Poly[2]catenanes-based hydrogels prepared by hydroxyl-yne click chemistry

Polycatenanes as a typical type of mechanically interlocked polymers (MIP), composing of some interlocked cycles through topology bonding has been extensively investigated. However, the comprehension regarding polycatenanes-based materials still lags behind other kinds of MIP. Therein, polyrotaxanes...

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Main Authors: Jinsa Li, Ziqing Hu, Hanwei Zhang, Xiaofan Ji
Format: Article
Language:English
Published: KeAi Communications Co., Ltd. 2024-12-01
Series:Supramolecular Materials
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Online Access:http://www.sciencedirect.com/science/article/pii/S266724052400014X
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author Jinsa Li
Ziqing Hu
Hanwei Zhang
Xiaofan Ji
author_facet Jinsa Li
Ziqing Hu
Hanwei Zhang
Xiaofan Ji
author_sort Jinsa Li
collection DOAJ
description Polycatenanes as a typical type of mechanically interlocked polymers (MIP), composing of some interlocked cycles through topology bonding has been extensively investigated. However, the comprehension regarding polycatenanes-based materials still lags behind other kinds of MIP. Therein, polyrotaxanes and slide-ring gels were able to fabricate in water to produce hydrogel. Hydrogel materials play an important role in tissue engineering, cell culture, flexible devices and other fields because of their softness and good biocompatibility. However, there was rare reports concerning polycatenanes-based hydrogels. Here, we prepared poly[2]catenanes-based hydrogel G12 incorporating hydrogen bonds through hydroxyl‑yne click reactions from M1 and M2. Comparative tests of substituting M2 with M3 involving mechanical bonds only, hydrophobic alkyl diols M4 and hydrophilic ethylene glycol M5 demonstrated that the mechanical bonds and hydrogen bonds could significantly enhance the hydrogel properties. Besides, temperature and acid responsiveness of G12 was elucidated.
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institution DOAJ
issn 2667-2405
language English
publishDate 2024-12-01
publisher KeAi Communications Co., Ltd.
record_format Article
series Supramolecular Materials
spelling doaj-art-5abdf5bff4d84b5c852f76d239d6bdca2025-08-20T02:58:30ZengKeAi Communications Co., Ltd.Supramolecular Materials2667-24052024-12-01310007610.1016/j.supmat.2024.100076Poly[2]catenanes-based hydrogels prepared by hydroxyl-yne click chemistryJinsa Li0Ziqing Hu1Hanwei Zhang2Xiaofan Ji3Key Laboratory of Materials Chemistry for Energy Conversion and Storage, Ministry of Education, Hubei Key Laboratory of Materials Chemistry and Service Failure, Hubei Engineering Research Center for Biomaterials and Medical Protective Materials, State Key Laboratory of Materials Processing and Die & Mould Technology, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, ChinaKey Laboratory of Materials Chemistry for Energy Conversion and Storage, Ministry of Education, Hubei Key Laboratory of Materials Chemistry and Service Failure, Hubei Engineering Research Center for Biomaterials and Medical Protective Materials, State Key Laboratory of Materials Processing and Die & Mould Technology, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, ChinaKey Laboratory of Materials Chemistry for Energy Conversion and Storage, Ministry of Education, Hubei Key Laboratory of Materials Chemistry and Service Failure, Hubei Engineering Research Center for Biomaterials and Medical Protective Materials, State Key Laboratory of Materials Processing and Die & Mould Technology, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, ChinaCorresponding author.; Key Laboratory of Materials Chemistry for Energy Conversion and Storage, Ministry of Education, Hubei Key Laboratory of Materials Chemistry and Service Failure, Hubei Engineering Research Center for Biomaterials and Medical Protective Materials, State Key Laboratory of Materials Processing and Die & Mould Technology, School of Chemistry and Chemical Engineering, Huazhong University of Science and Technology, Wuhan 430074, ChinaPolycatenanes as a typical type of mechanically interlocked polymers (MIP), composing of some interlocked cycles through topology bonding has been extensively investigated. However, the comprehension regarding polycatenanes-based materials still lags behind other kinds of MIP. Therein, polyrotaxanes and slide-ring gels were able to fabricate in water to produce hydrogel. Hydrogel materials play an important role in tissue engineering, cell culture, flexible devices and other fields because of their softness and good biocompatibility. However, there was rare reports concerning polycatenanes-based hydrogels. Here, we prepared poly[2]catenanes-based hydrogel G12 incorporating hydrogen bonds through hydroxyl‑yne click reactions from M1 and M2. Comparative tests of substituting M2 with M3 involving mechanical bonds only, hydrophobic alkyl diols M4 and hydrophilic ethylene glycol M5 demonstrated that the mechanical bonds and hydrogen bonds could significantly enhance the hydrogel properties. Besides, temperature and acid responsiveness of G12 was elucidated.http://www.sciencedirect.com/science/article/pii/S266724052400014XPoly[2]catenanesHydrogelClick chemistry
spellingShingle Jinsa Li
Ziqing Hu
Hanwei Zhang
Xiaofan Ji
Poly[2]catenanes-based hydrogels prepared by hydroxyl-yne click chemistry
Supramolecular Materials
Poly[2]catenanes
Hydrogel
Click chemistry
title Poly[2]catenanes-based hydrogels prepared by hydroxyl-yne click chemistry
title_full Poly[2]catenanes-based hydrogels prepared by hydroxyl-yne click chemistry
title_fullStr Poly[2]catenanes-based hydrogels prepared by hydroxyl-yne click chemistry
title_full_unstemmed Poly[2]catenanes-based hydrogels prepared by hydroxyl-yne click chemistry
title_short Poly[2]catenanes-based hydrogels prepared by hydroxyl-yne click chemistry
title_sort poly 2 catenanes based hydrogels prepared by hydroxyl yne click chemistry
topic Poly[2]catenanes
Hydrogel
Click chemistry
url http://www.sciencedirect.com/science/article/pii/S266724052400014X
work_keys_str_mv AT jinsali poly2catenanesbasedhydrogelspreparedbyhydroxylyneclickchemistry
AT ziqinghu poly2catenanesbasedhydrogelspreparedbyhydroxylyneclickchemistry
AT hanweizhang poly2catenanesbasedhydrogelspreparedbyhydroxylyneclickchemistry
AT xiaofanji poly2catenanesbasedhydrogelspreparedbyhydroxylyneclickchemistry