N-Ethylmaleimide influenced the evaluation of disulfide cross-links in the oxidized myofibrillar proteins using the non-reducing SDS-PAGE

The present study aimed to investigate the effect of N-Ethylmaleimide (NEM) on the evaluation of disulfide formation in the oxi  dized myofibrillar proteins during the sample preparation of the non-reducing SDS-PAGE procedure. For this purpose, extracted myofibrillar proteins were oxidized firstly v...

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Main Authors: W. Wang, S. Wang, S. Li
Format: Article
Language:English
Published: The V.M. Gorbatov All-Russian Meat Research  Institute 2022-07-01
Series:Теория и практика переработки мяса
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Online Access:https://www.meatjournal.ru/jour/article/view/221
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author W. Wang
S. Wang
S. Li
author_facet W. Wang
S. Wang
S. Li
author_sort W. Wang
collection DOAJ
description The present study aimed to investigate the effect of N-Ethylmaleimide (NEM) on the evaluation of disulfide formation in the oxi  dized myofibrillar proteins during the sample preparation of the non-reducing SDS-PAGE procedure. For this purpose, extracted myofibrillar proteins were oxidized firstly via a Fenton oxidation reaction, and non-oxidized proteins were used as a control. Before running SDS-PAGE, in the sample preparation, these oxidized and non-oxidized proteins were prepared according to the three dif  ferent sample preparation methods with or without the presence of N-Ethylmaleimide or β-mercaptoethanol. Results showed that oxidized proteins treated with NEM regardless of sample preparation methods presented attenuated bands of myosin heavy chain monomer in the non-reducing SDS-PAGE gels, suggesting that the disulfide bonds formed as a result of protein oxidation could be preserved by NEM during sample preparation. Meanwhile, a possible mechanism for the effect of NEM was proposed.
format Article
id doaj-art-66153030a3ea41319b2ac53422396abb
institution DOAJ
issn 2414-438X
2414-441X
language English
publishDate 2022-07-01
publisher The V.M. Gorbatov All-Russian Meat Research  Institute
record_format Article
series Теория и практика переработки мяса
spelling doaj-art-66153030a3ea41319b2ac53422396abb2025-08-20T03:00:59ZengThe V.M. Gorbatov All-Russian Meat Research  InstituteТеория и практика переработки мяса2414-438X2414-441X2022-07-0172919610.21323/2414-438X-2022-7-2-91-96189N-Ethylmaleimide influenced the evaluation of disulfide cross-links in the oxidized myofibrillar proteins using the non-reducing SDS-PAGEW. Wang0S. Wang1S. Li2School of Food Science and Technology, Dalian Polytechnic UniversitySchool of Food Science and Technology, Dalian Polytechnic UniversitySchool of Food Science and Technology, Dalian Polytechnic University; National Engineering Research Center of SeafoodThe present study aimed to investigate the effect of N-Ethylmaleimide (NEM) on the evaluation of disulfide formation in the oxi  dized myofibrillar proteins during the sample preparation of the non-reducing SDS-PAGE procedure. For this purpose, extracted myofibrillar proteins were oxidized firstly via a Fenton oxidation reaction, and non-oxidized proteins were used as a control. Before running SDS-PAGE, in the sample preparation, these oxidized and non-oxidized proteins were prepared according to the three dif  ferent sample preparation methods with or without the presence of N-Ethylmaleimide or β-mercaptoethanol. Results showed that oxidized proteins treated with NEM regardless of sample preparation methods presented attenuated bands of myosin heavy chain monomer in the non-reducing SDS-PAGE gels, suggesting that the disulfide bonds formed as a result of protein oxidation could be preserved by NEM during sample preparation. Meanwhile, a possible mechanism for the effect of NEM was proposed.https://www.meatjournal.ru/jour/article/view/221protein oxidationdisulfide bondn-ethylmaleimidesds-page
spellingShingle W. Wang
S. Wang
S. Li
N-Ethylmaleimide influenced the evaluation of disulfide cross-links in the oxidized myofibrillar proteins using the non-reducing SDS-PAGE
Теория и практика переработки мяса
protein oxidation
disulfide bond
n-ethylmaleimide
sds-page
title N-Ethylmaleimide influenced the evaluation of disulfide cross-links in the oxidized myofibrillar proteins using the non-reducing SDS-PAGE
title_full N-Ethylmaleimide influenced the evaluation of disulfide cross-links in the oxidized myofibrillar proteins using the non-reducing SDS-PAGE
title_fullStr N-Ethylmaleimide influenced the evaluation of disulfide cross-links in the oxidized myofibrillar proteins using the non-reducing SDS-PAGE
title_full_unstemmed N-Ethylmaleimide influenced the evaluation of disulfide cross-links in the oxidized myofibrillar proteins using the non-reducing SDS-PAGE
title_short N-Ethylmaleimide influenced the evaluation of disulfide cross-links in the oxidized myofibrillar proteins using the non-reducing SDS-PAGE
title_sort n ethylmaleimide influenced the evaluation of disulfide cross links in the oxidized myofibrillar proteins using the non reducing sds page
topic protein oxidation
disulfide bond
n-ethylmaleimide
sds-page
url https://www.meatjournal.ru/jour/article/view/221
work_keys_str_mv AT wwang nethylmaleimideinfluencedtheevaluationofdisulfidecrosslinksintheoxidizedmyofibrillarproteinsusingthenonreducingsdspage
AT swang nethylmaleimideinfluencedtheevaluationofdisulfidecrosslinksintheoxidizedmyofibrillarproteinsusingthenonreducingsdspage
AT sli nethylmaleimideinfluencedtheevaluationofdisulfidecrosslinksintheoxidizedmyofibrillarproteinsusingthenonreducingsdspage