Cryogenic System for FTIR Analysis of Hydrocarbon Fuels at Low Temperature and Atmospheric Pressure
This study presents a novel approach to FTIR spectroscopy at low temperatures under atmospheric pressure. The work aimed to confirm the efficiency of a fundamentally new cryogenic setup that enables material research under the specified conditions. The new technique combines a nitrogen-based cryogen...
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| Format: | Article |
| Language: | English |
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MDPI AG
2025-07-01
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| Series: | Applied Sciences |
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| Online Access: | https://www.mdpi.com/2076-3417/15/14/7944 |
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| author | Gulzhan Turlybekova Alisher Kenbay Abdurakhman Aldiyarov Yevgeniy Korshikov Aidos Lesbayev Assel Nurmukan Darkhan Yerezhep |
| author_facet | Gulzhan Turlybekova Alisher Kenbay Abdurakhman Aldiyarov Yevgeniy Korshikov Aidos Lesbayev Assel Nurmukan Darkhan Yerezhep |
| author_sort | Gulzhan Turlybekova |
| collection | DOAJ |
| description | This study presents a novel approach to FTIR spectroscopy at low temperatures under atmospheric pressure. The work aimed to confirm the efficiency of a fundamentally new cryogenic setup that enables material research under the specified conditions. The new technique combines a nitrogen-based cryogenic capillary cooling system with precise temperature monitoring via a PID controller, along with DRIFT spectroscopy for hydrocarbon materials. New fundamental data were obtained on the properties and behavior of hydrocarbon compounds such as methanol, kerosene, and ethanol. The IR spectra of these samples contain key characteristic vibrations of hydrocarbon functional groups, which demonstrate the effective operability of the cryogenic device. A detailed description of the setup and measurement technique is provided, along with a thorough comparison of the results with data from other authors. The application scope of the cryogenic device, the relevance of the research, and potential future developments are also discussed. |
| format | Article |
| id | doaj-art-516e07f9ccdf4684a746ba9d3371bd71 |
| institution | Kabale University |
| issn | 2076-3417 |
| language | English |
| publishDate | 2025-07-01 |
| publisher | MDPI AG |
| record_format | Article |
| series | Applied Sciences |
| spelling | doaj-art-516e07f9ccdf4684a746ba9d3371bd712025-08-20T03:36:19ZengMDPI AGApplied Sciences2076-34172025-07-011514794410.3390/app15147944Cryogenic System for FTIR Analysis of Hydrocarbon Fuels at Low Temperature and Atmospheric PressureGulzhan Turlybekova0Alisher Kenbay1Abdurakhman Aldiyarov2Yevgeniy Korshikov3Aidos Lesbayev4Assel Nurmukan5Darkhan Yerezhep6Institute of Energy and Mechanical Engineering, Satbayev University, 22a Satpaev Str., Almaty 050013, KazakhstanInstitute of Energy and Mechanical Engineering, Satbayev University, 22a Satpaev Str., Almaty 050013, KazakhstanInstitute Experimental and Theoretical Physics, Al Farabi Kazakh National University, 71 al-Farabi Ave., Almaty 050040, KazakhstanInstitute Experimental and Theoretical Physics, Al Farabi Kazakh National University, 71 al-Farabi Ave., Almaty 050040, KazakhstanInstitute of Energy and Mechanical Engineering, Satbayev University, 22a Satpaev Str., Almaty 050013, KazakhstanInstitute Experimental and Theoretical Physics, Al Farabi Kazakh National University, 71 al-Farabi Ave., Almaty 050040, KazakhstanInstitute of Energy and Mechanical Engineering, Satbayev University, 22a Satpaev Str., Almaty 050013, KazakhstanThis study presents a novel approach to FTIR spectroscopy at low temperatures under atmospheric pressure. The work aimed to confirm the efficiency of a fundamentally new cryogenic setup that enables material research under the specified conditions. The new technique combines a nitrogen-based cryogenic capillary cooling system with precise temperature monitoring via a PID controller, along with DRIFT spectroscopy for hydrocarbon materials. New fundamental data were obtained on the properties and behavior of hydrocarbon compounds such as methanol, kerosene, and ethanol. The IR spectra of these samples contain key characteristic vibrations of hydrocarbon functional groups, which demonstrate the effective operability of the cryogenic device. A detailed description of the setup and measurement technique is provided, along with a thorough comparison of the results with data from other authors. The application scope of the cryogenic device, the relevance of the research, and potential future developments are also discussed.https://www.mdpi.com/2076-3417/15/14/7944FTIRcryogenichydrocarbonatmospheric pressurelow temperaturemethanol |
| spellingShingle | Gulzhan Turlybekova Alisher Kenbay Abdurakhman Aldiyarov Yevgeniy Korshikov Aidos Lesbayev Assel Nurmukan Darkhan Yerezhep Cryogenic System for FTIR Analysis of Hydrocarbon Fuels at Low Temperature and Atmospheric Pressure Applied Sciences FTIR cryogenic hydrocarbon atmospheric pressure low temperature methanol |
| title | Cryogenic System for FTIR Analysis of Hydrocarbon Fuels at Low Temperature and Atmospheric Pressure |
| title_full | Cryogenic System for FTIR Analysis of Hydrocarbon Fuels at Low Temperature and Atmospheric Pressure |
| title_fullStr | Cryogenic System for FTIR Analysis of Hydrocarbon Fuels at Low Temperature and Atmospheric Pressure |
| title_full_unstemmed | Cryogenic System for FTIR Analysis of Hydrocarbon Fuels at Low Temperature and Atmospheric Pressure |
| title_short | Cryogenic System for FTIR Analysis of Hydrocarbon Fuels at Low Temperature and Atmospheric Pressure |
| title_sort | cryogenic system for ftir analysis of hydrocarbon fuels at low temperature and atmospheric pressure |
| topic | FTIR cryogenic hydrocarbon atmospheric pressure low temperature methanol |
| url | https://www.mdpi.com/2076-3417/15/14/7944 |
| work_keys_str_mv | AT gulzhanturlybekova cryogenicsystemforftiranalysisofhydrocarbonfuelsatlowtemperatureandatmosphericpressure AT alisherkenbay cryogenicsystemforftiranalysisofhydrocarbonfuelsatlowtemperatureandatmosphericpressure AT abdurakhmanaldiyarov cryogenicsystemforftiranalysisofhydrocarbonfuelsatlowtemperatureandatmosphericpressure AT yevgeniykorshikov cryogenicsystemforftiranalysisofhydrocarbonfuelsatlowtemperatureandatmosphericpressure AT aidoslesbayev cryogenicsystemforftiranalysisofhydrocarbonfuelsatlowtemperatureandatmosphericpressure AT asselnurmukan cryogenicsystemforftiranalysisofhydrocarbonfuelsatlowtemperatureandatmosphericpressure AT darkhanyerezhep cryogenicsystemforftiranalysisofhydrocarbonfuelsatlowtemperatureandatmosphericpressure |