Preparation and mechanical properties of (SiCnp+NiTip)/Al composites with triple-modal grain structure

A controllable composite powder ball milling and assembly strategy were employed to achieve a tri-modal grain structure in silicon carbide (SiC) nanoparticles plus NiTi particles (SiCnp+NiTip)/Al composites. High-energy ball milling was used for SiCnp with small-sized pure Al powder, which formed ul...

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Main Authors: Xue Zhang, Mingfang Qian, Xuexi Zhang, Lin Geng
Format: Article
Language:English
Published: Elsevier 2025-03-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425001024
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author Xue Zhang
Mingfang Qian
Xuexi Zhang
Lin Geng
author_facet Xue Zhang
Mingfang Qian
Xuexi Zhang
Lin Geng
author_sort Xue Zhang
collection DOAJ
description A controllable composite powder ball milling and assembly strategy were employed to achieve a tri-modal grain structure in silicon carbide (SiC) nanoparticles plus NiTi particles (SiCnp+NiTip)/Al composites. High-energy ball milling was used for SiCnp with small-sized pure Al powder, which formed ultrafine grains (UFG) smaller than 500 nm. NiTip and large-size pure Al powder use the same process as Al-SiCnp powder to forming 0.5–5 μm fine grains (FG). Large-size pure Al powder with coarse grains (CG, average grain size 9.4 μm) were mixed with Al-SiCnp and Al-NiTip powders via low energy ball milling. The mixed powders were spark plasma sintered (SPS) to prepare UFG-FG-CG tri-modal grain structure composites with superior strength-ductility synergy. For Com 35-35-30, the ultimate tensile strength (UTS) (285.7 ± 3.1 MPa) and elongation (δ) (10.5 ± 2.7%) were 25.6% and 228% higher than those of the homogeneous composite counterpart, respectively. These simultaneously enhanced strength and ductility were attributed to the good interfacial bonding strength of NiTi/Al and the back stress strengthening effect from the tri-modal grain structure design that meets the stress matching requirements of NiTip. Therefore, the step-wise ball milling of composite powders and their assembly have been demonstrated to be an effective technique for fabricating Al matrix nanocomposites with heterogeneous structures.
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institution Kabale University
issn 2238-7854
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series Journal of Materials Research and Technology
spelling doaj-art-64a27bd8292d48708c9738daa120469b2025-01-26T05:03:55ZengElsevierJournal of Materials Research and Technology2238-78542025-03-013518421853Preparation and mechanical properties of (SiCnp+NiTip)/Al composites with triple-modal grain structureXue Zhang0Mingfang Qian1Xuexi Zhang2Lin Geng3School of Materials Science and Engineering, Harbin Institute of Technology, Harbin, 150001, ChinaCorresponding author.; School of Materials Science and Engineering, Harbin Institute of Technology, Harbin, 150001, ChinaCorresponding author.; School of Materials Science and Engineering, Harbin Institute of Technology, Harbin, 150001, ChinaSchool of Materials Science and Engineering, Harbin Institute of Technology, Harbin, 150001, ChinaA controllable composite powder ball milling and assembly strategy were employed to achieve a tri-modal grain structure in silicon carbide (SiC) nanoparticles plus NiTi particles (SiCnp+NiTip)/Al composites. High-energy ball milling was used for SiCnp with small-sized pure Al powder, which formed ultrafine grains (UFG) smaller than 500 nm. NiTip and large-size pure Al powder use the same process as Al-SiCnp powder to forming 0.5–5 μm fine grains (FG). Large-size pure Al powder with coarse grains (CG, average grain size 9.4 μm) were mixed with Al-SiCnp and Al-NiTip powders via low energy ball milling. The mixed powders were spark plasma sintered (SPS) to prepare UFG-FG-CG tri-modal grain structure composites with superior strength-ductility synergy. For Com 35-35-30, the ultimate tensile strength (UTS) (285.7 ± 3.1 MPa) and elongation (δ) (10.5 ± 2.7%) were 25.6% and 228% higher than those of the homogeneous composite counterpart, respectively. These simultaneously enhanced strength and ductility were attributed to the good interfacial bonding strength of NiTi/Al and the back stress strengthening effect from the tri-modal grain structure design that meets the stress matching requirements of NiTip. Therefore, the step-wise ball milling of composite powders and their assembly have been demonstrated to be an effective technique for fabricating Al matrix nanocomposites with heterogeneous structures.http://www.sciencedirect.com/science/article/pii/S2238785425001024Al matrix nanocomposites (AMCs)Low-temperature hot extrusionTri-modal grain structureStrengthening and toughening
spellingShingle Xue Zhang
Mingfang Qian
Xuexi Zhang
Lin Geng
Preparation and mechanical properties of (SiCnp+NiTip)/Al composites with triple-modal grain structure
Journal of Materials Research and Technology
Al matrix nanocomposites (AMCs)
Low-temperature hot extrusion
Tri-modal grain structure
Strengthening and toughening
title Preparation and mechanical properties of (SiCnp+NiTip)/Al composites with triple-modal grain structure
title_full Preparation and mechanical properties of (SiCnp+NiTip)/Al composites with triple-modal grain structure
title_fullStr Preparation and mechanical properties of (SiCnp+NiTip)/Al composites with triple-modal grain structure
title_full_unstemmed Preparation and mechanical properties of (SiCnp+NiTip)/Al composites with triple-modal grain structure
title_short Preparation and mechanical properties of (SiCnp+NiTip)/Al composites with triple-modal grain structure
title_sort preparation and mechanical properties of sicnp nitip al composites with triple modal grain structure
topic Al matrix nanocomposites (AMCs)
Low-temperature hot extrusion
Tri-modal grain structure
Strengthening and toughening
url http://www.sciencedirect.com/science/article/pii/S2238785425001024
work_keys_str_mv AT xuezhang preparationandmechanicalpropertiesofsicnpnitipalcompositeswithtriplemodalgrainstructure
AT mingfangqian preparationandmechanicalpropertiesofsicnpnitipalcompositeswithtriplemodalgrainstructure
AT xuexizhang preparationandmechanicalpropertiesofsicnpnitipalcompositeswithtriplemodalgrainstructure
AT lingeng preparationandmechanicalpropertiesofsicnpnitipalcompositeswithtriplemodalgrainstructure