Speciation of uranium and radionuclides in the bottom sediments of premises 001/3 of the "Shelter" object

The results of experimental determination of the forms of uranium and radionuclides 90Sr, 137Cs, 154Eu, 238Pu, 239+240Pu, 241Am, and 244Cm in the bottom sediments of the premises 001/3 of the "Shelter" object are presented. By the sequential extraction procedure, the following amounts are...

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Main Authors: O. O. Odintsov, L. A. Palamar, L. B. Chikur
Format: Article
Language:English
Published: Institute for Nuclear Research, National Academy of Sciences of Ukraine 2021-12-01
Series:Ядерна фізика та енергетика
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Online Access:http://jnpae.kinr.kiev.ua/22.4/html/22.4.0365.html
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author O. O. Odintsov
L. A. Palamar
L. B. Chikur
author_facet O. O. Odintsov
L. A. Palamar
L. B. Chikur
author_sort O. O. Odintsov
collection DOAJ
description The results of experimental determination of the forms of uranium and radionuclides 90Sr, 137Cs, 154Eu, 238Pu, 239+240Pu, 241Am, and 244Cm in the bottom sediments of the premises 001/3 of the "Shelter" object are presented. By the sequential extraction procedure, the following amounts are determined: water-soluble, exchange, carbonate, and acid-soluble forms of uranium, fission products (90Sr, 137Cs, 154Eu), and transuranium elements (238Pu, 239+240Pu, 241Am, 244Cm) in the bottom sediments in the premises 001/3 on a mark of -2.60 m of auxiliary systems of the reactor compartment of the "Shelter" object. The concentration of uranium in the bottom sediments of room 001/3 is 3.1 ± 0.5 g/kg. Specific activity of 90Sr, 137Cs in the bottom sediments is within the range of 6·108 - 1·109 Bq/kg, and 239+240Pu and 241Am within the range of 6·105 - 8·106 Bq/kg. Radionuclides 90Sr, 137Cs, 154Eu, 238Pu, 239+240Pu, 241Am, 244Сm in the bottom sediments are in different chemical forms that will define their different potential mobility. Uranium and 137Cs in the bottom sediments of premises 001/3 mainly are in exchange forms. The amount of water-soluble forms of uranium and cesium is 1.5 - 3 %. The basic amount of 90Sr, more than 60 %, is carbonate soluble in a weak acid at рН 4.8. More than 65 % of 238Pu and 239+240Pu in the bottom sediments are in acid-soluble forms. The mobility of 154Eu, 241Am and 244Cm in the bottom sediments is much higher than that of plutonium; at pH 4.8 more than 40 % of 241Am go to soluble state. The ratio between the activities of 137Cs/90Sr, 90Sr/239+240Pu, 241Am/239+240Pu, and 244Cm/239+240Pu in the bottom sediments considerably differ from the analogical relations of radionuclides in a fuel containing materials of the "Shelter" object.
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spelling doaj-art-466a741ba1104e5ea2c9263f5d48922c2025-08-20T01:56:42ZengInstitute for Nuclear Research, National Academy of Sciences of UkraineЯдерна фізика та енергетика1818-331X2074-05652021-12-01224365374https://doi.org/10.15407/jnpae2021.04.365Speciation of uranium and radionuclides in the bottom sediments of premises 001/3 of the "Shelter" objectO. O. Odintsov0L. A. Palamar1L. B. Chikur2Institute for Safety Problems of Nuclear Power Plants, National Academy of Sciences of Ukraine, Chornobyl, UkraineInstitute for Safety Problems of Nuclear Power Plants, National Academy of Sciences of Ukraine, Chornobyl, UkraineInstitute for Safety Problems of Nuclear Power Plants, National Academy of Sciences of Ukraine, Chornobyl, UkraineThe results of experimental determination of the forms of uranium and radionuclides 90Sr, 137Cs, 154Eu, 238Pu, 239+240Pu, 241Am, and 244Cm in the bottom sediments of the premises 001/3 of the "Shelter" object are presented. By the sequential extraction procedure, the following amounts are determined: water-soluble, exchange, carbonate, and acid-soluble forms of uranium, fission products (90Sr, 137Cs, 154Eu), and transuranium elements (238Pu, 239+240Pu, 241Am, 244Cm) in the bottom sediments in the premises 001/3 on a mark of -2.60 m of auxiliary systems of the reactor compartment of the "Shelter" object. The concentration of uranium in the bottom sediments of room 001/3 is 3.1 ± 0.5 g/kg. Specific activity of 90Sr, 137Cs in the bottom sediments is within the range of 6·108 - 1·109 Bq/kg, and 239+240Pu and 241Am within the range of 6·105 - 8·106 Bq/kg. Radionuclides 90Sr, 137Cs, 154Eu, 238Pu, 239+240Pu, 241Am, 244Сm in the bottom sediments are in different chemical forms that will define their different potential mobility. Uranium and 137Cs in the bottom sediments of premises 001/3 mainly are in exchange forms. The amount of water-soluble forms of uranium and cesium is 1.5 - 3 %. The basic amount of 90Sr, more than 60 %, is carbonate soluble in a weak acid at рН 4.8. More than 65 % of 238Pu and 239+240Pu in the bottom sediments are in acid-soluble forms. The mobility of 154Eu, 241Am and 244Cm in the bottom sediments is much higher than that of plutonium; at pH 4.8 more than 40 % of 241Am go to soluble state. The ratio between the activities of 137Cs/90Sr, 90Sr/239+240Pu, 241Am/239+240Pu, and 244Cm/239+240Pu in the bottom sediments considerably differ from the analogical relations of radionuclides in a fuel containing materials of the "Shelter" object.http://jnpae.kinr.kiev.ua/22.4/html/22.4.0365.htmluranium137cs90srplutoniumamericiumsequential extractionspeciation of radionuclidesbottom sediments"shelter" object.
spellingShingle O. O. Odintsov
L. A. Palamar
L. B. Chikur
Speciation of uranium and radionuclides in the bottom sediments of premises 001/3 of the "Shelter" object
Ядерна фізика та енергетика
uranium
137cs
90sr
plutonium
americium
sequential extraction
speciation of radionuclides
bottom sediments
"shelter" object.
title Speciation of uranium and radionuclides in the bottom sediments of premises 001/3 of the "Shelter" object
title_full Speciation of uranium and radionuclides in the bottom sediments of premises 001/3 of the "Shelter" object
title_fullStr Speciation of uranium and radionuclides in the bottom sediments of premises 001/3 of the "Shelter" object
title_full_unstemmed Speciation of uranium and radionuclides in the bottom sediments of premises 001/3 of the "Shelter" object
title_short Speciation of uranium and radionuclides in the bottom sediments of premises 001/3 of the "Shelter" object
title_sort speciation of uranium and radionuclides in the bottom sediments of premises 001 3 of the shelter object
topic uranium
137cs
90sr
plutonium
americium
sequential extraction
speciation of radionuclides
bottom sediments
"shelter" object.
url http://jnpae.kinr.kiev.ua/22.4/html/22.4.0365.html
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AT lbchikur speciationofuraniumandradionuclidesinthebottomsedimentsofpremises0013oftheshelterobject