Evaluation methods of mechanical properties for low-k dielectrics

This review introduces the study of state-of-art methods for assessing the mechanical properties of insulating materials with low dielectric constant. The main features of measuring Young’s modulus of thin films insulating materials with low dielectric constant are determined by usage of Brillouin l...

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Main Author: I. S. Ovchinnikov
Format: Article
Language:Russian
Published: MIREA - Russian Technological University 2021-06-01
Series:Российский технологический журнал
Subjects:
Online Access:https://www.rtj-mirea.ru/jour/article/view/326
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author I. S. Ovchinnikov
author_facet I. S. Ovchinnikov
author_sort I. S. Ovchinnikov
collection DOAJ
description This review introduces the study of state-of-art methods for assessing the mechanical properties of insulating materials with low dielectric constant. The main features of measuring Young’s modulus of thin films insulating materials with low dielectric constant are determined by usage of Brillouin light scattering, surface acoustic wave spectroscopy, picosecond laser-acoustic method, ellipsometric porosimetry, nanoindentation and atomic force microscopy in various modes. The author estimated the optimum lateral and optimum depth resolution for each above method. The review analyzes the degree of sample preparation complexity for the measurements by these methods and describes what methods of measurement are destructive for the samples. Besides, the review makes a comparison for the results of evaluating Young’s modulus of insulating materials with low dielectric constant achieved by different methods. Comparative analysis of the methods for assessing mechanical properties lead us to the conclusion that the method of atomic force microscopy is superior to other methods described above, both in lateral (8 nm) and optimum depth (10 nm) resolution. It is shown that due to the small impact force of the atomic force microscope probe on the surface, the method does not have a destructive effect on the sample. In addition, there is no need to create special conditions for the experiment (e.g., the cleanliness level of the premises, the possibility of an experiment under environmental conditions, etc.). This makes the experiment relatively simple in terms of preparing the object of research. It has been also established that the method of atomic force microscopy in the mode of quantitative nanomechanical mapping allows forming a map of the distribution of the Young’s modulus of the insulating material as part of the metallization system of integrated circuits.
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spelling doaj-art-5704d085e3da40338d0af5ec37be507c2025-08-20T02:53:51ZrusMIREA - Russian Technological UniversityРоссийский технологический журнал2782-32102500-316X2021-06-0193404810.32362/2500-316X-2021-9-3-40-48260Evaluation methods of mechanical properties for low-k dielectricsI. S. Ovchinnikov0MIREA – Russian Technological UniversityThis review introduces the study of state-of-art methods for assessing the mechanical properties of insulating materials with low dielectric constant. The main features of measuring Young’s modulus of thin films insulating materials with low dielectric constant are determined by usage of Brillouin light scattering, surface acoustic wave spectroscopy, picosecond laser-acoustic method, ellipsometric porosimetry, nanoindentation and atomic force microscopy in various modes. The author estimated the optimum lateral and optimum depth resolution for each above method. The review analyzes the degree of sample preparation complexity for the measurements by these methods and describes what methods of measurement are destructive for the samples. Besides, the review makes a comparison for the results of evaluating Young’s modulus of insulating materials with low dielectric constant achieved by different methods. Comparative analysis of the methods for assessing mechanical properties lead us to the conclusion that the method of atomic force microscopy is superior to other methods described above, both in lateral (8 nm) and optimum depth (10 nm) resolution. It is shown that due to the small impact force of the atomic force microscope probe on the surface, the method does not have a destructive effect on the sample. In addition, there is no need to create special conditions for the experiment (e.g., the cleanliness level of the premises, the possibility of an experiment under environmental conditions, etc.). This makes the experiment relatively simple in terms of preparing the object of research. It has been also established that the method of atomic force microscopy in the mode of quantitative nanomechanical mapping allows forming a map of the distribution of the Young’s modulus of the insulating material as part of the metallization system of integrated circuits.https://www.rtj-mirea.ru/jour/article/view/326young’s moduluslow-k dielectricsnanoindentationatomic force microscopyquantitative nanomechanical mapping mode
spellingShingle I. S. Ovchinnikov
Evaluation methods of mechanical properties for low-k dielectrics
Российский технологический журнал
young’s modulus
low-k dielectrics
nanoindentation
atomic force microscopy
quantitative nanomechanical mapping mode
title Evaluation methods of mechanical properties for low-k dielectrics
title_full Evaluation methods of mechanical properties for low-k dielectrics
title_fullStr Evaluation methods of mechanical properties for low-k dielectrics
title_full_unstemmed Evaluation methods of mechanical properties for low-k dielectrics
title_short Evaluation methods of mechanical properties for low-k dielectrics
title_sort evaluation methods of mechanical properties for low k dielectrics
topic young’s modulus
low-k dielectrics
nanoindentation
atomic force microscopy
quantitative nanomechanical mapping mode
url https://www.rtj-mirea.ru/jour/article/view/326
work_keys_str_mv AT isovchinnikov evaluationmethodsofmechanicalpropertiesforlowkdielectrics