Synthesis, Identification, and anti-cancer Evaluation of Some heterocyclic Chitosan-Thiosemicarbazones compounds and their nickle (II) complexes

Chitosan (CS) a chemical substance taken from the shells of sea creatures that has various uses in industry, farming, and medicine, for example in medical dressings. Its derivatives significantly inhibit two types of cancer cells: Madin Darby Canine Kidney MDCK and MCF-7. These derivatives include t...

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Main Authors: Mohsin Omar Mohammed, Hameed Madlool Mohammed Alkubaisi, Nadia Qader Haj
Format: Article
Language:English
Published: Elsevier 2024-12-01
Series:Results in Chemistry
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Online Access:http://www.sciencedirect.com/science/article/pii/S2211715624005551
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author Mohsin Omar Mohammed
Hameed Madlool Mohammed Alkubaisi
Nadia Qader Haj
author_facet Mohsin Omar Mohammed
Hameed Madlool Mohammed Alkubaisi
Nadia Qader Haj
author_sort Mohsin Omar Mohammed
collection DOAJ
description Chitosan (CS) a chemical substance taken from the shells of sea creatures that has various uses in industry, farming, and medicine, for example in medical dressings. Its derivatives significantly inhibit two types of cancer cells: Madin Darby Canine Kidney MDCK and MCF-7. These derivatives include thiosemicarbazones, heterocyclic moieties, and their metal (II) complexes. In this study, CS from crab shells is mixed with thiosemicarbazide (TSC). Then, imidazole-2-carboxaldehyde, oxazole-2-carboxaldehyde, and thiazole-2-carboxaldehyde reacted to make three different compounds from CS-TSC: [2a], [2b], and [2c]. The chemicals were mixed with nickel chloride to create nickel (II) chitosan 2-acetyl heterocyclic-2-thiosemicarbazone complexes. SEM and X-ray tests were performed on the powder, which showed that the nickel (II) chitosan thiosemicarbazone complexes had square and flat shapes. The synthesized compounds were tested to check their effectiveness in preventing MDCK and MCF-7. The study found that chitosan derivatives significantly inhibited MDCK and MCF-7.
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spelling doaj-art-5efb9c6803cb4dafa35e853181da21f12025-08-20T02:39:02ZengElsevierResults in Chemistry2211-71562024-12-011210185910.1016/j.rechem.2024.101859Synthesis, Identification, and anti-cancer Evaluation of Some heterocyclic Chitosan-Thiosemicarbazones compounds and their nickle (II) complexesMohsin Omar Mohammed0Hameed Madlool Mohammed Alkubaisi1Nadia Qader Haj2Chemistry Department, College of Science, University of Kirkuk, Iraq; Corresponding authors.Biotechnology and Environmental centre, University of Fallujah, IraqGeology Department, College of Science, University of Kirkuk, IraqChitosan (CS) a chemical substance taken from the shells of sea creatures that has various uses in industry, farming, and medicine, for example in medical dressings. Its derivatives significantly inhibit two types of cancer cells: Madin Darby Canine Kidney MDCK and MCF-7. These derivatives include thiosemicarbazones, heterocyclic moieties, and their metal (II) complexes. In this study, CS from crab shells is mixed with thiosemicarbazide (TSC). Then, imidazole-2-carboxaldehyde, oxazole-2-carboxaldehyde, and thiazole-2-carboxaldehyde reacted to make three different compounds from CS-TSC: [2a], [2b], and [2c]. The chemicals were mixed with nickel chloride to create nickel (II) chitosan 2-acetyl heterocyclic-2-thiosemicarbazone complexes. SEM and X-ray tests were performed on the powder, which showed that the nickel (II) chitosan thiosemicarbazone complexes had square and flat shapes. The synthesized compounds were tested to check their effectiveness in preventing MDCK and MCF-7. The study found that chitosan derivatives significantly inhibited MDCK and MCF-7.http://www.sciencedirect.com/science/article/pii/S2211715624005551ChitosanCancerComplexesThiosemicarbazonesHeterocyclic compounds
spellingShingle Mohsin Omar Mohammed
Hameed Madlool Mohammed Alkubaisi
Nadia Qader Haj
Synthesis, Identification, and anti-cancer Evaluation of Some heterocyclic Chitosan-Thiosemicarbazones compounds and their nickle (II) complexes
Results in Chemistry
Chitosan
Cancer
Complexes
Thiosemicarbazones
Heterocyclic compounds
title Synthesis, Identification, and anti-cancer Evaluation of Some heterocyclic Chitosan-Thiosemicarbazones compounds and their nickle (II) complexes
title_full Synthesis, Identification, and anti-cancer Evaluation of Some heterocyclic Chitosan-Thiosemicarbazones compounds and their nickle (II) complexes
title_fullStr Synthesis, Identification, and anti-cancer Evaluation of Some heterocyclic Chitosan-Thiosemicarbazones compounds and their nickle (II) complexes
title_full_unstemmed Synthesis, Identification, and anti-cancer Evaluation of Some heterocyclic Chitosan-Thiosemicarbazones compounds and their nickle (II) complexes
title_short Synthesis, Identification, and anti-cancer Evaluation of Some heterocyclic Chitosan-Thiosemicarbazones compounds and their nickle (II) complexes
title_sort synthesis identification and anti cancer evaluation of some heterocyclic chitosan thiosemicarbazones compounds and their nickle ii complexes
topic Chitosan
Cancer
Complexes
Thiosemicarbazones
Heterocyclic compounds
url http://www.sciencedirect.com/science/article/pii/S2211715624005551
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AT hameedmadloolmohammedalkubaisi synthesisidentificationandanticancerevaluationofsomeheterocyclicchitosanthiosemicarbazonescompoundsandtheirnickleiicomplexes
AT nadiaqaderhaj synthesisidentificationandanticancerevaluationofsomeheterocyclicchitosanthiosemicarbazonescompoundsandtheirnickleiicomplexes