Trema micranthum (L.) Blume as a new source of cannabinoids

Abstract Trema micranthum (Cannabaceae) has emerged as a promising new source of cannabinoids, including cannabidiol (CBD). Given the substantial medicinal demand for cannabinoids and the regulatory challenges associated with Cannabis sativa due to the presence of Δ9-tetrahydrocannabinol (THC), this...

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Main Authors: Rayssa Ribeiro, Yasmin Cunha da Silva, Ricardo Finotti, Gabriel Reis Alves Carneiro, Gustavo Ramalho Cardoso dos Santos, Henrique Marcelo Gualberto Pereira, Monica Costa Padilha, Valdir F. Veiga-Junior
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Language:English
Published: Nature Portfolio 2024-11-01
Series:Scientific Reports
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Online Access:https://doi.org/10.1038/s41598-024-80857-6
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author Rayssa Ribeiro
Yasmin Cunha da Silva
Ricardo Finotti
Gabriel Reis Alves Carneiro
Gustavo Ramalho Cardoso dos Santos
Henrique Marcelo Gualberto Pereira
Monica Costa Padilha
Valdir F. Veiga-Junior
author_facet Rayssa Ribeiro
Yasmin Cunha da Silva
Ricardo Finotti
Gabriel Reis Alves Carneiro
Gustavo Ramalho Cardoso dos Santos
Henrique Marcelo Gualberto Pereira
Monica Costa Padilha
Valdir F. Veiga-Junior
author_sort Rayssa Ribeiro
collection DOAJ
description Abstract Trema micranthum (Cannabaceae) has emerged as a promising new source of cannabinoids, including cannabidiol (CBD). Given the substantial medicinal demand for cannabinoids and the regulatory challenges associated with Cannabis sativa due to the presence of Δ9-tetrahydrocannabinol (THC), this study sought to explore the presence of CBD, THC, and their precursors, Δ9-tetrahydrocannabinolic acid A (THCA A) and cannabidiolic acid (CBDA), in various parts of Trema micranthum using UHPLC-HRMS/MS (Orbitrap). Extracts from fruits, leaves, inflorescences, and stems were obtained using a methanol/hexane (9:1, v/v) solvent mixture. UHPLC coupled with an Orbitrap mass spectrometer was employed for cannabinoid identification and quantification, with standard mixtures prepared in methanol. The extracts yielded significant quantities, such as 6.6%/g from leaves and 3%/g from fruits. Cannabinoids were detected in fruits, leaves, and inflorescences, with acidic forms (CBDA and THCA A) present in higher concentrations than their neutral counterparts. Notably, leaves contained 4.43 × 10−3 µg/g of CBD and 1.05 ×  10−3 µg/g of THC. These findings, facilitated by high-resolution analytical methods, underscore the potential of Trema micranthum as an alternative source for cannabinoids, guiding future research in this area.
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spelling doaj-art-5675ffaf062d45bdb722635f606e79e02025-08-20T02:49:17ZengNature PortfolioScientific Reports2045-23222024-11-011411910.1038/s41598-024-80857-6Trema micranthum (L.) Blume as a new source of cannabinoidsRayssa Ribeiro0Yasmin Cunha da Silva1Ricardo Finotti2Gabriel Reis Alves Carneiro3Gustavo Ramalho Cardoso dos Santos4Henrique Marcelo Gualberto Pereira5Monica Costa Padilha6Valdir F. Veiga-Junior7Department of Chemical Engineering, Military Institute of EngineeringDepartment of Chemical Engineering, Military Institute of EngineeringDepartment of Biology, Universidade Estácio de Sá (UNESA)Chemistry Institute, Federal University of Rio de Janeiro, Brazilian Doping Control Laboratory (LBCD/IQ-UFRJ)Chemistry Institute, Federal University of Rio de Janeiro, Brazilian Doping Control Laboratory (LBCD/IQ-UFRJ)Chemistry Institute, Federal University of Rio de Janeiro, Brazilian Doping Control Laboratory (LBCD/IQ-UFRJ)Chemistry Institute, Federal University of Rio de Janeiro, Brazilian Doping Control Laboratory (LBCD/IQ-UFRJ)Department of Chemical Engineering, Military Institute of EngineeringAbstract Trema micranthum (Cannabaceae) has emerged as a promising new source of cannabinoids, including cannabidiol (CBD). Given the substantial medicinal demand for cannabinoids and the regulatory challenges associated with Cannabis sativa due to the presence of Δ9-tetrahydrocannabinol (THC), this study sought to explore the presence of CBD, THC, and their precursors, Δ9-tetrahydrocannabinolic acid A (THCA A) and cannabidiolic acid (CBDA), in various parts of Trema micranthum using UHPLC-HRMS/MS (Orbitrap). Extracts from fruits, leaves, inflorescences, and stems were obtained using a methanol/hexane (9:1, v/v) solvent mixture. UHPLC coupled with an Orbitrap mass spectrometer was employed for cannabinoid identification and quantification, with standard mixtures prepared in methanol. The extracts yielded significant quantities, such as 6.6%/g from leaves and 3%/g from fruits. Cannabinoids were detected in fruits, leaves, and inflorescences, with acidic forms (CBDA and THCA A) present in higher concentrations than their neutral counterparts. Notably, leaves contained 4.43 × 10−3 µg/g of CBD and 1.05 ×  10−3 µg/g of THC. These findings, facilitated by high-resolution analytical methods, underscore the potential of Trema micranthum as an alternative source for cannabinoids, guiding future research in this area.https://doi.org/10.1038/s41598-024-80857-6CannabaceaeTrema micranthumCannabinoidsCBD/THCUHPLC-HRMS/MS
spellingShingle Rayssa Ribeiro
Yasmin Cunha da Silva
Ricardo Finotti
Gabriel Reis Alves Carneiro
Gustavo Ramalho Cardoso dos Santos
Henrique Marcelo Gualberto Pereira
Monica Costa Padilha
Valdir F. Veiga-Junior
Trema micranthum (L.) Blume as a new source of cannabinoids
Scientific Reports
Cannabaceae
Trema micranthum
Cannabinoids
CBD/THC
UHPLC-HRMS/MS
title Trema micranthum (L.) Blume as a new source of cannabinoids
title_full Trema micranthum (L.) Blume as a new source of cannabinoids
title_fullStr Trema micranthum (L.) Blume as a new source of cannabinoids
title_full_unstemmed Trema micranthum (L.) Blume as a new source of cannabinoids
title_short Trema micranthum (L.) Blume as a new source of cannabinoids
title_sort trema micranthum l blume as a new source of cannabinoids
topic Cannabaceae
Trema micranthum
Cannabinoids
CBD/THC
UHPLC-HRMS/MS
url https://doi.org/10.1038/s41598-024-80857-6
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