Demonstrating In Situ Formation of Globular Microstructure for Thixotropic Printing of EN AW-4043 Aluminum Alloy

This study explores the feasibility of generating a globular microstructure in situ during the thixotropic 3D printing of the EN AW-4043 alloy, starting from a conventional cold-rolled wire. Thermodynamic simulations using Thermo-Calc software were first conducted to identify the semi-solid processi...

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Main Authors: Silvia Marola, Maurizio Vedani
Format: Article
Language:English
Published: MDPI AG 2025-07-01
Series:Metals
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Online Access:https://www.mdpi.com/2075-4701/15/7/804
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author Silvia Marola
Maurizio Vedani
author_facet Silvia Marola
Maurizio Vedani
author_sort Silvia Marola
collection DOAJ
description This study explores the feasibility of generating a globular microstructure in situ during the thixotropic 3D printing of the EN AW-4043 alloy, starting from a conventional cold-rolled wire. Thermodynamic simulations using Thermo-Calc software were first conducted to identify the semi-solid processing window of the alloy, based on the evolution of liquid and solid fractions as a function of temperature. Guided by these results, thermal treatments were performed on cold-rolled wires to promote the formation of a globular microstructure. A laboratory-scale printing head prototype was then designed and built to test continuous heating and deposition conditions representative of a thixotropic additive manufacturing process. The results showed that a globular microstructure could be achieved in the cold-rolled EN AW-4043 wires by heating them at 590 °C for 5 min in a static muffle furnace. A similar effect was observed when continuously heating the wire while it flowed through the heated printing head. Preliminary deposition tests confirmed the viability of this approach and demonstrated that thixotropic 3D printing of EN AW-4043 alloy is achievable without the need for pre-globular feedstock.
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spelling doaj-art-60b7a3ca34ab47ba8a0b035c57bde21c2025-08-20T03:08:01ZengMDPI AGMetals2075-47012025-07-0115780410.3390/met15070804Demonstrating In Situ Formation of Globular Microstructure for Thixotropic Printing of EN AW-4043 Aluminum AlloySilvia Marola0Maurizio Vedani1Department of Mechanical Engineering, Politecnico di Milano, Via G. La Masa 1, 20156 Milano, ItalyDepartment of Mechanical Engineering, Politecnico di Milano, Via G. La Masa 1, 20156 Milano, ItalyThis study explores the feasibility of generating a globular microstructure in situ during the thixotropic 3D printing of the EN AW-4043 alloy, starting from a conventional cold-rolled wire. Thermodynamic simulations using Thermo-Calc software were first conducted to identify the semi-solid processing window of the alloy, based on the evolution of liquid and solid fractions as a function of temperature. Guided by these results, thermal treatments were performed on cold-rolled wires to promote the formation of a globular microstructure. A laboratory-scale printing head prototype was then designed and built to test continuous heating and deposition conditions representative of a thixotropic additive manufacturing process. The results showed that a globular microstructure could be achieved in the cold-rolled EN AW-4043 wires by heating them at 590 °C for 5 min in a static muffle furnace. A similar effect was observed when continuously heating the wire while it flowed through the heated printing head. Preliminary deposition tests confirmed the viability of this approach and demonstrated that thixotropic 3D printing of EN AW-4043 alloy is achievable without the need for pre-globular feedstock.https://www.mdpi.com/2075-4701/15/7/804thixotropic 3D printingsemi-solid metal processingaluminum alloyglobular microstructure
spellingShingle Silvia Marola
Maurizio Vedani
Demonstrating In Situ Formation of Globular Microstructure for Thixotropic Printing of EN AW-4043 Aluminum Alloy
Metals
thixotropic 3D printing
semi-solid metal processing
aluminum alloy
globular microstructure
title Demonstrating In Situ Formation of Globular Microstructure for Thixotropic Printing of EN AW-4043 Aluminum Alloy
title_full Demonstrating In Situ Formation of Globular Microstructure for Thixotropic Printing of EN AW-4043 Aluminum Alloy
title_fullStr Demonstrating In Situ Formation of Globular Microstructure for Thixotropic Printing of EN AW-4043 Aluminum Alloy
title_full_unstemmed Demonstrating In Situ Formation of Globular Microstructure for Thixotropic Printing of EN AW-4043 Aluminum Alloy
title_short Demonstrating In Situ Formation of Globular Microstructure for Thixotropic Printing of EN AW-4043 Aluminum Alloy
title_sort demonstrating in situ formation of globular microstructure for thixotropic printing of en aw 4043 aluminum alloy
topic thixotropic 3D printing
semi-solid metal processing
aluminum alloy
globular microstructure
url https://www.mdpi.com/2075-4701/15/7/804
work_keys_str_mv AT silviamarola demonstratinginsituformationofglobularmicrostructureforthixotropicprintingofenaw4043aluminumalloy
AT mauriziovedani demonstratinginsituformationofglobularmicrostructureforthixotropicprintingofenaw4043aluminumalloy