency. This work contributes a novel and easy-to-use method to greatly improve the performances of the bonding process of precision optical structures.http://www.sciencedirect.com/science/article/pii/S2666330924000591Adhesive bondingSilicone adhesiveBonding strengthCuringAcetone
spellingShingle Ye Yang
Jinfeng Xu
Xusheng Chen
Wang Yang
Lina Si
Hongjuan Yan
Zhaoliang Dou
Fengbin Liu
Huanxiong Xia
Improvements in manufacturability, bonding strength, and curing efficiency of a silicone adhesive
Journal of Advanced Joining Processes
Adhesive bonding
Silicone adhesive
Bonding strength
Curing
Acetone
title Improvements in manufacturability, bonding strength, and curing efficiency of a silicone adhesive
title_full Improvements in manufacturability, bonding strength, and curing efficiency of a silicone adhesive
title_fullStr Improvements in manufacturability, bonding strength, and curing efficiency of a silicone adhesive
title_full_unstemmed Improvements in manufacturability, bonding strength, and curing efficiency of a silicone adhesive
title_short Improvements in manufacturability, bonding strength, and curing efficiency of a silicone adhesive
title_sort improvements in manufacturability bonding strength and curing efficiency of a silicone adhesive
topic Adhesive bonding
Silicone adhesive
Bonding strength
Curing
Acetone
url http://www.sciencedirect.com/science/article/pii/S2666330924000591
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