Effect of sintering duration on structure and properties of Ni-Al metal-intermetallic composites produced by SPS

The fabrication of Ni-Al based metal-intermetallic layered (MIL) composites is one of the actively developing directions in the production of materials for aircraft and space industries. Alternating hard intermetallic layers with ductile metal layers provides a unique combination of mechanical prope...

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Main Authors: Tatiana Ogneva, Alexander Anisimov, Ruslan Kuzmin, Andrey Tyurin, Yulia Emurlaeva, Natalya Aleksandrova
Format: Article
Language:English
Published: Ural Federal University 2023-10-01
Series:Chimica Techno Acta
Subjects:
Online Access:https://chimicatechnoacta.ru/article/view/7087
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author Tatiana Ogneva
Alexander Anisimov
Ruslan Kuzmin
Andrey Tyurin
Yulia Emurlaeva
Natalya Aleksandrova
author_facet Tatiana Ogneva
Alexander Anisimov
Ruslan Kuzmin
Andrey Tyurin
Yulia Emurlaeva
Natalya Aleksandrova
author_sort Tatiana Ogneva
collection DOAJ
description The fabrication of Ni-Al based metal-intermetallic layered (MIL) composites is one of the actively developing directions in the production of materials for aircraft and space industries. Alternating hard intermetallic layers with ductile metal layers provides a unique combination of mechanical properties. In this study, metal-intermetallic layered composites consisting of Ni and nickel aluminides were fabricated using spark plasma sintering (SPS) of Ni and Al foils 100 and 25 μm in thickness, respectively. Samples sintered at 1100 °C for 0.5, 3, and 8 min were obtained. The purpose of this study was to fabricate Ni-Al MIL composites with increased strength properties using SPS technique and to investigate the effect of sintering duration on structure and properties. The structure of the samples sintered for 0.5 min consisted of Ni layers and intermetallic layers containing the sublayers with stoichiometric and Ni-rich B2 NiAl, L10 twinned martensite NiAl. The tensile strength of such composites was 485 MPa. The intermetallic layers in the sample sintered for 3 min have more Ni-rich NiAl, martensite NiAl, and Ni3Al phases, which promoted to an increase in tensile strength to 575 MPa. The sample sintered for 8 min consisted of Ni and a solid solution of Al in Ni and showed the highest tensile strength, 610 MPa, due to solid solution hardening in the interlayers. The samples did not break when applying bending load, which is the evidence of the good reliability and durability of the composites.
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spelling doaj-art-4ce78d2e2ed74acfa62ac0a9326babc02025-08-20T02:38:38ZengUral Federal UniversityChimica Techno Acta2411-14142023-10-0110310.15826/chimtech.2023.10.3.145028Effect of sintering duration on structure and properties of Ni-Al metal-intermetallic composites produced by SPSTatiana Ogneva0Alexander Anisimov1Ruslan Kuzmin2Andrey Tyurin3Yulia Emurlaeva4Natalya Aleksandrova5Novosibirsk State Technical UniversityLavrent’ev Institute of HydrodynamicsNovosibirsk State Technical UniversityNovosibirsk State Technical UniversityNovosibirsk State Technical UniversityNovosibirsk State Technical UniversityThe fabrication of Ni-Al based metal-intermetallic layered (MIL) composites is one of the actively developing directions in the production of materials for aircraft and space industries. Alternating hard intermetallic layers with ductile metal layers provides a unique combination of mechanical properties. In this study, metal-intermetallic layered composites consisting of Ni and nickel aluminides were fabricated using spark plasma sintering (SPS) of Ni and Al foils 100 and 25 μm in thickness, respectively. Samples sintered at 1100 °C for 0.5, 3, and 8 min were obtained. The purpose of this study was to fabricate Ni-Al MIL composites with increased strength properties using SPS technique and to investigate the effect of sintering duration on structure and properties. The structure of the samples sintered for 0.5 min consisted of Ni layers and intermetallic layers containing the sublayers with stoichiometric and Ni-rich B2 NiAl, L10 twinned martensite NiAl. The tensile strength of such composites was 485 MPa. The intermetallic layers in the sample sintered for 3 min have more Ni-rich NiAl, martensite NiAl, and Ni3Al phases, which promoted to an increase in tensile strength to 575 MPa. The sample sintered for 8 min consisted of Ni and a solid solution of Al in Ni and showed the highest tensile strength, 610 MPa, due to solid solution hardening in the interlayers. The samples did not break when applying bending load, which is the evidence of the good reliability and durability of the composites.https://chimicatechnoacta.ru/article/view/7087spark plasma sinteringstructurepropertiesnickel aluminidelaminated compositesxrdedx
spellingShingle Tatiana Ogneva
Alexander Anisimov
Ruslan Kuzmin
Andrey Tyurin
Yulia Emurlaeva
Natalya Aleksandrova
Effect of sintering duration on structure and properties of Ni-Al metal-intermetallic composites produced by SPS
Chimica Techno Acta
spark plasma sintering
structure
properties
nickel aluminide
laminated composites
xrd
edx
title Effect of sintering duration on structure and properties of Ni-Al metal-intermetallic composites produced by SPS
title_full Effect of sintering duration on structure and properties of Ni-Al metal-intermetallic composites produced by SPS
title_fullStr Effect of sintering duration on structure and properties of Ni-Al metal-intermetallic composites produced by SPS
title_full_unstemmed Effect of sintering duration on structure and properties of Ni-Al metal-intermetallic composites produced by SPS
title_short Effect of sintering duration on structure and properties of Ni-Al metal-intermetallic composites produced by SPS
title_sort effect of sintering duration on structure and properties of ni al metal intermetallic composites produced by sps
topic spark plasma sintering
structure
properties
nickel aluminide
laminated composites
xrd
edx
url https://chimicatechnoacta.ru/article/view/7087
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AT ruslankuzmin effectofsinteringdurationonstructureandpropertiesofnialmetalintermetalliccompositesproducedbysps
AT andreytyurin effectofsinteringdurationonstructureandpropertiesofnialmetalintermetalliccompositesproducedbysps
AT yuliaemurlaeva effectofsinteringdurationonstructureandpropertiesofnialmetalintermetalliccompositesproducedbysps
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