4-Methyl-<i>N</i>-(1-benzyl)-<i>N</i>’-(1-benzylidene)benzenesulfonohydrazide

4-Methyl-<i>N</i>-(1-benzyl)-<i>N</i>’-(1-benzylidene)benzenesulfonohydrazide

4-Methyl-<i>N</i>-(1-benzyl)-<i>N</i>’-(1-benzylidene)benzenesulfonohydrazide is formed through a direct, solventless reaction between benzaldehyde tosylhydrazone and potassium carbonate, which is carried out using an eco-friendly grinding method. The NMR spectra of the compo...

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Bibliographic Details
Main Authors: Leticia Almazán-Sánchez, Marco A. García-Eleno, Diego Martínez-Otero, Erick Cuevas-Yañez
Format: Article
Language:English
Published: MDPI AG 2025-06-01
Series:Molbank
Subjects:
tosylhydrazone
sulfonohydrazide
carbene insertion
crystal structure
Online Access:https://www.mdpi.com/1422-8599/2025/2/M2022
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Summary:4-Methyl-<i>N</i>-(1-benzyl)-<i>N</i>’-(1-benzylidene)benzenesulfonohydrazide is formed through a direct, solventless reaction between benzaldehyde tosylhydrazone and potassium carbonate, which is carried out using an eco-friendly grinding method. The NMR spectra of the compound are here described. The structure was unequivocally determined by X-ray analysis. As suggested by Hirshfeld surface analysis, the predominant intermolecular H-O interactions in this molecule are involved in crystal packing.
ISSN:1422-8599

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