Study of matrix micro-cracking in nano clay and acrylic tri-block-copolymer modified epoxy/basalt fiber-reinforced pressure-retaining structures

In fiber-reinforced polymer pressure-retaining structures, such as pipes and vessels, micro-level failure commonly causes fluid permeation due to matrix cracking. This study explores the effect of nano-reinforcements on matrix cracking in filament-wound basalt fiber/epoxy composite structures. The m...

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Format: Article
Language:English
Published: Budapest University of Technology and Economics 2011-10-01
Series:eXPRESS Polymer Letters
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Online Access:http://www.expresspolymlett.com/letolt.php?file=EPL-0002355&mi=cd
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description In fiber-reinforced polymer pressure-retaining structures, such as pipes and vessels, micro-level failure commonly causes fluid permeation due to matrix cracking. This study explores the effect of nano-reinforcements on matrix cracking in filament-wound basalt fiber/epoxy composite structures. The microstructure and mechanical properties of bulk epoxy nanocomposites and hybrid fiber-reinforced composite pipes modified with acrylic tri-block-copolymer and organophilic layered silicate clay were investigated. In cured epoxy, the tri-block-copolymer phase separated into disordered spherical micelle inclusions; an exfoliated and intercalated structure was observed for the nano-clay. Block-copolymer addition significantly enhanced epoxy fracture toughness by a mechanism of particle cavitation and matrix shear yielding, whereas toughness remained unchanged in nano-clay filled nanocomposites due to the occurrence of lower energy resistance phenomena such as crack deflection and branching.Tensile stiffness increased with nano-clay content, while it decreased slightly for block-copolymer modified epoxy. Composite pipes modified with either the organic and inorganic nanoparticles exhibited moderate improvements in leakage failure strain (i.e. matrix cracking strain); however, reductions in functional and structural failure strength were observed.
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series eXPRESS Polymer Letters
spelling doaj-art-4ec2c5be290c476e891e175af885818f2025-08-20T03:33:35ZengBudapest University of Technology and EconomicseXPRESS Polymer Letters1788-618X2011-10-0151088289610.3144/expresspolymlett.2011.87Study of matrix micro-cracking in nano clay and acrylic tri-block-copolymer modified epoxy/basalt fiber-reinforced pressure-retaining structuresIn fiber-reinforced polymer pressure-retaining structures, such as pipes and vessels, micro-level failure commonly causes fluid permeation due to matrix cracking. This study explores the effect of nano-reinforcements on matrix cracking in filament-wound basalt fiber/epoxy composite structures. The microstructure and mechanical properties of bulk epoxy nanocomposites and hybrid fiber-reinforced composite pipes modified with acrylic tri-block-copolymer and organophilic layered silicate clay were investigated. In cured epoxy, the tri-block-copolymer phase separated into disordered spherical micelle inclusions; an exfoliated and intercalated structure was observed for the nano-clay. Block-copolymer addition significantly enhanced epoxy fracture toughness by a mechanism of particle cavitation and matrix shear yielding, whereas toughness remained unchanged in nano-clay filled nanocomposites due to the occurrence of lower energy resistance phenomena such as crack deflection and branching.Tensile stiffness increased with nano-clay content, while it decreased slightly for block-copolymer modified epoxy. Composite pipes modified with either the organic and inorganic nanoparticles exhibited moderate improvements in leakage failure strain (i.e. matrix cracking strain); however, reductions in functional and structural failure strength were observed.http://www.expresspolymlett.com/letolt.php?file=EPL-0002355&mi=cdPolymer compositesEpoxy nanocompositesFilament windingFracture toughnessMatrix cracking
spellingShingle Study of matrix micro-cracking in nano clay and acrylic tri-block-copolymer modified epoxy/basalt fiber-reinforced pressure-retaining structures
eXPRESS Polymer Letters
Polymer composites
Epoxy nanocomposites
Filament winding
Fracture toughness
Matrix cracking
title Study of matrix micro-cracking in nano clay and acrylic tri-block-copolymer modified epoxy/basalt fiber-reinforced pressure-retaining structures
title_full Study of matrix micro-cracking in nano clay and acrylic tri-block-copolymer modified epoxy/basalt fiber-reinforced pressure-retaining structures
title_fullStr Study of matrix micro-cracking in nano clay and acrylic tri-block-copolymer modified epoxy/basalt fiber-reinforced pressure-retaining structures
title_full_unstemmed Study of matrix micro-cracking in nano clay and acrylic tri-block-copolymer modified epoxy/basalt fiber-reinforced pressure-retaining structures
title_short Study of matrix micro-cracking in nano clay and acrylic tri-block-copolymer modified epoxy/basalt fiber-reinforced pressure-retaining structures
title_sort study of matrix micro cracking in nano clay and acrylic tri block copolymer modified epoxy basalt fiber reinforced pressure retaining structures
topic Polymer composites
Epoxy nanocomposites
Filament winding
Fracture toughness
Matrix cracking
url http://www.expresspolymlett.com/letolt.php?file=EPL-0002355&mi=cd