Effect of calcium content on geopolymer consolidation of saline soils in the seasonally frozen zone

Abstract Geopolymers have long been used to stabilise unique soils, and the stabilising conditions and freeze–thaw cycles (FTs) have a substantial impact on the engineering qualities of stabilised soils. The mechanical characteristics and microstructure of lime (Ca(OH)2) fly ash (FA) stabilised sali...

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Main Authors: Sining Li, Yong Huang, Qiushuang Cui, Ruyun Bai, Huan Li, Liran Jiao
Format: Article
Language:English
Published: Nature Portfolio 2025-05-01
Series:Scientific Reports
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Online Access:https://doi.org/10.1038/s41598-025-00307-9
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author Sining Li
Yong Huang
Qiushuang Cui
Ruyun Bai
Huan Li
Liran Jiao
author_facet Sining Li
Yong Huang
Qiushuang Cui
Ruyun Bai
Huan Li
Liran Jiao
author_sort Sining Li
collection DOAJ
description Abstract Geopolymers have long been used to stabilise unique soils, and the stabilising conditions and freeze–thaw cycles (FTs) have a substantial impact on the engineering qualities of stabilised soils. The mechanical characteristics and microstructure of lime (Ca(OH)2) fly ash (FA) stabilised saline soils were investigated in this study using the Unconfined Compressive Strength (UCS), Splitting Strength, and Residual Strength (IR) tests in conjunction with X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Fourier Transform Infrared Spectroscopy (FTIR), and Thermogravimetry (TG). The results indicated that the mechanical properties were optimal at 3% Ca(OH)2 with constant 13% FA content and stabilised soils with UCS and splitting strength of 8.78 MPa and 1.43 MPa, respectively. The stabilised soils strength showed a trend of rapid decrease and then stabilisation with increasing FTs, and frost resistance was optimal at 3% Ca(OH)2. At FTs = 20, the UCS and splitting strength IR were 40.94% and 32.51%, respectively, which were higher than those of other proportions of stabilised soils. This was attributed to the fact that calcium assisted FA stabilisation was primarily attributed to the formation of dense network structure of hydrated calcium silicate and hydrated calcium aluminate gels, as well as the generation of ettringite with sulphate.
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spelling doaj-art-4eb4fc737cd44f36a16249a64a017c8a2025-08-20T03:09:34ZengNature PortfolioScientific Reports2045-23222025-05-0115111410.1038/s41598-025-00307-9Effect of calcium content on geopolymer consolidation of saline soils in the seasonally frozen zoneSining Li0Yong Huang1Qiushuang Cui2Ruyun Bai3Huan Li4Liran Jiao5State Key Laboratory of Chemistry and Utilization of Carbon Based Energy Resources, College of Chemistry, Xinjiang UniversityState Key Laboratory of Chemistry and Utilization of Carbon Based Energy Resources, College of Chemistry, Xinjiang UniversityState Key Laboratory of Chemistry and Utilization of Carbon Based Energy Resources, College of Chemistry, Xinjiang UniversityState Key Laboratory of Chemistry and Utilization of Carbon Based Energy Resources, College of Chemistry, Xinjiang UniversityState Key Laboratory of Chemistry and Utilization of Carbon Based Energy Resources, College of Chemistry, Xinjiang UniversityState Key Laboratory of Chemistry and Utilization of Carbon Based Energy Resources, College of Chemistry, Xinjiang UniversityAbstract Geopolymers have long been used to stabilise unique soils, and the stabilising conditions and freeze–thaw cycles (FTs) have a substantial impact on the engineering qualities of stabilised soils. The mechanical characteristics and microstructure of lime (Ca(OH)2) fly ash (FA) stabilised saline soils were investigated in this study using the Unconfined Compressive Strength (UCS), Splitting Strength, and Residual Strength (IR) tests in conjunction with X-ray Diffraction (XRD), Scanning Electron Microscopy (SEM), Fourier Transform Infrared Spectroscopy (FTIR), and Thermogravimetry (TG). The results indicated that the mechanical properties were optimal at 3% Ca(OH)2 with constant 13% FA content and stabilised soils with UCS and splitting strength of 8.78 MPa and 1.43 MPa, respectively. The stabilised soils strength showed a trend of rapid decrease and then stabilisation with increasing FTs, and frost resistance was optimal at 3% Ca(OH)2. At FTs = 20, the UCS and splitting strength IR were 40.94% and 32.51%, respectively, which were higher than those of other proportions of stabilised soils. This was attributed to the fact that calcium assisted FA stabilisation was primarily attributed to the formation of dense network structure of hydrated calcium silicate and hydrated calcium aluminate gels, as well as the generation of ettringite with sulphate.https://doi.org/10.1038/s41598-025-00307-9Calcium assisted geopolymerSulphate saline soilsFly ashMechanical propertiesMicrostructure
spellingShingle Sining Li
Yong Huang
Qiushuang Cui
Ruyun Bai
Huan Li
Liran Jiao
Effect of calcium content on geopolymer consolidation of saline soils in the seasonally frozen zone
Scientific Reports
Calcium assisted geopolymer
Sulphate saline soils
Fly ash
Mechanical properties
Microstructure
title Effect of calcium content on geopolymer consolidation of saline soils in the seasonally frozen zone
title_full Effect of calcium content on geopolymer consolidation of saline soils in the seasonally frozen zone
title_fullStr Effect of calcium content on geopolymer consolidation of saline soils in the seasonally frozen zone
title_full_unstemmed Effect of calcium content on geopolymer consolidation of saline soils in the seasonally frozen zone
title_short Effect of calcium content on geopolymer consolidation of saline soils in the seasonally frozen zone
title_sort effect of calcium content on geopolymer consolidation of saline soils in the seasonally frozen zone
topic Calcium assisted geopolymer
Sulphate saline soils
Fly ash
Mechanical properties
Microstructure
url https://doi.org/10.1038/s41598-025-00307-9
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AT qiushuangcui effectofcalciumcontentongeopolymerconsolidationofsalinesoilsintheseasonallyfrozenzone
AT ruyunbai effectofcalciumcontentongeopolymerconsolidationofsalinesoilsintheseasonallyfrozenzone
AT huanli effectofcalciumcontentongeopolymerconsolidationofsalinesoilsintheseasonallyfrozenzone
AT liranjiao effectofcalciumcontentongeopolymerconsolidationofsalinesoilsintheseasonallyfrozenzone