Free Reducing Agent, One Pot, and Two Steps Synthesis of Ag@SiO2 Core-shells using Microwave Irradiation
In this work a new method for the fabrication of Ag@SiO2 nanoparticles have been proposed that is completely different from Stober method. Ag nanoparticles were synthesized using microwave irradiation. polyvinylpyrrolidone was used as stabilizer and capping agent, 3-Aminopropyltriethoxysilane as fun...
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| Format: | Article |
| Language: | English |
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Sumy State University
2016-10-01
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| Series: | Журнал нано- та електронної фізики |
| Subjects: | |
| Online Access: | http://jnep.sumdu.edu.ua/download/numbers/2016/3/articles/Proof_jnep_2016_V8_03020.pdf |
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| author | M. Karimipour S. Mostoufirad M. Molaei H. Rezvani Nikabadi A. Ghasempour Nesheli |
| author_facet | M. Karimipour S. Mostoufirad M. Molaei H. Rezvani Nikabadi A. Ghasempour Nesheli |
| author_sort | M. Karimipour |
| collection | DOAJ |
| description | In this work a new method for the fabrication of Ag@SiO2 nanoparticles have been proposed that is completely different from Stober method. Ag nanoparticles were synthesized using microwave irradiation. polyvinylpyrrolidone was used as stabilizer and capping agent, 3-Aminopropyltriethoxysilane as functionalizer of silver particles in fully ethanol solution. The Ag nanoparticles were used subsequently without any subtraction and treatment in the preparation of Ag@SiO2 core-shell nanoparticles. UV-Vis spectroscopy shows a characteristic plasmon peak at 400 nm and 430 nm for Ag nanoparticles and Ag@SiO2 core-shells. Transmission electron microscope images show that Ag nanoparticles have the average size of 10 nm. It is also depicted that SiO2 shell structure was formed uniformly with the average size of 10 nm. The application of 3-Aminopropyltriethoxysilane in the preparation of core-shells yields single Ag core structure. |
| format | Article |
| id | doaj-art-5aa7e960e1f54e67bb1d5bc8520f3fae |
| institution | OA Journals |
| issn | 2077-6772 |
| language | English |
| publishDate | 2016-10-01 |
| publisher | Sumy State University |
| record_format | Article |
| series | Журнал нано- та електронної фізики |
| spelling | doaj-art-5aa7e960e1f54e67bb1d5bc8520f3fae2025-08-20T01:57:25ZengSumy State UniversityЖурнал нано- та електронної фізики2077-67722016-10-018303020-103020-410.21272/jnep.8(3).03020Free Reducing Agent, One Pot, and Two Steps Synthesis of Ag@SiO2 Core-shells using Microwave IrradiationM. Karimipour0S. Mostoufirad1M. Molaei2H. Rezvani Nikabadi3A. Ghasempour Nesheli4Department of Physics, Vali-e-Asr University of Rafsanjan, 77139-36417 Rafsanjan, IranDepartment of Physics, Vali-e-Asr University of Rafsanjan, 77139-36417 Rafsanjan, IranDepartment of Physics, Vali-e-Asr University of Rafsanjan, 77139-36417 Rafsanjan, IranFaculty of science, International University of Imam Reza, Mashhad, IranDepartment of Physics, Shiraz Branch, Islamic Azad University, Shiraz, IranIn this work a new method for the fabrication of Ag@SiO2 nanoparticles have been proposed that is completely different from Stober method. Ag nanoparticles were synthesized using microwave irradiation. polyvinylpyrrolidone was used as stabilizer and capping agent, 3-Aminopropyltriethoxysilane as functionalizer of silver particles in fully ethanol solution. The Ag nanoparticles were used subsequently without any subtraction and treatment in the preparation of Ag@SiO2 core-shell nanoparticles. UV-Vis spectroscopy shows a characteristic plasmon peak at 400 nm and 430 nm for Ag nanoparticles and Ag@SiO2 core-shells. Transmission electron microscope images show that Ag nanoparticles have the average size of 10 nm. It is also depicted that SiO2 shell structure was formed uniformly with the average size of 10 nm. The application of 3-Aminopropyltriethoxysilane in the preparation of core-shells yields single Ag core structure.http://jnep.sumdu.edu.ua/download/numbers/2016/3/articles/Proof_jnep_2016_V8_03020.pdfAg@SiO2MicrowaveAPTSPolyvinylpyrrolidonePlasmo |
| spellingShingle | M. Karimipour S. Mostoufirad M. Molaei H. Rezvani Nikabadi A. Ghasempour Nesheli Free Reducing Agent, One Pot, and Two Steps Synthesis of Ag@SiO2 Core-shells using Microwave Irradiation Журнал нано- та електронної фізики Ag@SiO2 Microwave APTS Polyvinylpyrrolidone Plasmo |
| title | Free Reducing Agent, One Pot, and Two Steps Synthesis of Ag@SiO2 Core-shells using Microwave Irradiation |
| title_full | Free Reducing Agent, One Pot, and Two Steps Synthesis of Ag@SiO2 Core-shells using Microwave Irradiation |
| title_fullStr | Free Reducing Agent, One Pot, and Two Steps Synthesis of Ag@SiO2 Core-shells using Microwave Irradiation |
| title_full_unstemmed | Free Reducing Agent, One Pot, and Two Steps Synthesis of Ag@SiO2 Core-shells using Microwave Irradiation |
| title_short | Free Reducing Agent, One Pot, and Two Steps Synthesis of Ag@SiO2 Core-shells using Microwave Irradiation |
| title_sort | free reducing agent one pot and two steps synthesis of ag sio2 core shells using microwave irradiation |
| topic | Ag@SiO2 Microwave APTS Polyvinylpyrrolidone Plasmo |
| url | http://jnep.sumdu.edu.ua/download/numbers/2016/3/articles/Proof_jnep_2016_V8_03020.pdf |
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