EXTRACTION-SPECTROPHOTOMETRIC DETERMINATION OF AMMONIUM ION BY DIBENZO- 18-CROWN-6 AND CALMAGITE

An extraction-spectrophotometric method for the determination of trace amounts of ammonium ion is described. Ammonium ion is effectively extracted as a neutral ternary complex NH . DB 18C6. calmagite at pH 3.0 into chloroform, followed by spectrophotometric determination at =48 5 nm. Molar absorpti...

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Format: Article
Language:English
Published: University of Tehran 1993-06-01
Series:Journal of Sciences, Islamic Republic of Iran
Online Access:https://jsciences.ut.ac.ir/article_31398_ac3c9d1f32105a6fc85ad3a172cdee87.pdf
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description An extraction-spectrophotometric method for the determination of trace amounts of ammonium ion is described. Ammonium ion is effectively extracted as a neutral ternary complex NH . DB 18C6. calmagite at pH 3.0 into chloroform, followed by spectrophotometric determination at =48 5 nm. Molar absorptivity of the ternary complex at this wavelength is 1.08 10 mol cm . Beer's law is obeyed over the range 0.5-9.0 g ml and the Sandell's sensitivity for 0.001 absorbance unit is 16.7 ng cm . The method is simple, rapid and free from interferences of several cations and anions which are usually present with NH ion in real samples
format Article
id doaj-art-65d730320c3949378698a90f42dbb2e5
institution OA Journals
issn 1016-1104
2345-6914
language English
publishDate 1993-06-01
publisher University of Tehran
record_format Article
series Journal of Sciences, Islamic Republic of Iran
spelling doaj-art-65d730320c3949378698a90f42dbb2e52025-08-20T02:25:51ZengUniversity of TehranJournal of Sciences, Islamic Republic of Iran1016-11042345-69141993-06-014231398EXTRACTION-SPECTROPHOTOMETRIC DETERMINATION OF AMMONIUM ION BY DIBENZO- 18-CROWN-6 AND CALMAGITEAn extraction-spectrophotometric method for the determination of trace amounts of ammonium ion is described. Ammonium ion is effectively extracted as a neutral ternary complex NH . DB 18C6. calmagite at pH 3.0 into chloroform, followed by spectrophotometric determination at =48 5 nm. Molar absorptivity of the ternary complex at this wavelength is 1.08 10 mol cm . Beer's law is obeyed over the range 0.5-9.0 g ml and the Sandell's sensitivity for 0.001 absorbance unit is 16.7 ng cm . The method is simple, rapid and free from interferences of several cations and anions which are usually present with NH ion in real sampleshttps://jsciences.ut.ac.ir/article_31398_ac3c9d1f32105a6fc85ad3a172cdee87.pdf
spellingShingle EXTRACTION-SPECTROPHOTOMETRIC DETERMINATION OF AMMONIUM ION BY DIBENZO- 18-CROWN-6 AND CALMAGITE
Journal of Sciences, Islamic Republic of Iran
title EXTRACTION-SPECTROPHOTOMETRIC DETERMINATION OF AMMONIUM ION BY DIBENZO- 18-CROWN-6 AND CALMAGITE
title_full EXTRACTION-SPECTROPHOTOMETRIC DETERMINATION OF AMMONIUM ION BY DIBENZO- 18-CROWN-6 AND CALMAGITE
title_fullStr EXTRACTION-SPECTROPHOTOMETRIC DETERMINATION OF AMMONIUM ION BY DIBENZO- 18-CROWN-6 AND CALMAGITE
title_full_unstemmed EXTRACTION-SPECTROPHOTOMETRIC DETERMINATION OF AMMONIUM ION BY DIBENZO- 18-CROWN-6 AND CALMAGITE
title_short EXTRACTION-SPECTROPHOTOMETRIC DETERMINATION OF AMMONIUM ION BY DIBENZO- 18-CROWN-6 AND CALMAGITE
title_sort extraction spectrophotometric determination of ammonium ion by dibenzo 18 crown 6 and calmagite
url https://jsciences.ut.ac.ir/article_31398_ac3c9d1f32105a6fc85ad3a172cdee87.pdf