Effect of the photoinitiator system on the properties of a dental material based on a hybrid polymer

Objective: In this study, the effects of two different cure protocols upon the properties of composites using a hybrid-polymer as dental resin were evaluated. Material and Methods: Two distinct dental composites were prepared, one containing a mixture of TEGDMA/bis-GMA (50:50) and, another containi...

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Main Authors: Sandro Aurélio de Souza Venter, Gedalias Custódio Martim, Andressa dos Santos, Tiago Roerto Detomini, Eduardo Radovanovic, Emerson Marcelo Girotto
Format: Article
Language:English
Published: Universidade Estadual Paulista 2016-03-01
Series:Brazilian Dental Science
Online Access:https://ojs.ict.unesp.br/index.php/cob/article/view/1233
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author Sandro Aurélio de Souza Venter
Gedalias Custódio Martim
Andressa dos Santos
Tiago Roerto Detomini
Eduardo Radovanovic
Emerson Marcelo Girotto
author_facet Sandro Aurélio de Souza Venter
Gedalias Custódio Martim
Andressa dos Santos
Tiago Roerto Detomini
Eduardo Radovanovic
Emerson Marcelo Girotto
author_sort Sandro Aurélio de Souza Venter
collection DOAJ
description Objective: In this study, the effects of two different cure protocols upon the properties of composites using a hybrid-polymer as dental resin were evaluated. Material and Methods: Two distinct dental composites were prepared, one containing a mixture of TEGDMA/bis-GMA (50:50) and, another containing a mixture of TEGDMA/p-MEMO (50:50), [p-MEMO: oligomeric inorganic precursor]. Both composites were polymerized with lucirin and canphorquinone as photoinitiators. The composites were made with a 70 % wt of inorganic filler. Flexural strength was evaluated with a universal test machine and the degree of conversion was measured by infrared spectroscopy. A helium pycnometer was used to obtain polymer shrinkage data. Sorption tests were performed and SEM microscopy was used to show deleterious effects upon the resins’ surfaces. Results: The sample base on TEGDMA/p-MEMO polymerized with lucirin (L-T/p) showed the best values of the monitored properties. Conclusion: Lucirin is the most suitable photoinitiator for dental composites containing hybrid polymers. Keywords Dental resins; Flexural strength; Hybrid polymer; Photoinitiator system; Polymerization shrinkage.
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series Brazilian Dental Science
spelling doaj-art-4636a32a769d42daa07fabef70a469cb2025-08-22T18:13:22ZengUniversidade Estadual PaulistaBrazilian Dental Science2178-60112016-03-0119110.14295/bds.2016.v19i1.1233Effect of the photoinitiator system on the properties of a dental material based on a hybrid polymerSandro Aurélio de Souza Venter0Gedalias Custódio Martim1Andressa dos Santos2Tiago Roerto Detomini3Eduardo Radovanovic4Emerson Marcelo Girotto5Chemistry Department - UTFPR - Universidade Tecnológica Federal do Paraná, Apucarana - PR, Brasil.Chemistry Department - UEM - Universidade Estadual de Maringá, Maringá - PR, Brasil.Chemistry Department - UEM - Universidade Estadual de Maringá, Maringá - PR, Brasil.Chemistry Department - UEM - Universidade Estadual de Maringá, Maringá - PR, Brasil.Chemistry Department - UEM - Universidade Estadual de Maringá, Maringá - PR, Brasil.Chemistry Department - UEM - Universidade Estadual de Maringá, Maringá - PR, Brasil. Objective: In this study, the effects of two different cure protocols upon the properties of composites using a hybrid-polymer as dental resin were evaluated. Material and Methods: Two distinct dental composites were prepared, one containing a mixture of TEGDMA/bis-GMA (50:50) and, another containing a mixture of TEGDMA/p-MEMO (50:50), [p-MEMO: oligomeric inorganic precursor]. Both composites were polymerized with lucirin and canphorquinone as photoinitiators. The composites were made with a 70 % wt of inorganic filler. Flexural strength was evaluated with a universal test machine and the degree of conversion was measured by infrared spectroscopy. A helium pycnometer was used to obtain polymer shrinkage data. Sorption tests were performed and SEM microscopy was used to show deleterious effects upon the resins’ surfaces. Results: The sample base on TEGDMA/p-MEMO polymerized with lucirin (L-T/p) showed the best values of the monitored properties. Conclusion: Lucirin is the most suitable photoinitiator for dental composites containing hybrid polymers. Keywords Dental resins; Flexural strength; Hybrid polymer; Photoinitiator system; Polymerization shrinkage. https://ojs.ict.unesp.br/index.php/cob/article/view/1233
spellingShingle Sandro Aurélio de Souza Venter
Gedalias Custódio Martim
Andressa dos Santos
Tiago Roerto Detomini
Eduardo Radovanovic
Emerson Marcelo Girotto
Effect of the photoinitiator system on the properties of a dental material based on a hybrid polymer
Brazilian Dental Science
title Effect of the photoinitiator system on the properties of a dental material based on a hybrid polymer
title_full Effect of the photoinitiator system on the properties of a dental material based on a hybrid polymer
title_fullStr Effect of the photoinitiator system on the properties of a dental material based on a hybrid polymer
title_full_unstemmed Effect of the photoinitiator system on the properties of a dental material based on a hybrid polymer
title_short Effect of the photoinitiator system on the properties of a dental material based on a hybrid polymer
title_sort effect of the photoinitiator system on the properties of a dental material based on a hybrid polymer
url https://ojs.ict.unesp.br/index.php/cob/article/view/1233
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