The Effect of Surface Functionalization on the Immobilization of Gold Nanoparticles on Graphene Sheets

In our study, graphene oxide is synthesized by Hummers method. And then, carboxylic acid functionalized graphene (graphene-COOH), thiol-functionalized graphene (graphene-SH), and highly dispersive graphene are prepared by chemical modification of respective groups on the graphene surface. Furthermor...

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Main Authors: Min Song, Juan Xu, Changzi Wu
Format: Article
Language:English
Published: Wiley 2012-01-01
Series:Journal of Nanotechnology
Online Access:http://dx.doi.org/10.1155/2012/329318
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author Min Song
Juan Xu
Changzi Wu
author_facet Min Song
Juan Xu
Changzi Wu
author_sort Min Song
collection DOAJ
description In our study, graphene oxide is synthesized by Hummers method. And then, carboxylic acid functionalized graphene (graphene-COOH), thiol-functionalized graphene (graphene-SH), and highly dispersive graphene are prepared by chemical modification of respective groups on the graphene surface. Furthermore, we explore a solution-based approach to prepare three differently functionalized graphene-gold composites by one-step chemical reduction of AuCl4 - ions in respective functionalized graphene suspensions, where the gold nanoparticles are deposited on the functionalized graphene surface during their synthesis process. In addition, we compare the influence of surface functionalization on the growth of gold nanoparticles on graphene surface. Transmission electron morphology (TEM) and ultraviolet-visible (UV-Vis) spectroscopy are employed to study the effect of surface functionalities on AuNPs distribution onto the graphene surface and demonstrate the successful immobilization of AuNPs on graphene surface.
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spelling doaj-art-5576dbbb32504400b14442477cb593bb2025-02-03T05:57:08ZengWileyJournal of Nanotechnology1687-95031687-95112012-01-01201210.1155/2012/329318329318The Effect of Surface Functionalization on the Immobilization of Gold Nanoparticles on Graphene SheetsMin Song0Juan Xu1Changzi Wu2Key Laboratory of Energy Thermal Conversion and Control of Ministry of Education, School of Energy and Environment, Southeast University, Nanjing 210096, ChinaKey Laboratory of Energy Thermal Conversion and Control of Ministry of Education, School of Energy and Environment, Southeast University, Nanjing 210096, ChinaKey Laboratory of Energy Thermal Conversion and Control of Ministry of Education, School of Energy and Environment, Southeast University, Nanjing 210096, ChinaIn our study, graphene oxide is synthesized by Hummers method. And then, carboxylic acid functionalized graphene (graphene-COOH), thiol-functionalized graphene (graphene-SH), and highly dispersive graphene are prepared by chemical modification of respective groups on the graphene surface. Furthermore, we explore a solution-based approach to prepare three differently functionalized graphene-gold composites by one-step chemical reduction of AuCl4 - ions in respective functionalized graphene suspensions, where the gold nanoparticles are deposited on the functionalized graphene surface during their synthesis process. In addition, we compare the influence of surface functionalization on the growth of gold nanoparticles on graphene surface. Transmission electron morphology (TEM) and ultraviolet-visible (UV-Vis) spectroscopy are employed to study the effect of surface functionalities on AuNPs distribution onto the graphene surface and demonstrate the successful immobilization of AuNPs on graphene surface.http://dx.doi.org/10.1155/2012/329318
spellingShingle Min Song
Juan Xu
Changzi Wu
The Effect of Surface Functionalization on the Immobilization of Gold Nanoparticles on Graphene Sheets
Journal of Nanotechnology
title The Effect of Surface Functionalization on the Immobilization of Gold Nanoparticles on Graphene Sheets
title_full The Effect of Surface Functionalization on the Immobilization of Gold Nanoparticles on Graphene Sheets
title_fullStr The Effect of Surface Functionalization on the Immobilization of Gold Nanoparticles on Graphene Sheets
title_full_unstemmed The Effect of Surface Functionalization on the Immobilization of Gold Nanoparticles on Graphene Sheets
title_short The Effect of Surface Functionalization on the Immobilization of Gold Nanoparticles on Graphene Sheets
title_sort effect of surface functionalization on the immobilization of gold nanoparticles on graphene sheets
url http://dx.doi.org/10.1155/2012/329318
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