The In Situ Polymerization and Characterization of PA6/LiCl Composites

PA6/LiCl composites were synthesized by in situ anionic polymerization based on the interaction between the inorganic salts and PA6. Sodium hydroxide as initiator and N-acetylcaprolactam as activator were used in the preparation of PA6/LiCl composites with variety of LiCl content. X-ray diffraction...

Full description

Saved in:
Bibliographic Details
Main Authors: Dandan Sun, Jiang Li, Qinghua Pan, Chaowei Hao, Guoqiao Lai
Format: Article
Language:English
Published: Wiley 2013-01-01
Series:Journal of Spectroscopy
Online Access:http://dx.doi.org/10.1155/2013/164275
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1832552568702631936
author Dandan Sun
Jiang Li
Qinghua Pan
Chaowei Hao
Guoqiao Lai
author_facet Dandan Sun
Jiang Li
Qinghua Pan
Chaowei Hao
Guoqiao Lai
author_sort Dandan Sun
collection DOAJ
description PA6/LiCl composites were synthesized by in situ anionic polymerization based on the interaction between the inorganic salts and PA6. Sodium hydroxide as initiator and N-acetylcaprolactam as activator were used in the preparation of PA6/LiCl composites with variety of LiCl content. X-ray diffraction (XRD) and differential scanning calorimeter (DSC) testing results showed that both of degree of crystallinity and melting temperature of the composites were decreased under the influence of LiCl. And the γ crystal phase proportion increased with increasing the LiCl content to appropriate amount.
format Article
id doaj-art-620e8af1d53a44858a99786aa45afb0e
institution Kabale University
issn 2314-4920
2314-4939
language English
publishDate 2013-01-01
publisher Wiley
record_format Article
series Journal of Spectroscopy
spelling doaj-art-620e8af1d53a44858a99786aa45afb0e2025-02-03T05:58:18ZengWileyJournal of Spectroscopy2314-49202314-49392013-01-01201310.1155/2013/164275164275The In Situ Polymerization and Characterization of PA6/LiCl CompositesDandan Sun0Jiang Li1Qinghua Pan2Chaowei Hao3Guoqiao Lai4Key Laboratory of Organosilicon Chemistry and Material Technology Ministry of Education, Hangzhou Normal University, Hangzhou 310012, ChinaKey Laboratory of Organosilicon Chemistry and Material Technology Ministry of Education, Hangzhou Normal University, Hangzhou 310012, ChinaKey Laboratory of Organosilicon Chemistry and Material Technology Ministry of Education, Hangzhou Normal University, Hangzhou 310012, ChinaKey Laboratory of Organosilicon Chemistry and Material Technology Ministry of Education, Hangzhou Normal University, Hangzhou 310012, ChinaKey Laboratory of Organosilicon Chemistry and Material Technology Ministry of Education, Hangzhou Normal University, Hangzhou 310012, ChinaPA6/LiCl composites were synthesized by in situ anionic polymerization based on the interaction between the inorganic salts and PA6. Sodium hydroxide as initiator and N-acetylcaprolactam as activator were used in the preparation of PA6/LiCl composites with variety of LiCl content. X-ray diffraction (XRD) and differential scanning calorimeter (DSC) testing results showed that both of degree of crystallinity and melting temperature of the composites were decreased under the influence of LiCl. And the γ crystal phase proportion increased with increasing the LiCl content to appropriate amount.http://dx.doi.org/10.1155/2013/164275
spellingShingle Dandan Sun
Jiang Li
Qinghua Pan
Chaowei Hao
Guoqiao Lai
The In Situ Polymerization and Characterization of PA6/LiCl Composites
Journal of Spectroscopy
title The In Situ Polymerization and Characterization of PA6/LiCl Composites
title_full The In Situ Polymerization and Characterization of PA6/LiCl Composites
title_fullStr The In Situ Polymerization and Characterization of PA6/LiCl Composites
title_full_unstemmed The In Situ Polymerization and Characterization of PA6/LiCl Composites
title_short The In Situ Polymerization and Characterization of PA6/LiCl Composites
title_sort in situ polymerization and characterization of pa6 licl composites
url http://dx.doi.org/10.1155/2013/164275
work_keys_str_mv AT dandansun theinsitupolymerizationandcharacterizationofpa6liclcomposites
AT jiangli theinsitupolymerizationandcharacterizationofpa6liclcomposites
AT qinghuapan theinsitupolymerizationandcharacterizationofpa6liclcomposites
AT chaoweihao theinsitupolymerizationandcharacterizationofpa6liclcomposites
AT guoqiaolai theinsitupolymerizationandcharacterizationofpa6liclcomposites
AT dandansun insitupolymerizationandcharacterizationofpa6liclcomposites
AT jiangli insitupolymerizationandcharacterizationofpa6liclcomposites
AT qinghuapan insitupolymerizationandcharacterizationofpa6liclcomposites
AT chaoweihao insitupolymerizationandcharacterizationofpa6liclcomposites
AT guoqiaolai insitupolymerizationandcharacterizationofpa6liclcomposites