Protocol for constructing asymmetric triple-atoms supported on nitrogen-doped carbon nanotubes via atomic layer deposition

Summary: The precise construction of highly efficient triple-atom catalysts (TACs) remains a significant challenge. Here, we present a protocol for constructing asymmetric Pt-Ru-Co triple-atoms (TAs) supported on nitrogen-doped carbon nanotubes (NCNTs) via selective atomic layer deposition (ALD) tec...

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Main Authors: Jingyan Zhang, Zhongxin Song, Xiaozhang Yao, Yi Guan, Ziwei Huo, Ning Chen, Lei Zhang, Xueliang Sun
Format: Article
Language:English
Published: Elsevier 2025-09-01
Series:STAR Protocols
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Online Access:http://www.sciencedirect.com/science/article/pii/S2666166725004113
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Summary:Summary: The precise construction of highly efficient triple-atom catalysts (TACs) remains a significant challenge. Here, we present a protocol for constructing asymmetric Pt-Ru-Co triple-atoms (TAs) supported on nitrogen-doped carbon nanotubes (NCNTs) via selective atomic layer deposition (ALD) technology. We describe steps for synthesizing the NCNT substrate, deposition of Pt-Ru-Co TAs, and characterizing the materials. We then detail procedures for preparing the electrolyte solution and working electrode followed by electrochemistry measurements for hydrogen evolution and hydrogen oxidative reactions with a typical three-electrode system.For complete details on the use and execution of this protocol, please refer to Zhang et al.1 : Publisher’s note: Undertaking any experimental protocol requires adherence to local institutional guidelines for laboratory safety and ethics.
ISSN:2666-1667