Developing antioxidant of gold nanofilm by a facile electrodeposition method

Antioxidant activity of gold nanoparticles (AuNPs) is known to have considerable therapeutic benefits in the field of medicine. This study aimed to synthesize AuNPs in the form of gold nanofilms (AuNFs) and characterize their antioxidant activity by controlling preparation parameters of scan rate. T...

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Main Authors: Setia Budi, Babay Asih Suliasih, Ibrahim Dhuafa Fikri, Afrizal, Marissa Angelina
Format: Article
Language:English
Published: Wolters Kluwer Medknow Publications 2024-10-01
Series:Journal of Advanced Pharmaceutical Technology & Research
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Online Access:https://journals.lww.com/japtr/fulltext/2024/15040/developing_antioxidant_of_gold_nanofilm_by_a.13.aspx
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author Setia Budi
Babay Asih Suliasih
Ibrahim Dhuafa Fikri
Afrizal
Marissa Angelina
author_facet Setia Budi
Babay Asih Suliasih
Ibrahim Dhuafa Fikri
Afrizal
Marissa Angelina
author_sort Setia Budi
collection DOAJ
description Antioxidant activity of gold nanoparticles (AuNPs) is known to have considerable therapeutic benefits in the field of medicine. This study aimed to synthesize AuNPs in the form of gold nanofilms (AuNFs) and characterize their antioxidant activity by controlling preparation parameters of scan rate. The AuNFs were synthesized by cyclic voltammetry technique by varying scan rates. The antioxidant capacity was measured using in vitro 2,2-diphenyl-1-picrylhydrazyl assay. The effect of incubation time on the assay was also observed by varying the incubation periods to 30, 45, 60, 75, and 90 min. Antioxidant activity of AuNPs gradually increased from 15.18% ±1.8% to 46.17% ±1.87% with the increase in the scan rate. The examination of the variation in incubation time reveals that all samples exhibited a slight increase of inhibition percentage that ranged from 0.47 to 2.17 for each incubation time. This phenomenon showed that the generated AuNFs are classified as slow hydrogen atom transfer. The AuNFs synthesized using the cyclic voltammetry technique exhibited significant antioxidant activity, which was influenced by the scan rate factor. In addition, based on the analysis of incubation time variation, these AuNFs demonstrated a slow hydrogen atom transfer in relation to their reaction kinetics with free radicals.
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issn 0976-2094
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publishDate 2024-10-01
publisher Wolters Kluwer Medknow Publications
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spelling doaj-art-59e4aa8c34f8464bb87e8b580072fc222025-08-20T02:35:39ZengWolters Kluwer Medknow PublicationsJournal of Advanced Pharmaceutical Technology & Research0976-20942024-10-0115432032510.4103/JAPTR.JAPTR_138_24Developing antioxidant of gold nanofilm by a facile electrodeposition methodSetia BudiBabay Asih SuliasihIbrahim Dhuafa FikriAfrizalMarissa AngelinaAntioxidant activity of gold nanoparticles (AuNPs) is known to have considerable therapeutic benefits in the field of medicine. This study aimed to synthesize AuNPs in the form of gold nanofilms (AuNFs) and characterize their antioxidant activity by controlling preparation parameters of scan rate. The AuNFs were synthesized by cyclic voltammetry technique by varying scan rates. The antioxidant capacity was measured using in vitro 2,2-diphenyl-1-picrylhydrazyl assay. The effect of incubation time on the assay was also observed by varying the incubation periods to 30, 45, 60, 75, and 90 min. Antioxidant activity of AuNPs gradually increased from 15.18% ±1.8% to 46.17% ±1.87% with the increase in the scan rate. The examination of the variation in incubation time reveals that all samples exhibited a slight increase of inhibition percentage that ranged from 0.47 to 2.17 for each incubation time. This phenomenon showed that the generated AuNFs are classified as slow hydrogen atom transfer. The AuNFs synthesized using the cyclic voltammetry technique exhibited significant antioxidant activity, which was influenced by the scan rate factor. In addition, based on the analysis of incubation time variation, these AuNFs demonstrated a slow hydrogen atom transfer in relation to their reaction kinetics with free radicals.https://journals.lww.com/japtr/fulltext/2024/15040/developing_antioxidant_of_gold_nanofilm_by_a.13.aspxantioxidant; electrodeposition; gold nanofilm
spellingShingle Setia Budi
Babay Asih Suliasih
Ibrahim Dhuafa Fikri
Afrizal
Marissa Angelina
Developing antioxidant of gold nanofilm by a facile electrodeposition method
Journal of Advanced Pharmaceutical Technology & Research
antioxidant; electrodeposition; gold nanofilm
title Developing antioxidant of gold nanofilm by a facile electrodeposition method
title_full Developing antioxidant of gold nanofilm by a facile electrodeposition method
title_fullStr Developing antioxidant of gold nanofilm by a facile electrodeposition method
title_full_unstemmed Developing antioxidant of gold nanofilm by a facile electrodeposition method
title_short Developing antioxidant of gold nanofilm by a facile electrodeposition method
title_sort developing antioxidant of gold nanofilm by a facile electrodeposition method
topic antioxidant; electrodeposition; gold nanofilm
url https://journals.lww.com/japtr/fulltext/2024/15040/developing_antioxidant_of_gold_nanofilm_by_a.13.aspx
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AT ibrahimdhuafafikri developingantioxidantofgoldnanofilmbyafacileelectrodepositionmethod
AT afrizal developingantioxidantofgoldnanofilmbyafacileelectrodepositionmethod
AT marissaangelina developingantioxidantofgoldnanofilmbyafacileelectrodepositionmethod