Efficient Removal of Ciprofloxacin from Water Using High-Surface-Area Activated Carbon Derived from Rice Husks: Adsorption Isotherms, Kinetics, and Thermodynamic Evaluation

Activated carbon is widely recognized as an effective material for removing pollutants, especially pharmaceutical residues, from water. In this study, high-surface-area activated carbon derived from rice husks (RHAC) was synthesized via KOH activation and used for the adsorption of ciprofloxacin, a...

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Main Authors: Esra Demirdağ, Mehmet Ferit Demirel, Veysel Benek, Elif Doğru, Yunus Önal, Mehmet Hüseyin Alkan, Kadir Erol, İhsan Alacabey
Format: Article
Language:English
Published: MDPI AG 2025-06-01
Series:Molecules
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Online Access:https://www.mdpi.com/1420-3049/30/12/2501
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Summary:Activated carbon is widely recognized as an effective material for removing pollutants, especially pharmaceutical residues, from water. In this study, high-surface-area activated carbon derived from rice husks (RHAC) was synthesized via KOH activation and used for the adsorption of ciprofloxacin, a widely used fluoroquinolone antibiotic. Its adsorption behavior was systematically investigated through batch experiments varying the pH, adsorbent dosage, contact time, initial concentration, and temperature. The RHAC exhibited a high surface area of 1539.7 m<sup>2</sup>/g and achieved a maximum adsorption capacity of 398.4 mg·g<sup>−1</sup>. The Freundlich isotherm best describes its adsorption equilibrium, suggesting multilayer adsorption on a heterogeneous surface. Kinetic modeling revealed that the adsorption process followed a pseudo second-order model (R<sup>2</sup> = 0.9981), indicating chemisorption as the rate-limiting mechanism. Thermodynamic parameters (ΔH° = 6.61 kJ/mol, ΔG° < 0) confirmed that the process was endothermic and spontaneous. These findings demonstrate that RHAC is a highly efficient, low-cost, and sustainable adsorbent for removing ciprofloxacin from aqueous environments.
ISSN:1420-3049