Quantifying per- and polyfluoroalkyl substances (PFAS) in air emissions: Lab & field experiences from a hazardous waste incinerator

Per- and polyfluoroalkyl substances (PFAS) are ubiquitous in our environment and food chains but standardized monitoring methods are still lacking for the air compartment. This work presents methodological developments and validation experiments which led to a new compendium method (LUC) for the qua...

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Main Authors: Jelle Hofman, Griet Jacobs, Bart Baeyens, Aline Reis De Carvalho, Wim Aerts, Stefan Voorspoels, Gill Van den Bergh, Masha Van Deun, Patrick Berghmans, Andres Van Brecht, Gert Otten
Format: Article
Language:English
Published: Elsevier 2025-06-01
Series:Environment International
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Online Access:http://www.sciencedirect.com/science/article/pii/S0160412025002922
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author Jelle Hofman
Griet Jacobs
Bart Baeyens
Aline Reis De Carvalho
Wim Aerts
Stefan Voorspoels
Gill Van den Bergh
Masha Van Deun
Patrick Berghmans
Andres Van Brecht
Gert Otten
author_facet Jelle Hofman
Griet Jacobs
Bart Baeyens
Aline Reis De Carvalho
Wim Aerts
Stefan Voorspoels
Gill Van den Bergh
Masha Van Deun
Patrick Berghmans
Andres Van Brecht
Gert Otten
author_sort Jelle Hofman
collection DOAJ
description Per- and polyfluoroalkyl substances (PFAS) are ubiquitous in our environment and food chains but standardized monitoring methods are still lacking for the air compartment. This work presents methodological developments and validation experiments which led to a new compendium method (LUC) for the quantification of PFAS in air emissions. From 2021 onwards, relevant experience with the proposed OTM-45 method (EPA, 2021) was obtained through dedicated laboratory experiments and 15 repeated stack measurements at a hazardous waste-to-energy (WtE) plant. We optimized the sampling, extraction and analytical procedure and performed different lab and field validation exercises, resulting in the first available regulatory method for the detection and quantification of PFAS in air emissions (LUC/VI/003). This method turned into force in Flanders since January 15th, 2024, and is meanwhile applied on various stacks and industries to collect evidence on prevailing concentration levels, compositional fingerprints and impact evaluation from gas abatement technologies. We stress the need for harmonization of both PFAS sampling and analytical procedures in order to guarantee comparability of PFAS emission results. This methodological evidence paves the way for more standardized emission monitoring, more stringent environmental standards and improved public health protection.
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spelling doaj-art-4933be60d2a84292b57428bfd2cddedb2025-08-20T02:32:30ZengElsevierEnvironment International0160-41202025-06-0120010954110.1016/j.envint.2025.109541Quantifying per- and polyfluoroalkyl substances (PFAS) in air emissions: Lab & field experiences from a hazardous waste incineratorJelle Hofman0Griet Jacobs1Bart Baeyens2Aline Reis De Carvalho3Wim Aerts4Stefan Voorspoels5Gill Van den Bergh6Masha Van Deun7Patrick Berghmans8Andres Van Brecht9Gert Otten10VITO, Air Quality Management Systems (AQMS), Flemish Institute for Technological Research (VITO), Boeretang 200, 2400 Mol, Belgium; Corresponding author.VITO GOAL, Flemish Institute for Technological Research (VITO), Boeretang 200, 2400 Mol, BelgiumVITO, Air Quality Management Systems (AQMS), Flemish Institute for Technological Research (VITO), Boeretang 200, 2400 Mol, BelgiumVITO GOAL, Flemish Institute for Technological Research (VITO), Boeretang 200, 2400 Mol, BelgiumVITO, Air Quality Management Systems (AQMS), Flemish Institute for Technological Research (VITO), Boeretang 200, 2400 Mol, BelgiumVITO GOAL, Flemish Institute for Technological Research (VITO), Boeretang 200, 2400 Mol, BelgiumVITO GOAL, Flemish Institute for Technological Research (VITO), Boeretang 200, 2400 Mol, BelgiumVITO GOAL, Flemish Institute for Technological Research (VITO), Boeretang 200, 2400 Mol, BelgiumVITO, Air Quality Management Systems (AQMS), Flemish Institute for Technological Research (VITO), Boeretang 200, 2400 Mol, BelgiumIndaver Belgium nv, 2800 Mechelen, BelgiumVITO, Air Quality Management Systems (AQMS), Flemish Institute for Technological Research (VITO), Boeretang 200, 2400 Mol, BelgiumPer- and polyfluoroalkyl substances (PFAS) are ubiquitous in our environment and food chains but standardized monitoring methods are still lacking for the air compartment. This work presents methodological developments and validation experiments which led to a new compendium method (LUC) for the quantification of PFAS in air emissions. From 2021 onwards, relevant experience with the proposed OTM-45 method (EPA, 2021) was obtained through dedicated laboratory experiments and 15 repeated stack measurements at a hazardous waste-to-energy (WtE) plant. We optimized the sampling, extraction and analytical procedure and performed different lab and field validation exercises, resulting in the first available regulatory method for the detection and quantification of PFAS in air emissions (LUC/VI/003). This method turned into force in Flanders since January 15th, 2024, and is meanwhile applied on various stacks and industries to collect evidence on prevailing concentration levels, compositional fingerprints and impact evaluation from gas abatement technologies. We stress the need for harmonization of both PFAS sampling and analytical procedures in order to guarantee comparability of PFAS emission results. This methodological evidence paves the way for more standardized emission monitoring, more stringent environmental standards and improved public health protection.http://www.sciencedirect.com/science/article/pii/S0160412025002922Emerging contaminantsEmissionMonitoringValidationChimneyDestruction
spellingShingle Jelle Hofman
Griet Jacobs
Bart Baeyens
Aline Reis De Carvalho
Wim Aerts
Stefan Voorspoels
Gill Van den Bergh
Masha Van Deun
Patrick Berghmans
Andres Van Brecht
Gert Otten
Quantifying per- and polyfluoroalkyl substances (PFAS) in air emissions: Lab & field experiences from a hazardous waste incinerator
Environment International
Emerging contaminants
Emission
Monitoring
Validation
Chimney
Destruction
title Quantifying per- and polyfluoroalkyl substances (PFAS) in air emissions: Lab & field experiences from a hazardous waste incinerator
title_full Quantifying per- and polyfluoroalkyl substances (PFAS) in air emissions: Lab & field experiences from a hazardous waste incinerator
title_fullStr Quantifying per- and polyfluoroalkyl substances (PFAS) in air emissions: Lab & field experiences from a hazardous waste incinerator
title_full_unstemmed Quantifying per- and polyfluoroalkyl substances (PFAS) in air emissions: Lab & field experiences from a hazardous waste incinerator
title_short Quantifying per- and polyfluoroalkyl substances (PFAS) in air emissions: Lab & field experiences from a hazardous waste incinerator
title_sort quantifying per and polyfluoroalkyl substances pfas in air emissions lab amp field experiences from a hazardous waste incinerator
topic Emerging contaminants
Emission
Monitoring
Validation
Chimney
Destruction
url http://www.sciencedirect.com/science/article/pii/S0160412025002922
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