Physico-chemical characterization of Al2O3/Ti6A4V type thermal barrier systems

Al2O3 alumina deposits were deposited on Ti6A4V titanium alloy substrates by rf-PVD at different substrate polarizations 0V, -50V, -100V and without polarization (wp). SEM images, at the surface of the deposits, showed a very good substrate coverage with a dense morphology. Quantitative EDS analysis...

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Main Authors: Djamel Amari, Khaoula Rahmouni, Nadia Saoula, Hafit Khireddine, Youcef Khelfaoui
Format: Article
Language:English
Published: Renewable Energy Development Center (CDER) 2025-02-01
Series:Revue des Énergies Renouvelables
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Online Access:https://revue.cder.dz/index.php/rer/article/view/1345
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author Djamel Amari
Khaoula Rahmouni
Nadia Saoula
Hafit Khireddine
Youcef Khelfaoui
author_facet Djamel Amari
Khaoula Rahmouni
Nadia Saoula
Hafit Khireddine
Youcef Khelfaoui
author_sort Djamel Amari
collection DOAJ
description Al2O3 alumina deposits were deposited on Ti6A4V titanium alloy substrates by rf-PVD at different substrate polarizations 0V, -50V, -100V and without polarization (wp). SEM images, at the surface of the deposits, showed a very good substrate coverage with a dense morphology. Quantitative EDS analysis of these deposits revealed the presence of the elements Al and O in these deposits. The mass percentage of these elements, at different polarizations of the substrate, varies between 51.72% and 56.19% for Al and between 43.80% and 48.27% for O. The images, revealed by AFM, showed well-spread deposits on the surface of the substrates with relatively uniform grooves. The values of the arithmetic roughness Ra, ranging from 3.45 to 4.75 nm, testify to the low crystallinity of these deposits and an appreciable density. The DRX of these deposits in mode showed a weak crystallization of the Al2O3 phase and characteristic peaks of the partially crystallized phases Al0.3Ti1.7, and Ti0.7V0.3, resulting from the interaction of the elements of the Ti6A4V substrate and those of the Al2O3 deposit.
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institution Kabale University
issn 1112-2242
2716-8247
language English
publishDate 2025-02-01
publisher Renewable Energy Development Center (CDER)
record_format Article
series Revue des Énergies Renouvelables
spelling doaj-art-4c2738adb0754d70864b967ed00cabfe2025-08-20T03:28:58ZengRenewable Energy Development Center (CDER)Revue des Énergies Renouvelables1112-22422716-82472025-02-0131510.54966/jreen.v28i1.13451345Physico-chemical characterization of Al2O3/Ti6A4V type thermal barrier systemsDjamel Amari0Khaoula Rahmouni1Nadia Saoula2Hafit Khireddine3Youcef Khelfaoui4Laboratoire de génie de l’environnement (LGE), Université de Bejaia, route de Targa Ouzamour, Bejaia, Algérielaboratoire des matériaux et composantes actives (LMCA), Institut des sciences et technologies appliquées (ISTA), Université de Oum El Bouaghi, 04000, AlgérieCentre de Développement des Technologies Avancées (CDTA), Cité, 20 Août 1956, Baba Hassen, Alger, AlgérieLaboratoire de génie de l’environnement (LGE), Université de Bejaia, route de Targa Ouzamour, Bejaia, AlgérieLaboratoire de mécanique, matériaux et énergétique (L2ME), Université de Bejaia, route de Targa Ouzamour, Bejaia, AlgérieAl2O3 alumina deposits were deposited on Ti6A4V titanium alloy substrates by rf-PVD at different substrate polarizations 0V, -50V, -100V and without polarization (wp). SEM images, at the surface of the deposits, showed a very good substrate coverage with a dense morphology. Quantitative EDS analysis of these deposits revealed the presence of the elements Al and O in these deposits. The mass percentage of these elements, at different polarizations of the substrate, varies between 51.72% and 56.19% for Al and between 43.80% and 48.27% for O. The images, revealed by AFM, showed well-spread deposits on the surface of the substrates with relatively uniform grooves. The values of the arithmetic roughness Ra, ranging from 3.45 to 4.75 nm, testify to the low crystallinity of these deposits and an appreciable density. The DRX of these deposits in mode showed a weak crystallization of the Al2O3 phase and characteristic peaks of the partially crystallized phases Al0.3Ti1.7, and Ti0.7V0.3, resulting from the interaction of the elements of the Ti6A4V substrate and those of the Al2O3 deposit.https://revue.cder.dz/index.php/rer/article/view/1345al2o3ti6a4vdepositsrugositécristallisationpolarisation
spellingShingle Djamel Amari
Khaoula Rahmouni
Nadia Saoula
Hafit Khireddine
Youcef Khelfaoui
Physico-chemical characterization of Al2O3/Ti6A4V type thermal barrier systems
Revue des Énergies Renouvelables
al2o3
ti6a4v
deposits
rugosité
cristallisation
polarisation
title Physico-chemical characterization of Al2O3/Ti6A4V type thermal barrier systems
title_full Physico-chemical characterization of Al2O3/Ti6A4V type thermal barrier systems
title_fullStr Physico-chemical characterization of Al2O3/Ti6A4V type thermal barrier systems
title_full_unstemmed Physico-chemical characterization of Al2O3/Ti6A4V type thermal barrier systems
title_short Physico-chemical characterization of Al2O3/Ti6A4V type thermal barrier systems
title_sort physico chemical characterization of al2o3 ti6a4v type thermal barrier systems
topic al2o3
ti6a4v
deposits
rugosité
cristallisation
polarisation
url https://revue.cder.dz/index.php/rer/article/view/1345
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AT nadiasaoula physicochemicalcharacterizationofal2o3ti6a4vtypethermalbarriersystems
AT hafitkhireddine physicochemicalcharacterizationofal2o3ti6a4vtypethermalbarriersystems
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