MODELING OF EX VIVO INTERNALIZATION METHOD OF WATER- SOLUBLE ANTICANCER DRUGS IN SMALL INTESTINE USING CHEMILUMINESCENCE

Introduction. the ability of the small intestine (internalization) to absorb water-soluble anticancer cytostatics determines the possibility of their oral administration. the ex-vivo express method that simulates the internalization of substances using a modified technique of an isolated «inverted»...

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Main Authors: H. M. Treshalina, N. V. Andronova, J. R. Tcherkassova, E. Yu. Klinski, G. Babayeva, E. V. Lukasheva, M. I. Treshchalin, S. A. Tsurkan
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Language:Russian
Published: Russian Academy of Sciences, Tomsk National Research Medical Center 2020-01-01
Series:Сибирский онкологический журнал
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Online Access:https://www.siboncoj.ru/jour/article/view/1246
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author H. M. Treshalina
N. V. Andronova
J. R. Tcherkassova
E. Yu. Klinski
G. Babayeva
E. V. Lukasheva
M. I. Treshchalin
S. A. Tsurkan
author_facet H. M. Treshalina
N. V. Andronova
J. R. Tcherkassova
E. Yu. Klinski
G. Babayeva
E. V. Lukasheva
M. I. Treshchalin
S. A. Tsurkan
author_sort H. M. Treshalina
collection DOAJ
description Introduction. the ability of the small intestine (internalization) to absorb water-soluble anticancer cytostatics determines the possibility of their oral administration. the ex-vivo express method that simulates the internalization of substances using a modified technique of an isolated «inverted» segment of the rat small intestine with flash chemiluminescence is adequate to solve the problem. Objectives: to evaluate the absorption of the new water-soluble anticancer cytostatics with different properties from the rat small intestine for preclinical study by oral administration. Material and methods. conjugated with acridinium (Acridinium NHS Ester, Toronto Research Chemicals, Canada) cytostatics were studied: low molecular weight (1) anthrafuran-acridinium (MW 0.8 kDa) and high molecular weight (2) aimpila-acridinium (MW 105 kDa) and (3) L-lysine-α-oxidase (LO-acridinium, MW 122 kDa). absorption was determined in a modified model of an isolated «inverted» segment of the rat small intestine using flash-chemiluminescence with the calculation of the relative light units (RLu). Results. It was shown that the absorption level of acridinium-conjugated cytostatics depending on molar concentration ranged from 55 % (1) to 1.7–11 % (2, 3) and 2500 (1) to 9.2–188 nmol/l (2, 3), respectively. the level of internalized anthrafuran-acridinium (55 %) was consistent with the known value of the effective non-conjugated cytostatic oral dose, which was two times higher than equitherapeutical parenteral dose: 100 mg/kg vs 50 mg/kg. Conclusion. the data obtained allow us to consider ex vivo express method for preclinical study of the various water-soluble anticancer cytostatics for screening and identification of an opportunity for oral administration and estimation of starting dose. the method has a good correlation with in vivo tests and economically favorable due to a quick response and small number of the tested agent.
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record_format Article
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spelling doaj-art-63a8968c442b412ca10b74da86b9b6ae2025-08-20T03:35:48ZrusRussian Academy of Sciences, Tomsk National Research Medical CenterСибирский онкологический журнал1814-48612312-31682020-01-01186758110.21294/1814-4861-2019-18-6-75-81692MODELING OF EX VIVO INTERNALIZATION METHOD OF WATER- SOLUBLE ANTICANCER DRUGS IN SMALL INTESTINE USING CHEMILUMINESCENCEH. M. Treshalina0N. V. Andronova1J. R. Tcherkassova2E. Yu. Klinski3G. Babayeva4E. V. Lukasheva5M. I. Treshchalin6S. A. Tsurkan7N.N. Blokhin National Medical Research Center of Oncology, Ministry of Health of RussiaN.N. Blokhin National Medical Research Center of Oncology, Ministry of Health of RussiaJVS Diagnostics LLC«JVS Diagnostics LLC» Skolkovo Innovation CenterPeoples’ Friendship University of RussiaPeoples’ Friendship University of RussiaGause Institute of New Antibiotics«JVS Diagnostics LLC» Skolkovo Innovation CenterIntroduction. the ability of the small intestine (internalization) to absorb water-soluble anticancer cytostatics determines the possibility of their oral administration. the ex-vivo express method that simulates the internalization of substances using a modified technique of an isolated «inverted» segment of the rat small intestine with flash chemiluminescence is adequate to solve the problem. Objectives: to evaluate the absorption of the new water-soluble anticancer cytostatics with different properties from the rat small intestine for preclinical study by oral administration. Material and methods. conjugated with acridinium (Acridinium NHS Ester, Toronto Research Chemicals, Canada) cytostatics were studied: low molecular weight (1) anthrafuran-acridinium (MW 0.8 kDa) and high molecular weight (2) aimpila-acridinium (MW 105 kDa) and (3) L-lysine-α-oxidase (LO-acridinium, MW 122 kDa). absorption was determined in a modified model of an isolated «inverted» segment of the rat small intestine using flash-chemiluminescence with the calculation of the relative light units (RLu). Results. It was shown that the absorption level of acridinium-conjugated cytostatics depending on molar concentration ranged from 55 % (1) to 1.7–11 % (2, 3) and 2500 (1) to 9.2–188 nmol/l (2, 3), respectively. the level of internalized anthrafuran-acridinium (55 %) was consistent with the known value of the effective non-conjugated cytostatic oral dose, which was two times higher than equitherapeutical parenteral dose: 100 mg/kg vs 50 mg/kg. Conclusion. the data obtained allow us to consider ex vivo express method for preclinical study of the various water-soluble anticancer cytostatics for screening and identification of an opportunity for oral administration and estimation of starting dose. the method has a good correlation with in vivo tests and economically favorable due to a quick response and small number of the tested agent.https://www.siboncoj.ru/jour/article/view/1246cytostaticsinternalizationrat small intestineexpress-methodex vivo
spellingShingle H. M. Treshalina
N. V. Andronova
J. R. Tcherkassova
E. Yu. Klinski
G. Babayeva
E. V. Lukasheva
M. I. Treshchalin
S. A. Tsurkan
MODELING OF EX VIVO INTERNALIZATION METHOD OF WATER- SOLUBLE ANTICANCER DRUGS IN SMALL INTESTINE USING CHEMILUMINESCENCE
Сибирский онкологический журнал
cytostatics
internalization
rat small intestine
express-method
ex vivo
title MODELING OF EX VIVO INTERNALIZATION METHOD OF WATER- SOLUBLE ANTICANCER DRUGS IN SMALL INTESTINE USING CHEMILUMINESCENCE
title_full MODELING OF EX VIVO INTERNALIZATION METHOD OF WATER- SOLUBLE ANTICANCER DRUGS IN SMALL INTESTINE USING CHEMILUMINESCENCE
title_fullStr MODELING OF EX VIVO INTERNALIZATION METHOD OF WATER- SOLUBLE ANTICANCER DRUGS IN SMALL INTESTINE USING CHEMILUMINESCENCE
title_full_unstemmed MODELING OF EX VIVO INTERNALIZATION METHOD OF WATER- SOLUBLE ANTICANCER DRUGS IN SMALL INTESTINE USING CHEMILUMINESCENCE
title_short MODELING OF EX VIVO INTERNALIZATION METHOD OF WATER- SOLUBLE ANTICANCER DRUGS IN SMALL INTESTINE USING CHEMILUMINESCENCE
title_sort modeling of ex vivo internalization method of water soluble anticancer drugs in small intestine using chemiluminescence
topic cytostatics
internalization
rat small intestine
express-method
ex vivo
url https://www.siboncoj.ru/jour/article/view/1246
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