Sustainable development of bioepoxy composites reinforced with recycled rigid polyurethane foam for mechanical, thermal, acoustic, and electromagnetic applications in a circular economy approach

Abstract The accumulation of polyurethane (PU) waste presents a critical environmental challenge due to the inefficiencies of traditional disposal methods like landfilling and incineration. This study introduces a sustainable approach by repurposing 99.89% pure rigid polyurethane foam granules (~ 15...

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Main Authors: Vinoth Kumar Selvaraj, Jeyanthi Subramanian, S. Mouleswaran, T. R. Keshav Keerthan, Thangapandi Muneeswaran, A. Kishore Nath, M. Padmanabha Raju
Format: Article
Language:English
Published: Nature Portfolio 2025-03-01
Series:Scientific Reports
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Online Access:https://doi.org/10.1038/s41598-025-91273-9
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author Vinoth Kumar Selvaraj
Jeyanthi Subramanian
S. Mouleswaran
T. R. Keshav Keerthan
Thangapandi Muneeswaran
A. Kishore Nath
M. Padmanabha Raju
author_facet Vinoth Kumar Selvaraj
Jeyanthi Subramanian
S. Mouleswaran
T. R. Keshav Keerthan
Thangapandi Muneeswaran
A. Kishore Nath
M. Padmanabha Raju
author_sort Vinoth Kumar Selvaraj
collection DOAJ
description Abstract The accumulation of polyurethane (PU) waste presents a critical environmental challenge due to the inefficiencies of traditional disposal methods like landfilling and incineration. This study introduces a sustainable approach by repurposing 99.89% pure rigid polyurethane foam granules (~ 150 µm) as fillers (5 wt.%) in bio-epoxy composites, complemented with 99.89% pure vermiculite particles (~ 10 µm) at varying concentrations (2–10 wt.%). Comprehensive characterization techniques, including high-resolution scanning electron microscopy (HR-SEM) and Fourier transform infrared spectroscopy (FTIR), were employed to evaluate the composites’ mechanical, thermal, electrical, acoustic, and electromagnetic interference (EMI) shielding properties. The study specifically measured EMI shielding effectiveness in the frequency range of 8–12 GHz. Among the formulations, sample S5 exhibited superior mechanical performance, with tensile strength (10.47 N/mm2), impact strength (0.006 kJ/cm2), and flexural strength (46.80 N/mm2). EMI analysis revealed a dielectric constant of 1.111 and shielding effectiveness of -35.24 dB, while sample S3 achieved optimal acoustic absorption (NRC 0.295). Thermal assessments showed the lowest thermal conductivity (0.141 W/mK) and a reduced burning rate (6.8 mm/min) for S5. These results highlight the viability of recycled PU foam-based composites in minimizing plastic waste and advancing net-zero carbon emission goals. Potential applications include battery enclosures, engine bay insulation, and cabin soundproofing in electric vehicles. This work establishes the novelty of integrating recycled materials into bio-epoxy matrices to address environmental challenges and create high-performance composites.
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spelling doaj-art-4cb5e0d2a17e44679b875fadf8f39b642025-08-20T02:56:15ZengNature PortfolioScientific Reports2045-23222025-03-0115111910.1038/s41598-025-91273-9Sustainable development of bioepoxy composites reinforced with recycled rigid polyurethane foam for mechanical, thermal, acoustic, and electromagnetic applications in a circular economy approachVinoth Kumar Selvaraj0Jeyanthi Subramanian1S. Mouleswaran2T. R. Keshav Keerthan3Thangapandi Muneeswaran4A. Kishore Nath5M. Padmanabha Raju6School of Mechanical Engineering, Vellore Institute of TechnologySchool of Mechanical Engineering, Vellore Institute of TechnologySchool of Mechanical Engineering, Vellore Institute of TechnologySchool of Mechanical Engineering, Vellore Institute of TechnologySedaxis Advanced Materials Pvt Ltd.Advanced System Laboratory, Defence Research & Development OrganisationAdvanced System Laboratory, Defence Research & Development OrganisationAbstract The accumulation of polyurethane (PU) waste presents a critical environmental challenge due to the inefficiencies of traditional disposal methods like landfilling and incineration. This study introduces a sustainable approach by repurposing 99.89% pure rigid polyurethane foam granules (~ 150 µm) as fillers (5 wt.%) in bio-epoxy composites, complemented with 99.89% pure vermiculite particles (~ 10 µm) at varying concentrations (2–10 wt.%). Comprehensive characterization techniques, including high-resolution scanning electron microscopy (HR-SEM) and Fourier transform infrared spectroscopy (FTIR), were employed to evaluate the composites’ mechanical, thermal, electrical, acoustic, and electromagnetic interference (EMI) shielding properties. The study specifically measured EMI shielding effectiveness in the frequency range of 8–12 GHz. Among the formulations, sample S5 exhibited superior mechanical performance, with tensile strength (10.47 N/mm2), impact strength (0.006 kJ/cm2), and flexural strength (46.80 N/mm2). EMI analysis revealed a dielectric constant of 1.111 and shielding effectiveness of -35.24 dB, while sample S3 achieved optimal acoustic absorption (NRC 0.295). Thermal assessments showed the lowest thermal conductivity (0.141 W/mK) and a reduced burning rate (6.8 mm/min) for S5. These results highlight the viability of recycled PU foam-based composites in minimizing plastic waste and advancing net-zero carbon emission goals. Potential applications include battery enclosures, engine bay insulation, and cabin soundproofing in electric vehicles. This work establishes the novelty of integrating recycled materials into bio-epoxy matrices to address environmental challenges and create high-performance composites.https://doi.org/10.1038/s41598-025-91273-9RecyclingSustainable compositesBio-epoxyNet-zero carbon emissionHR-SEMFTIR, TGA
spellingShingle Vinoth Kumar Selvaraj
Jeyanthi Subramanian
S. Mouleswaran
T. R. Keshav Keerthan
Thangapandi Muneeswaran
A. Kishore Nath
M. Padmanabha Raju
Sustainable development of bioepoxy composites reinforced with recycled rigid polyurethane foam for mechanical, thermal, acoustic, and electromagnetic applications in a circular economy approach
Scientific Reports
Recycling
Sustainable composites
Bio-epoxy
Net-zero carbon emission
HR-SEM
FTIR, TGA
title Sustainable development of bioepoxy composites reinforced with recycled rigid polyurethane foam for mechanical, thermal, acoustic, and electromagnetic applications in a circular economy approach
title_full Sustainable development of bioepoxy composites reinforced with recycled rigid polyurethane foam for mechanical, thermal, acoustic, and electromagnetic applications in a circular economy approach
title_fullStr Sustainable development of bioepoxy composites reinforced with recycled rigid polyurethane foam for mechanical, thermal, acoustic, and electromagnetic applications in a circular economy approach
title_full_unstemmed Sustainable development of bioepoxy composites reinforced with recycled rigid polyurethane foam for mechanical, thermal, acoustic, and electromagnetic applications in a circular economy approach
title_short Sustainable development of bioepoxy composites reinforced with recycled rigid polyurethane foam for mechanical, thermal, acoustic, and electromagnetic applications in a circular economy approach
title_sort sustainable development of bioepoxy composites reinforced with recycled rigid polyurethane foam for mechanical thermal acoustic and electromagnetic applications in a circular economy approach
topic Recycling
Sustainable composites
Bio-epoxy
Net-zero carbon emission
HR-SEM
FTIR, TGA
url https://doi.org/10.1038/s41598-025-91273-9
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