Manipulating Li2S Redox Kinetics and Lithium Dendrites by Core–Shell Catalysts under High Sulfur Loading and Lean‐Electrolyte Conditions

Abstract For practical lithium–sulfur batteries (LSBs), the high sulfur loading and lean‐electrolyte are necessary conditions to achieve the high energy density. However, such extreme conditions will cause serious battery performance fading, due to the uncontrolled deposition of Li2S and lithium den...

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Main Authors: Mengmeng Zhen, Kaifeng Li, Mingyang Liu
Format: Article
Language:English
Published: Wiley 2023-05-01
Series:Advanced Science
Subjects:
Online Access:https://doi.org/10.1002/advs.202207442
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author Mengmeng Zhen
Kaifeng Li
Mingyang Liu
author_facet Mengmeng Zhen
Kaifeng Li
Mingyang Liu
author_sort Mengmeng Zhen
collection DOAJ
description Abstract For practical lithium–sulfur batteries (LSBs), the high sulfur loading and lean‐electrolyte are necessary conditions to achieve the high energy density. However, such extreme conditions will cause serious battery performance fading, due to the uncontrolled deposition of Li2S and lithium dendrite growth. Herein, the tiny Co nanoparticles embedded N‐doped carbon@Co9S8 core–shell material (CoNC@Co9S8NC) is designed to address these challenges. The Co9S8NC‐shell effectively captures lithium polysulfides (LiPSs) and electrolyte, and suppresses the lithium dendrite growth. The CoNC‐core not only improves electronic conductivity, but also promotes Li+ diffusion as well as accelerates Li2S deposition/decomposition. Consequently, the cell with CoNC@Co9S8NC modified separator delivers a high specific capacity of 700 mAh g−1 with a low‐capacity decay rate of 0.035% per cycle at 1.0 C after 750 cycles under a sulfur loading of 3.2 mg cm−2 and a E/S ratio of 12 µL mg−1, and a high initial areal capacity of 9.6 mAh cm−2 under a high sulfur loading of 8.8 mg cm−2 and a low E/S ratio of 4.5 µL mg−1. Besides, the CoNC@Co9S8NC exhibits an ultralow overpotential fluctuation of 11 mV at a current density of 0.5 mA cm–2 after 1000 h during a continuous Li plating/striping process.
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spelling doaj-art-6a4c4586412d45ea91c213ac0984fc712025-08-20T04:01:01ZengWileyAdvanced Science2198-38442023-05-011014n/an/a10.1002/advs.202207442Manipulating Li2S Redox Kinetics and Lithium Dendrites by Core–Shell Catalysts under High Sulfur Loading and Lean‐Electrolyte ConditionsMengmeng Zhen0Kaifeng Li1Mingyang Liu2State Key Laboratory of Medicinal Chemical Biology Nankai University 300350 Tianjin ChinaSchool of Energy and Environmental Engineering Hebei University of Technology Tianjin 300071 ChinaState Key Laboratory of Medicinal Chemical Biology Nankai University 300350 Tianjin ChinaAbstract For practical lithium–sulfur batteries (LSBs), the high sulfur loading and lean‐electrolyte are necessary conditions to achieve the high energy density. However, such extreme conditions will cause serious battery performance fading, due to the uncontrolled deposition of Li2S and lithium dendrite growth. Herein, the tiny Co nanoparticles embedded N‐doped carbon@Co9S8 core–shell material (CoNC@Co9S8NC) is designed to address these challenges. The Co9S8NC‐shell effectively captures lithium polysulfides (LiPSs) and electrolyte, and suppresses the lithium dendrite growth. The CoNC‐core not only improves electronic conductivity, but also promotes Li+ diffusion as well as accelerates Li2S deposition/decomposition. Consequently, the cell with CoNC@Co9S8NC modified separator delivers a high specific capacity of 700 mAh g−1 with a low‐capacity decay rate of 0.035% per cycle at 1.0 C after 750 cycles under a sulfur loading of 3.2 mg cm−2 and a E/S ratio of 12 µL mg−1, and a high initial areal capacity of 9.6 mAh cm−2 under a high sulfur loading of 8.8 mg cm−2 and a low E/S ratio of 4.5 µL mg−1. Besides, the CoNC@Co9S8NC exhibits an ultralow overpotential fluctuation of 11 mV at a current density of 0.5 mA cm–2 after 1000 h during a continuous Li plating/striping process.https://doi.org/10.1002/advs.202207442lean‐electrolyteLi2S deposition/decompositionlithium dendriteslithium–sulfur batteriesredox kinetics
spellingShingle Mengmeng Zhen
Kaifeng Li
Mingyang Liu
Manipulating Li2S Redox Kinetics and Lithium Dendrites by Core–Shell Catalysts under High Sulfur Loading and Lean‐Electrolyte Conditions
Advanced Science
lean‐electrolyte
Li2S deposition/decomposition
lithium dendrites
lithium–sulfur batteries
redox kinetics
title Manipulating Li2S Redox Kinetics and Lithium Dendrites by Core–Shell Catalysts under High Sulfur Loading and Lean‐Electrolyte Conditions
title_full Manipulating Li2S Redox Kinetics and Lithium Dendrites by Core–Shell Catalysts under High Sulfur Loading and Lean‐Electrolyte Conditions
title_fullStr Manipulating Li2S Redox Kinetics and Lithium Dendrites by Core–Shell Catalysts under High Sulfur Loading and Lean‐Electrolyte Conditions
title_full_unstemmed Manipulating Li2S Redox Kinetics and Lithium Dendrites by Core–Shell Catalysts under High Sulfur Loading and Lean‐Electrolyte Conditions
title_short Manipulating Li2S Redox Kinetics and Lithium Dendrites by Core–Shell Catalysts under High Sulfur Loading and Lean‐Electrolyte Conditions
title_sort manipulating li2s redox kinetics and lithium dendrites by core shell catalysts under high sulfur loading and lean electrolyte conditions
topic lean‐electrolyte
Li2S deposition/decomposition
lithium dendrites
lithium–sulfur batteries
redox kinetics
url https://doi.org/10.1002/advs.202207442
work_keys_str_mv AT mengmengzhen manipulatingli2sredoxkineticsandlithiumdendritesbycoreshellcatalystsunderhighsulfurloadingandleanelectrolyteconditions
AT kaifengli manipulatingli2sredoxkineticsandlithiumdendritesbycoreshellcatalystsunderhighsulfurloadingandleanelectrolyteconditions
AT mingyangliu manipulatingli2sredoxkineticsandlithiumdendritesbycoreshellcatalystsunderhighsulfurloadingandleanelectrolyteconditions