Synthesis and Crystal Structure of N-Dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine
A new compound, N-dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine, was synthesized and characterized. The crystal structure of the title compound (C11H10Cl3NO2, Mr=294.55) has been determined by single-crystal X-ray diffraction. The crystal belongs to monoclinic, space group P21/c, w...
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| Main Authors: | , , , |
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| Format: | Article |
| Language: | English |
| Published: |
Wiley
2015-01-01
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| Series: | Journal of Chemistry |
| Online Access: | http://dx.doi.org/10.1155/2015/268306 |
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| Summary: | A new compound, N-dichloroacetyl-3,4-dihydro-3-methyl-6-chloro-2H-1,4-benzoxazine, was synthesized and characterized. The crystal structure of the title compound (C11H10Cl3NO2, Mr=294.55) has been determined by single-crystal X-ray diffraction. The crystal belongs to monoclinic, space group P21/c, with a=6.7619(14), b=24.866(5), c=9.737(3) Å, α=90.00, β=130.982(18), γ=90.00°, V=1235.9(5) Å3, Z=4, Dx=1.583 Mg/cm3, λ(Mo Ka)=0.71073 Å, F(000)=600, μ=0.729 mm−1, R=0.0476, and wR=0.1274 for 2217 reflections with I>2σ(I). |
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| ISSN: | 2090-9063 2090-9071 |