Development of self-assembled poly(2-ethyl-2-oxazoline)-b-poly(ε-caprolactone) (PEtOx-b-PCL) copolymeric nanostructures in aqueous solution and evaluation of their morphological transitions

Amphiphilic block copolymers are known to self-assemble into various morphologies, including ellipsoids, tubular structures, toroids, vesicles, micellar structures. In this paper, we discuss the synthesis of copolymeric nanostructures (CNs) using poly(2-ethyl-2-oxazoline)-block-poly(ε-caprolactone)...

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Main Authors: U. U. Ozkose, S. Gulyuz, U. C. Oz, M. A. Tasdelen, O. Alpturk, A. Bozkir, O. Yilmaz
Format: Article
Language:English
Published: Budapest University of Technology and Economics 2020-11-01
Series:eXPRESS Polymer Letters
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Online Access:http://www.expresspolymlett.com/letolt.php?file=EPL-0010664&mi=cd
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author U. U. Ozkose
S. Gulyuz
U. C. Oz
M. A. Tasdelen
O. Alpturk
A. Bozkir
O. Yilmaz
author_facet U. U. Ozkose
S. Gulyuz
U. C. Oz
M. A. Tasdelen
O. Alpturk
A. Bozkir
O. Yilmaz
author_sort U. U. Ozkose
collection DOAJ
description Amphiphilic block copolymers are known to self-assemble into various morphologies, including ellipsoids, tubular structures, toroids, vesicles, micellar structures. In this paper, we discuss the synthesis of copolymeric nanostructures (CNs) using poly(2-ethyl-2-oxazoline)-block-poly(ε-caprolactone) (PEtOx-b-PCL) amphiphilic block copolymers. Our data indicate that - varying the molecular weight and the number of repeating units dictate the nature of morphology. That is, the formation of self-assembled morphologies from ellipsoid to rod-like architectures are observed in aqueous solution, depending on the mass ratio of the hydrophilic block (fPEtOx). To best of our knowledge, this is the first report on the morphological transitions of PEtOx-b-PCL amphiphilic block copolymer-based CNs with different fPEtOx values in the literature.
format Article
id doaj-art-45b48a24641b441084d185eedfe203f5
institution DOAJ
issn 1788-618X
language English
publishDate 2020-11-01
publisher Budapest University of Technology and Economics
record_format Article
series eXPRESS Polymer Letters
spelling doaj-art-45b48a24641b441084d185eedfe203f52025-08-20T03:14:39ZengBudapest University of Technology and EconomicseXPRESS Polymer Letters1788-618X2020-11-0114111048106210.3144/expresspolymlett.2020.85Development of self-assembled poly(2-ethyl-2-oxazoline)-b-poly(ε-caprolactone) (PEtOx-b-PCL) copolymeric nanostructures in aqueous solution and evaluation of their morphological transitionsU. U. OzkoseS. GulyuzU. C. OzM. A. TasdelenO. AlpturkA. BozkirO. YilmazAmphiphilic block copolymers are known to self-assemble into various morphologies, including ellipsoids, tubular structures, toroids, vesicles, micellar structures. In this paper, we discuss the synthesis of copolymeric nanostructures (CNs) using poly(2-ethyl-2-oxazoline)-block-poly(ε-caprolactone) (PEtOx-b-PCL) amphiphilic block copolymers. Our data indicate that - varying the molecular weight and the number of repeating units dictate the nature of morphology. That is, the formation of self-assembled morphologies from ellipsoid to rod-like architectures are observed in aqueous solution, depending on the mass ratio of the hydrophilic block (fPEtOx). To best of our knowledge, this is the first report on the morphological transitions of PEtOx-b-PCL amphiphilic block copolymer-based CNs with different fPEtOx values in the literature.http://www.expresspolymlett.com/letolt.php?file=EPL-0010664&mi=cdnanomaterialspoly(2-ethyl-2-oxazoline) amphiphilic block copolymersself-assemblymorphological transition
spellingShingle U. U. Ozkose
S. Gulyuz
U. C. Oz
M. A. Tasdelen
O. Alpturk
A. Bozkir
O. Yilmaz
Development of self-assembled poly(2-ethyl-2-oxazoline)-b-poly(ε-caprolactone) (PEtOx-b-PCL) copolymeric nanostructures in aqueous solution and evaluation of their morphological transitions
eXPRESS Polymer Letters
nanomaterials
poly(2-ethyl-2-oxazoline)
amphiphilic block copolymers
self-assembly
morphological transition
title Development of self-assembled poly(2-ethyl-2-oxazoline)-b-poly(ε-caprolactone) (PEtOx-b-PCL) copolymeric nanostructures in aqueous solution and evaluation of their morphological transitions
title_full Development of self-assembled poly(2-ethyl-2-oxazoline)-b-poly(ε-caprolactone) (PEtOx-b-PCL) copolymeric nanostructures in aqueous solution and evaluation of their morphological transitions
title_fullStr Development of self-assembled poly(2-ethyl-2-oxazoline)-b-poly(ε-caprolactone) (PEtOx-b-PCL) copolymeric nanostructures in aqueous solution and evaluation of their morphological transitions
title_full_unstemmed Development of self-assembled poly(2-ethyl-2-oxazoline)-b-poly(ε-caprolactone) (PEtOx-b-PCL) copolymeric nanostructures in aqueous solution and evaluation of their morphological transitions
title_short Development of self-assembled poly(2-ethyl-2-oxazoline)-b-poly(ε-caprolactone) (PEtOx-b-PCL) copolymeric nanostructures in aqueous solution and evaluation of their morphological transitions
title_sort development of self assembled poly 2 ethyl 2 oxazoline b poly ε caprolactone petox b pcl copolymeric nanostructures in aqueous solution and evaluation of their morphological transitions
topic nanomaterials
poly(2-ethyl-2-oxazoline)
amphiphilic block copolymers
self-assembly
morphological transition
url http://www.expresspolymlett.com/letolt.php?file=EPL-0010664&mi=cd
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