Microhotplate as a Platform for Calorimetry
Calorimetry is a powerful method for characterising materials. The heat of a reaction can be directly measured with good accuracy. The established method usually requires large amounts of materials, which is a major drawback when studying thin film reactions. A MEMS microhotplate-based microcalorime...
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| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
| Published: |
MDPI AG
2024-04-01
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| Series: | Proceedings |
| Subjects: | |
| Online Access: | https://www.mdpi.com/2504-3900/97/1/175 |
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| Summary: | Calorimetry is a powerful method for characterising materials. The heat of a reaction can be directly measured with good accuracy. The established method usually requires large amounts of materials, which is a major drawback when studying thin film reactions. A MEMS microhotplate-based microcalorimeter is developed in this study; it allows us to investigate thin film reactions by using a very small amount of materials. The temperature scale is calibrated by a well-known heat method of melting of two metal films. Energy calibration is also solved, and thus real information can be extracted for various solid-phase thin film reactions. In order to study reactions taking place close to room temperature, a cooled sample holder is developed, and the measurements can be started well below 0 °C. |
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| ISSN: | 2504-3900 |