Water adsorption properties of silica gel and hydroxyethyl cellulose composite coatings

Water scarcity is an increasingly significant global issue. Desiccant coated heat exchangers are a potential adsorption reactor for atmospheric water generation, which can alleviate water scarcity through the subsequent adsorption, desorption, and condensation of ambient humidity. Microporous and me...

Full description

Saved in:
Bibliographic Details
Main Authors: Lucas Lovis, Andrew Maddocks, Priscilla Tremain, Behdad Moghtaderi
Format: Article
Language:English
Published: Elsevier 2025-09-01
Series:Results in Materials
Subjects:
Online Access:http://www.sciencedirect.com/science/article/pii/S2590048X25000792
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849331020087689216
author Lucas Lovis
Andrew Maddocks
Priscilla Tremain
Behdad Moghtaderi
author_facet Lucas Lovis
Andrew Maddocks
Priscilla Tremain
Behdad Moghtaderi
author_sort Lucas Lovis
collection DOAJ
description Water scarcity is an increasingly significant global issue. Desiccant coated heat exchangers are a potential adsorption reactor for atmospheric water generation, which can alleviate water scarcity through the subsequent adsorption, desorption, and condensation of ambient humidity. Microporous and mesoporous silica gels are common and inexpensive desiccants that demonstrate moderate adsorption and desorption rates, and hence are suitable for multicyclic atmospheric water generation. To accurately model the behaviour of silica gel based desiccant coated heat exchanger-atmospheric water generation systems, the kinetic and equilibrium properties of silica gel were measured for varying coating thicknesses, hydroxyethyl cellulose binder concentrations, temperatures, and relative humidity conditions using thermogravimetric analysis. Additionally, the particle size, pore textural properties, and density of the samples were measured using scanning electron microscopy, nitrogen adsorption, and pycnometry respectively. The average particle size within the coatings increased with increasing hydroxyethyl cellulose concentration. The equilibrium uptake was lower for the coating samples compared to the powder sample and was not strongly dependant on the adsorption temperature. The kinetic constants and maximum ideal specific water production were inversely related to the coating thickness and were not strongly dependant on the hydroxyethyl cellulose concentration. The adsorption order and kinetic constant varied depending on whether monolayer adsorption, multilayer adsorption, pore filling, or capillary condensation were occurring. The effect of the change in adsorption mechanism on the kinetic constant was less significant for thicker layers and lower adsorption temperatures. The maximum ideal specific water production for the coating samples within the set of measured conditions was 57 L kg−1 day−1.
format Article
id doaj-art-62d35a8e73104362aec2eeb2b5ffa798
institution Kabale University
issn 2590-048X
language English
publishDate 2025-09-01
publisher Elsevier
record_format Article
series Results in Materials
spelling doaj-art-62d35a8e73104362aec2eeb2b5ffa7982025-08-20T03:46:45ZengElsevierResults in Materials2590-048X2025-09-012710073410.1016/j.rinma.2025.100734Water adsorption properties of silica gel and hydroxyethyl cellulose composite coatingsLucas Lovis0Andrew Maddocks1Priscilla Tremain2Behdad Moghtaderi3Corresponding author. Newcastle Institute for Energy and Resources NIERC120, University of Newcastle, University Drive, Callaghan, NSW, 2308, Australia.; Centre for Innovative Energy Technologies, Chemical Engineering, The University of Newcastle, University Drive, Callaghan, New South Wales, 2308, AustraliaCentre for Innovative Energy Technologies, Chemical Engineering, The University of Newcastle, University Drive, Callaghan, New South Wales, 2308, AustraliaCentre for Innovative Energy Technologies, Chemical Engineering, The University of Newcastle, University Drive, Callaghan, New South Wales, 2308, AustraliaCentre for Innovative Energy Technologies, Chemical Engineering, The University of Newcastle, University Drive, Callaghan, New South Wales, 2308, AustraliaWater scarcity is an increasingly significant global issue. Desiccant coated heat exchangers are a potential adsorption reactor for atmospheric water generation, which can alleviate water scarcity through the subsequent adsorption, desorption, and condensation of ambient humidity. Microporous and mesoporous silica gels are common and inexpensive desiccants that demonstrate moderate adsorption and desorption rates, and hence are suitable for multicyclic atmospheric water generation. To accurately model the behaviour of silica gel based desiccant coated heat exchanger-atmospheric water generation systems, the kinetic and equilibrium properties of silica gel were measured for varying coating thicknesses, hydroxyethyl cellulose binder concentrations, temperatures, and relative humidity conditions using thermogravimetric analysis. Additionally, the particle size, pore textural properties, and density of the samples were measured using scanning electron microscopy, nitrogen adsorption, and pycnometry respectively. The average particle size within the coatings increased with increasing hydroxyethyl cellulose concentration. The equilibrium uptake was lower for the coating samples compared to the powder sample and was not strongly dependant on the adsorption temperature. The kinetic constants and maximum ideal specific water production were inversely related to the coating thickness and were not strongly dependant on the hydroxyethyl cellulose concentration. The adsorption order and kinetic constant varied depending on whether monolayer adsorption, multilayer adsorption, pore filling, or capillary condensation were occurring. The effect of the change in adsorption mechanism on the kinetic constant was less significant for thicker layers and lower adsorption temperatures. The maximum ideal specific water production for the coating samples within the set of measured conditions was 57 L kg−1 day−1.http://www.sciencedirect.com/science/article/pii/S2590048X25000792Silica gelHydroxyethyl celluloseCoatingAdsorptionKinetics
spellingShingle Lucas Lovis
Andrew Maddocks
Priscilla Tremain
Behdad Moghtaderi
Water adsorption properties of silica gel and hydroxyethyl cellulose composite coatings
Results in Materials
Silica gel
Hydroxyethyl cellulose
Coating
Adsorption
Kinetics
title Water adsorption properties of silica gel and hydroxyethyl cellulose composite coatings
title_full Water adsorption properties of silica gel and hydroxyethyl cellulose composite coatings
title_fullStr Water adsorption properties of silica gel and hydroxyethyl cellulose composite coatings
title_full_unstemmed Water adsorption properties of silica gel and hydroxyethyl cellulose composite coatings
title_short Water adsorption properties of silica gel and hydroxyethyl cellulose composite coatings
title_sort water adsorption properties of silica gel and hydroxyethyl cellulose composite coatings
topic Silica gel
Hydroxyethyl cellulose
Coating
Adsorption
Kinetics
url http://www.sciencedirect.com/science/article/pii/S2590048X25000792
work_keys_str_mv AT lucaslovis wateradsorptionpropertiesofsilicagelandhydroxyethylcellulosecompositecoatings
AT andrewmaddocks wateradsorptionpropertiesofsilicagelandhydroxyethylcellulosecompositecoatings
AT priscillatremain wateradsorptionpropertiesofsilicagelandhydroxyethylcellulosecompositecoatings
AT behdadmoghtaderi wateradsorptionpropertiesofsilicagelandhydroxyethylcellulosecompositecoatings