5-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4H-pyran-3-carbonitrile dichlomethane hemisolvate
The title compound, 2C15H13FN2O2·CH2Cl2, crystallizes with two main molecules in the asymmetric unit with a disordered dichloromethane solvent molecule. The dihedral angles between the fluoro phenyl ring and 4H-pyran ring are 74.36 (15) and 80.69 (15)° in the two molecules. In the crystal, N—H...N a...
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| Format: | Article |
| Language: | English |
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International Union of Crystallography
2025-04-01
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| Series: | IUCrData |
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| Online Access: | https://journals.iucr.org/paper?S2414314625003372 |
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| author | Carren Nyapola Sizwe J. Zamisa Bernard Omondi Eric M. Njogu |
| author_facet | Carren Nyapola Sizwe J. Zamisa Bernard Omondi Eric M. Njogu |
| author_sort | Carren Nyapola |
| collection | DOAJ |
| description | The title compound, 2C15H13FN2O2·CH2Cl2, crystallizes with two main molecules in the asymmetric unit with a disordered dichloromethane solvent molecule. The dihedral angles between the fluoro phenyl ring and 4H-pyran ring are 74.36 (15) and 80.69 (15)° in the two molecules. In the crystal, N—H...N and N—H...O hydrogen bonds link the molecules into a two-dimensional supramolecular network propagating in the (100) plane. |
| format | Article |
| id | doaj-art-5ef66285d3684aec8ba8bcdebccd284b |
| institution | Kabale University |
| issn | 2414-3146 |
| language | English |
| publishDate | 2025-04-01 |
| publisher | International Union of Crystallography |
| record_format | Article |
| series | IUCrData |
| spelling | doaj-art-5ef66285d3684aec8ba8bcdebccd284b2025-08-20T03:52:10ZengInternational Union of CrystallographyIUCrData2414-31462025-04-01104x25033710.1107/S2414314625003372hb45095-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4H-pyran-3-carbonitrile dichlomethane hemisolvateCarren Nyapola0Sizwe J. Zamisa1Bernard Omondi2Eric M. Njogu3University of KwaZulu-Natal, School of Chemistry and Physics, Private bag X54001, Durban, 4000, South AfricaUniversity of KwaZulu-Natal, School of Chemistry and Physics, Private bag X54001, Durban, 4000, South AfricaUniversity of KwaZulu-Natal, School of Chemistry and Physics, Private bag X54001, Durban, 4000, South AfricaMultimedia University of Kenya, PO Box 15653-00503, Nairobi, KenyaThe title compound, 2C15H13FN2O2·CH2Cl2, crystallizes with two main molecules in the asymmetric unit with a disordered dichloromethane solvent molecule. The dihedral angles between the fluoro phenyl ring and 4H-pyran ring are 74.36 (15) and 80.69 (15)° in the two molecules. In the crystal, N—H...N and N—H...O hydrogen bonds link the molecules into a two-dimensional supramolecular network propagating in the (100) plane.https://journals.iucr.org/paper?S2414314625003372crystal structurepyranhydrogen bond |
| spellingShingle | Carren Nyapola Sizwe J. Zamisa Bernard Omondi Eric M. Njogu 5-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4H-pyran-3-carbonitrile dichlomethane hemisolvate IUCrData crystal structure pyran hydrogen bond |
| title | 5-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4H-pyran-3-carbonitrile dichlomethane hemisolvate |
| title_full | 5-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4H-pyran-3-carbonitrile dichlomethane hemisolvate |
| title_fullStr | 5-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4H-pyran-3-carbonitrile dichlomethane hemisolvate |
| title_full_unstemmed | 5-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4H-pyran-3-carbonitrile dichlomethane hemisolvate |
| title_short | 5-Acetyl-2-amino-4-(2-fluorophenyl)-6-methyl-4H-pyran-3-carbonitrile dichlomethane hemisolvate |
| title_sort | 5 acetyl 2 amino 4 2 fluorophenyl 6 methyl 4h pyran 3 carbonitrile dichlomethane hemisolvate |
| topic | crystal structure pyran hydrogen bond |
| url | https://journals.iucr.org/paper?S2414314625003372 |
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