Hydrothermal Synthesis of Ni/Al Layered Double Hydroxide Nanorods

Ni/Al layered double hydroxide (LDH) nanorods were successfully synthesized by the hydrothermal reaction. The crystal structure of the products was characterized by X-ray diffraction (XRD). The morphology of the products was observed using transmission electron microscopy (TEM) and field emission sc...

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Main Authors: Yun Zhao, Fenfei Xiao, Qingze Jiao
Format: Article
Language:English
Published: Wiley 2011-01-01
Series:Journal of Nanotechnology
Online Access:http://dx.doi.org/10.1155/2011/646409
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author Yun Zhao
Fenfei Xiao
Qingze Jiao
author_facet Yun Zhao
Fenfei Xiao
Qingze Jiao
author_sort Yun Zhao
collection DOAJ
description Ni/Al layered double hydroxide (LDH) nanorods were successfully synthesized by the hydrothermal reaction. The crystal structure of the products was characterized by X-ray diffraction (XRD). The morphology of the products was observed using transmission electron microscopy (TEM) and field emission scanning electron microscopy (SEM). The influences of reaction time and pH value on the morphology of the Ni/Al LDHs were investigated. The result showed that the well-crystallized nanorods of Ni/Al LDHs could be obtained when the pH value was about 10.0 with a long reaction time (12–18 h) at 180°C.
format Article
id doaj-art-5dfd02bd35f2441388a68e20fcd5f236
institution DOAJ
issn 1687-9503
1687-9511
language English
publishDate 2011-01-01
publisher Wiley
record_format Article
series Journal of Nanotechnology
spelling doaj-art-5dfd02bd35f2441388a68e20fcd5f2362025-08-20T03:18:08ZengWileyJournal of Nanotechnology1687-95031687-95112011-01-01201110.1155/2011/646409646409Hydrothermal Synthesis of Ni/Al Layered Double Hydroxide NanorodsYun Zhao0Fenfei Xiao1Qingze Jiao2School of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing 100081, ChinaSchool of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing 100081, ChinaSchool of Chemical Engineering and Environment, Beijing Institute of Technology, Beijing 100081, ChinaNi/Al layered double hydroxide (LDH) nanorods were successfully synthesized by the hydrothermal reaction. The crystal structure of the products was characterized by X-ray diffraction (XRD). The morphology of the products was observed using transmission electron microscopy (TEM) and field emission scanning electron microscopy (SEM). The influences of reaction time and pH value on the morphology of the Ni/Al LDHs were investigated. The result showed that the well-crystallized nanorods of Ni/Al LDHs could be obtained when the pH value was about 10.0 with a long reaction time (12–18 h) at 180°C.http://dx.doi.org/10.1155/2011/646409
spellingShingle Yun Zhao
Fenfei Xiao
Qingze Jiao
Hydrothermal Synthesis of Ni/Al Layered Double Hydroxide Nanorods
Journal of Nanotechnology
title Hydrothermal Synthesis of Ni/Al Layered Double Hydroxide Nanorods
title_full Hydrothermal Synthesis of Ni/Al Layered Double Hydroxide Nanorods
title_fullStr Hydrothermal Synthesis of Ni/Al Layered Double Hydroxide Nanorods
title_full_unstemmed Hydrothermal Synthesis of Ni/Al Layered Double Hydroxide Nanorods
title_short Hydrothermal Synthesis of Ni/Al Layered Double Hydroxide Nanorods
title_sort hydrothermal synthesis of ni al layered double hydroxide nanorods
url http://dx.doi.org/10.1155/2011/646409
work_keys_str_mv AT yunzhao hydrothermalsynthesisofniallayereddoublehydroxidenanorods
AT fenfeixiao hydrothermalsynthesisofniallayereddoublehydroxidenanorods
AT qingzejiao hydrothermalsynthesisofniallayereddoublehydroxidenanorods