Investigation of the Tribological Effects of Nano-Sized Transition Metal Oxides on a Base Oil Containing Pour Point Depressant and Viscosity Modifier

This study investigates the tribological effects of nano-sized metal oxides (ZrO<sub>2</sub>, CuO, Y<sub>2</sub>O<sub>3</sub> and TiO<sub>2</sub>) in Group III type base oil containing 0.3% pour point depressant (PPD) and 5% viscosity modifier (VM) to...

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Main Authors: Ádám István Szabó, Kevin Szabó, Hajnalka Hargitai
Format: Article
Language:English
Published: MDPI AG 2024-12-01
Series:ChemEngineering
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Online Access:https://www.mdpi.com/2305-7084/9/1/1
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author Ádám István Szabó
Kevin Szabó
Hajnalka Hargitai
author_facet Ádám István Szabó
Kevin Szabó
Hajnalka Hargitai
author_sort Ádám István Szabó
collection DOAJ
description This study investigates the tribological effects of nano-sized metal oxides (ZrO<sub>2</sub>, CuO, Y<sub>2</sub>O<sub>3</sub> and TiO<sub>2</sub>) in Group III type base oil containing 0.3% pour point depressant (PPD) and 5% viscosity modifier (VM) to enhance friction and wear performance. The homogenized lubricant samples with varying concentrations of oxide nanoparticles (0.1–0.5 wt%) on a linear oscillating tribometer performed static and dynamic frictional tests. Optical and confocal microscopy surface analysis evaluated the wear of the specimen, and SEM and EDX analyses characterized the wear tracks, nanoparticle distributions, and quantification. The cooperation between PPD and nanoparticles significantly improved friction and wear values; however, the worn surface suffered extensively from fatigue wear. The collaboration between VM and nanoparticles resulted in a nanoparticle-rich tribofilm on the contact surface, providing excellent wear resistance that protects the component while also favorably impacting friction reduction. This study found CuO reduced wear volume by 85% with PPD and 43% with VM at 0.5 wt%, while ZrO<sub>2</sub> achieved 80% and 63% reductions, respectively. Y<sub>2</sub>O<sub>3</sub> reduced wear volume by 82% with PPD, and TiO<sub>2</sub> reduced friction by 20% with VM. These nanoparticles enhanced tribological performance at optimal concentrations, but high concentrations caused tribofilm instability, highlighting the need for precise optimization.
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spelling doaj-art-49bef6b0c329485ba2a99cb3b0dc74802025-08-20T02:44:38ZengMDPI AGChemEngineering2305-70842024-12-0191110.3390/chemengineering9010001Investigation of the Tribological Effects of Nano-Sized Transition Metal Oxides on a Base Oil Containing Pour Point Depressant and Viscosity ModifierÁdám István Szabó0Kevin Szabó1Hajnalka Hargitai2Department of Propulsion Technology, Széchenyi István University, Egyetem tér 1, H-9026 Győr, HungaryDepartment of Propulsion Technology, Széchenyi István University, Egyetem tér 1, H-9026 Győr, HungaryDepartment of Materials Science and Technology, Széchenyi István University, Egyetem tér 1, H-9026 Győr, HungaryThis study investigates the tribological effects of nano-sized metal oxides (ZrO<sub>2</sub>, CuO, Y<sub>2</sub>O<sub>3</sub> and TiO<sub>2</sub>) in Group III type base oil containing 0.3% pour point depressant (PPD) and 5% viscosity modifier (VM) to enhance friction and wear performance. The homogenized lubricant samples with varying concentrations of oxide nanoparticles (0.1–0.5 wt%) on a linear oscillating tribometer performed static and dynamic frictional tests. Optical and confocal microscopy surface analysis evaluated the wear of the specimen, and SEM and EDX analyses characterized the wear tracks, nanoparticle distributions, and quantification. The cooperation between PPD and nanoparticles significantly improved friction and wear values; however, the worn surface suffered extensively from fatigue wear. The collaboration between VM and nanoparticles resulted in a nanoparticle-rich tribofilm on the contact surface, providing excellent wear resistance that protects the component while also favorably impacting friction reduction. This study found CuO reduced wear volume by 85% with PPD and 43% with VM at 0.5 wt%, while ZrO<sub>2</sub> achieved 80% and 63% reductions, respectively. Y<sub>2</sub>O<sub>3</sub> reduced wear volume by 82% with PPD, and TiO<sub>2</sub> reduced friction by 20% with VM. These nanoparticles enhanced tribological performance at optimal concentrations, but high concentrations caused tribofilm instability, highlighting the need for precise optimization.https://www.mdpi.com/2305-7084/9/1/1lubricantsnanoadditivesviscosity modifierpour point depressantfriction
spellingShingle Ádám István Szabó
Kevin Szabó
Hajnalka Hargitai
Investigation of the Tribological Effects of Nano-Sized Transition Metal Oxides on a Base Oil Containing Pour Point Depressant and Viscosity Modifier
ChemEngineering
lubricants
nanoadditives
viscosity modifier
pour point depressant
friction
title Investigation of the Tribological Effects of Nano-Sized Transition Metal Oxides on a Base Oil Containing Pour Point Depressant and Viscosity Modifier
title_full Investigation of the Tribological Effects of Nano-Sized Transition Metal Oxides on a Base Oil Containing Pour Point Depressant and Viscosity Modifier
title_fullStr Investigation of the Tribological Effects of Nano-Sized Transition Metal Oxides on a Base Oil Containing Pour Point Depressant and Viscosity Modifier
title_full_unstemmed Investigation of the Tribological Effects of Nano-Sized Transition Metal Oxides on a Base Oil Containing Pour Point Depressant and Viscosity Modifier
title_short Investigation of the Tribological Effects of Nano-Sized Transition Metal Oxides on a Base Oil Containing Pour Point Depressant and Viscosity Modifier
title_sort investigation of the tribological effects of nano sized transition metal oxides on a base oil containing pour point depressant and viscosity modifier
topic lubricants
nanoadditives
viscosity modifier
pour point depressant
friction
url https://www.mdpi.com/2305-7084/9/1/1
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