Modification of graphene with silica nanoparticles for use in hybrid network formation from epoxy, novolac, and epoxidized novolac resins by sol-gel method: Investigation of thermal properties

Thermal stability of hybrid composites prepared from epoxy, novolac, and epoxidized-novolac resins and also modified graphene oxide (SFGO) was studied. SFGO was prepared by covering graphene oxide with silica nanoparticles and a bifunctional silane modifier. The first hybrid was prepared from SFGO a...

Full description

Saved in:
Bibliographic Details
Main Authors: A. Mousavi, H. Roghani-Mamaqani, M. Salami-Kalajahi, S. Shahi, A. Abdollahi
Format: Article
Language:English
Published: Budapest University of Technology and Economics 2018-03-01
Series:eXPRESS Polymer Letters
Subjects:
Online Access:http://www.expresspolymlett.com/letolt.php?file=EPL-0008636&mi=cd
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1849412155092238336
author A. Mousavi
H. Roghani-Mamaqani
M. Salami-Kalajahi
S. Shahi
A. Abdollahi
author_facet A. Mousavi
H. Roghani-Mamaqani
M. Salami-Kalajahi
S. Shahi
A. Abdollahi
author_sort A. Mousavi
collection DOAJ
description Thermal stability of hybrid composites prepared from epoxy, novolac, and epoxidized-novolac resins and also modified graphene oxide (SFGO) was studied. SFGO was prepared by covering graphene oxide with silica nanoparticles and a bifunctional silane modifier. The first hybrid was prepared from SFGO and silane-modified epoxy resin. The second one was prepared from SFGO, and silane-modified epoxy and novolac resins. The third hybrid was formed from SFGO, silane-modified novolac, and epoxidized novolac resins. Fourier transform infrared (FT-IR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), and thermogravimetric analysis (TGA) results showed that modification of graphene oxide was carried out successfully. TGA results show that degradation temperature and char residue of resins were increased through their incorporation into hybrid network with SFGO. In addition, the most increase of char residue was observed for the hybrid composites formed from SFGO and modified novolac and epoxy resins.
format Article
id doaj-art-59f55e5fd7cc400bb181a979e93ade71
institution Kabale University
issn 1788-618X
language English
publishDate 2018-03-01
publisher Budapest University of Technology and Economics
record_format Article
series eXPRESS Polymer Letters
spelling doaj-art-59f55e5fd7cc400bb181a979e93ade712025-08-20T03:34:32ZengBudapest University of Technology and EconomicseXPRESS Polymer Letters1788-618X2018-03-0112318720210.3144/expresspolymlett.2018.18Modification of graphene with silica nanoparticles for use in hybrid network formation from epoxy, novolac, and epoxidized novolac resins by sol-gel method: Investigation of thermal propertiesA. MousaviH. Roghani-MamaqaniM. Salami-KalajahiS. ShahiA. AbdollahiThermal stability of hybrid composites prepared from epoxy, novolac, and epoxidized-novolac resins and also modified graphene oxide (SFGO) was studied. SFGO was prepared by covering graphene oxide with silica nanoparticles and a bifunctional silane modifier. The first hybrid was prepared from SFGO and silane-modified epoxy resin. The second one was prepared from SFGO, and silane-modified epoxy and novolac resins. The third hybrid was formed from SFGO, silane-modified novolac, and epoxidized novolac resins. Fourier transform infrared (FT-IR), X-ray photoelectron spectroscopy (XPS), X-ray diffraction (XRD), and thermogravimetric analysis (TGA) results showed that modification of graphene oxide was carried out successfully. TGA results show that degradation temperature and char residue of resins were increased through their incorporation into hybrid network with SFGO. In addition, the most increase of char residue was observed for the hybrid composites formed from SFGO and modified novolac and epoxy resins.http://www.expresspolymlett.com/letolt.php?file=EPL-0008636&mi=cdPolymer compositesgraphenesilica nanoparticleepoxidized novolac resinsol-gel
spellingShingle A. Mousavi
H. Roghani-Mamaqani
M. Salami-Kalajahi
S. Shahi
A. Abdollahi
Modification of graphene with silica nanoparticles for use in hybrid network formation from epoxy, novolac, and epoxidized novolac resins by sol-gel method: Investigation of thermal properties
eXPRESS Polymer Letters
Polymer composites
graphene
silica nanoparticle
epoxidized novolac resin
sol-gel
title Modification of graphene with silica nanoparticles for use in hybrid network formation from epoxy, novolac, and epoxidized novolac resins by sol-gel method: Investigation of thermal properties
title_full Modification of graphene with silica nanoparticles for use in hybrid network formation from epoxy, novolac, and epoxidized novolac resins by sol-gel method: Investigation of thermal properties
title_fullStr Modification of graphene with silica nanoparticles for use in hybrid network formation from epoxy, novolac, and epoxidized novolac resins by sol-gel method: Investigation of thermal properties
title_full_unstemmed Modification of graphene with silica nanoparticles for use in hybrid network formation from epoxy, novolac, and epoxidized novolac resins by sol-gel method: Investigation of thermal properties
title_short Modification of graphene with silica nanoparticles for use in hybrid network formation from epoxy, novolac, and epoxidized novolac resins by sol-gel method: Investigation of thermal properties
title_sort modification of graphene with silica nanoparticles for use in hybrid network formation from epoxy novolac and epoxidized novolac resins by sol gel method investigation of thermal properties
topic Polymer composites
graphene
silica nanoparticle
epoxidized novolac resin
sol-gel
url http://www.expresspolymlett.com/letolt.php?file=EPL-0008636&mi=cd
work_keys_str_mv AT amousavi modificationofgraphenewithsilicananoparticlesforuseinhybridnetworkformationfromepoxynovolacandepoxidizednovolacresinsbysolgelmethodinvestigationofthermalproperties
AT hroghanimamaqani modificationofgraphenewithsilicananoparticlesforuseinhybridnetworkformationfromepoxynovolacandepoxidizednovolacresinsbysolgelmethodinvestigationofthermalproperties
AT msalamikalajahi modificationofgraphenewithsilicananoparticlesforuseinhybridnetworkformationfromepoxynovolacandepoxidizednovolacresinsbysolgelmethodinvestigationofthermalproperties
AT sshahi modificationofgraphenewithsilicananoparticlesforuseinhybridnetworkformationfromepoxynovolacandepoxidizednovolacresinsbysolgelmethodinvestigationofthermalproperties
AT aabdollahi modificationofgraphenewithsilicananoparticlesforuseinhybridnetworkformationfromepoxynovolacandepoxidizednovolacresinsbysolgelmethodinvestigationofthermalproperties