Few-Layered MXene Modulating In Situ Growth of Carbon Nanotubes for Enhanced Microwave Absorption

MXene is widely used in the fields of microwave absorption and electromagnetic shielding to balance electromagnetic pollution with the development of communication technologies and human health, due to its excellent surface functional groups and tunable electronic properties. Although pure multilaye...

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Main Authors: Qing Tang, Qi Fan, Lei He, Ping Yu, Qing Huang, Yuanming Chen, Bingbing Fan, Kun Liang
Format: Article
Language:English
Published: MDPI AG 2025-04-01
Series:Molecules
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Online Access:https://www.mdpi.com/1420-3049/30/7/1625
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author Qing Tang
Qi Fan
Lei He
Ping Yu
Qing Huang
Yuanming Chen
Bingbing Fan
Kun Liang
author_facet Qing Tang
Qi Fan
Lei He
Ping Yu
Qing Huang
Yuanming Chen
Bingbing Fan
Kun Liang
author_sort Qing Tang
collection DOAJ
description MXene is widely used in the fields of microwave absorption and electromagnetic shielding to balance electromagnetic pollution with the development of communication technologies and human health, due to its excellent surface functional groups and tunable electronic properties. Although pure multilayered MXene has an excellent accordion-like structure, the weak dielectric loss and lack of magnetic loss result in poor microwave absorption performance. Here, we propose a strategy for the catalytic growth of CNTs by the electrophoretic deposition of adsorbed metal ions, leading to the successful preparation of Ni-MWCNTs/Ti<sub>3</sub>C<sub>2</sub>T<i><sub>x</sub></i> composites with a “layer-by-layer” structure, achieved through in situ regulated growth of CNTs. By introducing dielectric–magnetic synergy to improve the impedance matching conditions, and by regulating the diameter of the CNTs to alter the electromagnetic parameters of Ni-MWCNTs/Ti<sub>3</sub>C<sub>2</sub>T<i><sub>x</sub></i>, the 2-Ni-MWCNTs/Ti<sub>3</sub>C<sub>2</sub>T<i><sub>x</sub></i> composite achieves the best reflection loss (RL) value of −44.08 dB and an effective absorption bandwidth of 1.52 GHz at only 2.49 mm thickness. This unique layered structure and the regulation strategy provide new opportunities for the development of few-layered MXene composites.
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spelling doaj-art-570fa15b513346a8a2b13b00e06c9ca52025-08-20T03:08:57ZengMDPI AGMolecules1420-30492025-04-01307162510.3390/molecules30071625Few-Layered MXene Modulating In Situ Growth of Carbon Nanotubes for Enhanced Microwave AbsorptionQing Tang0Qi Fan1Lei He2Ping Yu3Qing Huang4Yuanming Chen5Bingbing Fan6Kun Liang7Nano Science and Technology Institute, University of Science and Technology of China, Suzhou 215123, ChinaZhejiang Key Laboratory of Data-Driven High-Safety Energy Materials and Applications, Ningbo Key Laboratory of Special Energy Materials and Chemistry, Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo 315201, ChinaZhejiang Key Laboratory of Data-Driven High-Safety Energy Materials and Applications, Ningbo Key Laboratory of Special Energy Materials and Chemistry, Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo 315201, ChinaSchool of Electronic and Information Engineering, Ningbo University of Technology, Ningbo 315211, ChinaZhejiang Key Laboratory of Data-Driven High-Safety Energy Materials and Applications, Ningbo Key Laboratory of Special Energy Materials and Chemistry, Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo 315201, ChinaSchool of Materials and Energy, University of Electronic Science and Technology of China, Chengdu 611731, ChinaSchool of Materials Science and Engineering, Zhengzhou University, Zhengzhou 450001, ChinaZhejiang Key Laboratory of Data-Driven High-Safety Energy Materials and Applications, Ningbo Key Laboratory of Special Energy Materials and Chemistry, Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo 315201, ChinaMXene is widely used in the fields of microwave absorption and electromagnetic shielding to balance electromagnetic pollution with the development of communication technologies and human health, due to its excellent surface functional groups and tunable electronic properties. Although pure multilayered MXene has an excellent accordion-like structure, the weak dielectric loss and lack of magnetic loss result in poor microwave absorption performance. Here, we propose a strategy for the catalytic growth of CNTs by the electrophoretic deposition of adsorbed metal ions, leading to the successful preparation of Ni-MWCNTs/Ti<sub>3</sub>C<sub>2</sub>T<i><sub>x</sub></i> composites with a “layer-by-layer” structure, achieved through in situ regulated growth of CNTs. By introducing dielectric–magnetic synergy to improve the impedance matching conditions, and by regulating the diameter of the CNTs to alter the electromagnetic parameters of Ni-MWCNTs/Ti<sub>3</sub>C<sub>2</sub>T<i><sub>x</sub></i>, the 2-Ni-MWCNTs/Ti<sub>3</sub>C<sub>2</sub>T<i><sub>x</sub></i> composite achieves the best reflection loss (RL) value of −44.08 dB and an effective absorption bandwidth of 1.52 GHz at only 2.49 mm thickness. This unique layered structure and the regulation strategy provide new opportunities for the development of few-layered MXene composites.https://www.mdpi.com/1420-3049/30/7/1625electromagnetic wave absorptiontwo-dimensional materialfew-layered MXeneMWCNTselectrophoretic deposition
spellingShingle Qing Tang
Qi Fan
Lei He
Ping Yu
Qing Huang
Yuanming Chen
Bingbing Fan
Kun Liang
Few-Layered MXene Modulating In Situ Growth of Carbon Nanotubes for Enhanced Microwave Absorption
Molecules
electromagnetic wave absorption
two-dimensional material
few-layered MXene
MWCNTs
electrophoretic deposition
title Few-Layered MXene Modulating In Situ Growth of Carbon Nanotubes for Enhanced Microwave Absorption
title_full Few-Layered MXene Modulating In Situ Growth of Carbon Nanotubes for Enhanced Microwave Absorption
title_fullStr Few-Layered MXene Modulating In Situ Growth of Carbon Nanotubes for Enhanced Microwave Absorption
title_full_unstemmed Few-Layered MXene Modulating In Situ Growth of Carbon Nanotubes for Enhanced Microwave Absorption
title_short Few-Layered MXene Modulating In Situ Growth of Carbon Nanotubes for Enhanced Microwave Absorption
title_sort few layered mxene modulating in situ growth of carbon nanotubes for enhanced microwave absorption
topic electromagnetic wave absorption
two-dimensional material
few-layered MXene
MWCNTs
electrophoretic deposition
url https://www.mdpi.com/1420-3049/30/7/1625
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AT qifan fewlayeredmxenemodulatinginsitugrowthofcarbonnanotubesforenhancedmicrowaveabsorption
AT leihe fewlayeredmxenemodulatinginsitugrowthofcarbonnanotubesforenhancedmicrowaveabsorption
AT pingyu fewlayeredmxenemodulatinginsitugrowthofcarbonnanotubesforenhancedmicrowaveabsorption
AT qinghuang fewlayeredmxenemodulatinginsitugrowthofcarbonnanotubesforenhancedmicrowaveabsorption
AT yuanmingchen fewlayeredmxenemodulatinginsitugrowthofcarbonnanotubesforenhancedmicrowaveabsorption
AT bingbingfan fewlayeredmxenemodulatinginsitugrowthofcarbonnanotubesforenhancedmicrowaveabsorption
AT kunliang fewlayeredmxenemodulatinginsitugrowthofcarbonnanotubesforenhancedmicrowaveabsorption