1-Hexadecyl-3-methylimidazolium tetrachloroindate ionic liquid as corrosion inhibitor for mild steel: Insight from experimental, computational, multivariate statistics and multi-quadratic regression based machine learning model

The current study is focused on the synthesis and evaluation of 1-Hexadecyl-3-methylimidazolium tetrachloroindate [C16 mim][In Cl4] based ionic liquid (IL) as a corrosion inhibitor for mild steel in 1M HCl. Various advanced methods were employed in this research, such as potentiodynamic polarization...

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Main Authors: Ndidiamaka Martina Amadi, Joseph Okechukwu Ezeugo, Chukwunonso Chukwuzuluoke Okoye, John Ifeanyi Obibuenyi, Maduabuchi Arinzechukwu Chidiebere, Dominic Okechukwu Onukwuli, Valentine Chikaodili Anadebe
Format: Article
Language:English
Published: Elsevier 2024-12-01
Series:Results in Engineering
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Online Access:http://www.sciencedirect.com/science/article/pii/S2590123024013707
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author Ndidiamaka Martina Amadi
Joseph Okechukwu Ezeugo
Chukwunonso Chukwuzuluoke Okoye
John Ifeanyi Obibuenyi
Maduabuchi Arinzechukwu Chidiebere
Dominic Okechukwu Onukwuli
Valentine Chikaodili Anadebe
author_facet Ndidiamaka Martina Amadi
Joseph Okechukwu Ezeugo
Chukwunonso Chukwuzuluoke Okoye
John Ifeanyi Obibuenyi
Maduabuchi Arinzechukwu Chidiebere
Dominic Okechukwu Onukwuli
Valentine Chikaodili Anadebe
author_sort Ndidiamaka Martina Amadi
collection DOAJ
description The current study is focused on the synthesis and evaluation of 1-Hexadecyl-3-methylimidazolium tetrachloroindate [C16 mim][In Cl4] based ionic liquid (IL) as a corrosion inhibitor for mild steel in 1M HCl. Various advanced methods were employed in this research, such as potentiodynamic polarization (PDP), quantum chemical computations, molecular dynamics simulations, weight loss assessments, electrochemical impedance spectroscopy (EIS) and multivariate statistics via machine learning models. The ionic liquid (IL) under investigation demonstrated a notable corrosion inhibition efficiency (93.88 % weight loss, 94. % PDP, 75 % EIS). The combine electrochemical approach suggested a mechanism influenced by electron transfer, underscoring the IL's as a mixed-type inhibitor. The experimental data based on weight loss was optimized using response surface methodology (RSM). Maximum inhibition efficiency of 93.72 % was predicted by the RSM model. Also, the machine learning models based on artificial neural network (ANN) and adaptive neuro-fuzzy inference system (ANFIS) demonstrated good predictive power in analyzing the interactive effects affecting the inhibition process. The adsorption behavior of [C16 mim][In Cl4] on the mild steel surface further conformed to the Langmuir isotherm, demonstrating a monolayer adsorption process. The comprehensive nature of this approach facilitated a more in-depth adsorption process through computational modelling based on DFT and molecular dynamics. The machine learning models aligned credibly with the experimental findings with pronounced degree of accuracy. Thus, these integrated approaches unravel the potential of the studied IL as effective and sustainable corrosion inhibitor for severe acidic environments.
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spelling doaj-art-5e3e723831cf478cb16bbf300894a2f72025-08-20T02:34:35ZengElsevierResults in Engineering2590-12302024-12-012410311510.1016/j.rineng.2024.1031151-Hexadecyl-3-methylimidazolium tetrachloroindate ionic liquid as corrosion inhibitor for mild steel: Insight from experimental, computational, multivariate statistics and multi-quadratic regression based machine learning modelNdidiamaka Martina Amadi0Joseph Okechukwu Ezeugo1Chukwunonso Chukwuzuluoke Okoye2John Ifeanyi Obibuenyi3Maduabuchi Arinzechukwu Chidiebere4Dominic Okechukwu Onukwuli5Valentine Chikaodili Anadebe6Department of Chemical Engineering, Federal University of Technology, PMB 1526, Owerri, Imo State, Nigeria; Department of Chemical Engineering, Chukwuemeka Odumegwu Ojukwu Univesity, PMB 02, Uli, Anambra State, Nigeria; Corresponding author. Department of Chemical Engineering, Federal University of Technology, PMB 1526, Owerri, Imo State, NigeriaDepartment of Chemical Engineering, Chukwuemeka Odumegwu Ojukwu Univesity, PMB 02, Uli, Anambra State, NigeriaDepartment of Chemical Engineering, Nnamdi Azikwe University, PMB 5025, Awka, Anambra State, NigeriaDepartment of Chemical Engineering, Madonna University, Akpugo Campus, 402105, Akpugo, Enugu State, NigeriaDepartment of Science Laboratory Technology, Federal University of Technology, PMB 1526, Owerri, Imo State, NigeriaDepartment of Chemical Engineering, Nnamdi Azikwe University, PMB 5025, Awka, Anambra State, Nigeria; Corresponding author.Department of Chemical Engineering, Alex Ekwueme Federal University Ndufu Alike, PMB 1010, Abakaliki, Ebonyi State, Nigeria; Corresponding author.The current study is focused on the synthesis and evaluation of 1-Hexadecyl-3-methylimidazolium tetrachloroindate [C16 mim][In Cl4] based ionic liquid (IL) as a corrosion inhibitor for mild steel in 1M HCl. Various advanced methods were employed in this research, such as potentiodynamic polarization (PDP), quantum chemical computations, molecular dynamics simulations, weight loss assessments, electrochemical impedance spectroscopy (EIS) and multivariate statistics via machine learning models. The ionic liquid (IL) under investigation demonstrated a notable corrosion inhibition efficiency (93.88 % weight loss, 94. % PDP, 75 % EIS). The combine electrochemical approach suggested a mechanism influenced by electron transfer, underscoring the IL's as a mixed-type inhibitor. The experimental data based on weight loss was optimized using response surface methodology (RSM). Maximum inhibition efficiency of 93.72 % was predicted by the RSM model. Also, the machine learning models based on artificial neural network (ANN) and adaptive neuro-fuzzy inference system (ANFIS) demonstrated good predictive power in analyzing the interactive effects affecting the inhibition process. The adsorption behavior of [C16 mim][In Cl4] on the mild steel surface further conformed to the Langmuir isotherm, demonstrating a monolayer adsorption process. The comprehensive nature of this approach facilitated a more in-depth adsorption process through computational modelling based on DFT and molecular dynamics. The machine learning models aligned credibly with the experimental findings with pronounced degree of accuracy. Thus, these integrated approaches unravel the potential of the studied IL as effective and sustainable corrosion inhibitor for severe acidic environments.http://www.sciencedirect.com/science/article/pii/S2590123024013707CorrosionIonic liquidMild steelMachine learningComputational
spellingShingle Ndidiamaka Martina Amadi
Joseph Okechukwu Ezeugo
Chukwunonso Chukwuzuluoke Okoye
John Ifeanyi Obibuenyi
Maduabuchi Arinzechukwu Chidiebere
Dominic Okechukwu Onukwuli
Valentine Chikaodili Anadebe
1-Hexadecyl-3-methylimidazolium tetrachloroindate ionic liquid as corrosion inhibitor for mild steel: Insight from experimental, computational, multivariate statistics and multi-quadratic regression based machine learning model
Results in Engineering
Corrosion
Ionic liquid
Mild steel
Machine learning
Computational
title 1-Hexadecyl-3-methylimidazolium tetrachloroindate ionic liquid as corrosion inhibitor for mild steel: Insight from experimental, computational, multivariate statistics and multi-quadratic regression based machine learning model
title_full 1-Hexadecyl-3-methylimidazolium tetrachloroindate ionic liquid as corrosion inhibitor for mild steel: Insight from experimental, computational, multivariate statistics and multi-quadratic regression based machine learning model
title_fullStr 1-Hexadecyl-3-methylimidazolium tetrachloroindate ionic liquid as corrosion inhibitor for mild steel: Insight from experimental, computational, multivariate statistics and multi-quadratic regression based machine learning model
title_full_unstemmed 1-Hexadecyl-3-methylimidazolium tetrachloroindate ionic liquid as corrosion inhibitor for mild steel: Insight from experimental, computational, multivariate statistics and multi-quadratic regression based machine learning model
title_short 1-Hexadecyl-3-methylimidazolium tetrachloroindate ionic liquid as corrosion inhibitor for mild steel: Insight from experimental, computational, multivariate statistics and multi-quadratic regression based machine learning model
title_sort 1 hexadecyl 3 methylimidazolium tetrachloroindate ionic liquid as corrosion inhibitor for mild steel insight from experimental computational multivariate statistics and multi quadratic regression based machine learning model
topic Corrosion
Ionic liquid
Mild steel
Machine learning
Computational
url http://www.sciencedirect.com/science/article/pii/S2590123024013707
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