Pharmacokinetics of Ziyuglycoside I and Ziyuglycoside II in Rat Plasma by UPLC-MS/MS

Ziyuglycoside I and ziyuglycoside II are important active components of Sanguisorba officinalis L., which have excellent pharmacological effects, such as antioxidant and anticancer effects. However, the bioavailability of ziyuglycoside I and ziyuglycoside II has not been reported. This work aims to...

Full description

Saved in:
Bibliographic Details
Main Authors: Xiuwei Shen, Ziyue Wang, Wenting Li, Shenshen Mei, Shunjun Ma, Xianqin Wang, Congcong Wen, Fan Chen, Guojun Zheng
Format: Article
Language:English
Published: Wiley 2024-01-01
Series:International Journal of Analytical Chemistry
Online Access:http://dx.doi.org/10.1155/2024/7971021
Tags: Add Tag
No Tags, Be the first to tag this record!
_version_ 1850110261017444352
author Xiuwei Shen
Ziyue Wang
Wenting Li
Shenshen Mei
Shunjun Ma
Xianqin Wang
Congcong Wen
Fan Chen
Guojun Zheng
author_facet Xiuwei Shen
Ziyue Wang
Wenting Li
Shenshen Mei
Shunjun Ma
Xianqin Wang
Congcong Wen
Fan Chen
Guojun Zheng
author_sort Xiuwei Shen
collection DOAJ
description Ziyuglycoside I and ziyuglycoside II are important active components of Sanguisorba officinalis L., which have excellent pharmacological effects, such as antioxidant and anticancer effects. However, the bioavailability of ziyuglycoside I and ziyuglycoside II has not been reported. This work aims to establish a UPLC-MS/MS method to study the pharmacokinetics of ziyuglycoside I and ziyuglycoside II in rats under different administration routes (intragastric and intravenous administration) and to calculate the bioavailability. The concentration of ziyuglycoside I and ziyuglycoside II in rat plasma in the range of 2–2000 ng/mL showed a good linear relationship (r > 0.99). The intra-day accuracies of ziyuglycoside I and ziyuglycoside II ranged from 87% to 110%, and the inter-day accuracies ranged from 97% to 109%. The intra-day precision was less than 15% and the inter-day precision was less than 14%. The matrix effects ranged from 88% to 113%. The recoveries were all above 84%. The developed UPLC-MS/MS method for the determination of ziyuglycoside I and ziyuglycoside II in rat plasma was applied to pharmacokinetics. The bioavailability of ziyuglycoside I and ziyuglycoside II was measured at 2.6% and 4.6%, respectively.
format Article
id doaj-art-4561e6adc19f406eb27ebaad92846cc1
institution OA Journals
issn 1687-8779
language English
publishDate 2024-01-01
publisher Wiley
record_format Article
series International Journal of Analytical Chemistry
spelling doaj-art-4561e6adc19f406eb27ebaad92846cc12025-08-20T02:37:52ZengWileyInternational Journal of Analytical Chemistry1687-87792024-01-01202410.1155/2024/7971021Pharmacokinetics of Ziyuglycoside I and Ziyuglycoside II in Rat Plasma by UPLC-MS/MSXiuwei Shen0Ziyue Wang1Wenting Li2Shenshen Mei3Shunjun Ma4Xianqin Wang5Congcong Wen6Fan Chen7Guojun Zheng8Ruian People’s HospitalLaboratory Animal CentreSchool of Pharmaceutical SciencesLaboratory Animal CentreLaboratory Animal CentreSchool of Pharmaceutical SciencesLaboratory Animal CentreRuian People’s HospitalRuian People’s HospitalZiyuglycoside I and ziyuglycoside II are important active components of Sanguisorba officinalis L., which have excellent pharmacological effects, such as antioxidant and anticancer effects. However, the bioavailability of ziyuglycoside I and ziyuglycoside II has not been reported. This work aims to establish a UPLC-MS/MS method to study the pharmacokinetics of ziyuglycoside I and ziyuglycoside II in rats under different administration routes (intragastric and intravenous administration) and to calculate the bioavailability. The concentration of ziyuglycoside I and ziyuglycoside II in rat plasma in the range of 2–2000 ng/mL showed a good linear relationship (r > 0.99). The intra-day accuracies of ziyuglycoside I and ziyuglycoside II ranged from 87% to 110%, and the inter-day accuracies ranged from 97% to 109%. The intra-day precision was less than 15% and the inter-day precision was less than 14%. The matrix effects ranged from 88% to 113%. The recoveries were all above 84%. The developed UPLC-MS/MS method for the determination of ziyuglycoside I and ziyuglycoside II in rat plasma was applied to pharmacokinetics. The bioavailability of ziyuglycoside I and ziyuglycoside II was measured at 2.6% and 4.6%, respectively.http://dx.doi.org/10.1155/2024/7971021
spellingShingle Xiuwei Shen
Ziyue Wang
Wenting Li
Shenshen Mei
Shunjun Ma
Xianqin Wang
Congcong Wen
Fan Chen
Guojun Zheng
Pharmacokinetics of Ziyuglycoside I and Ziyuglycoside II in Rat Plasma by UPLC-MS/MS
International Journal of Analytical Chemistry
title Pharmacokinetics of Ziyuglycoside I and Ziyuglycoside II in Rat Plasma by UPLC-MS/MS
title_full Pharmacokinetics of Ziyuglycoside I and Ziyuglycoside II in Rat Plasma by UPLC-MS/MS
title_fullStr Pharmacokinetics of Ziyuglycoside I and Ziyuglycoside II in Rat Plasma by UPLC-MS/MS
title_full_unstemmed Pharmacokinetics of Ziyuglycoside I and Ziyuglycoside II in Rat Plasma by UPLC-MS/MS
title_short Pharmacokinetics of Ziyuglycoside I and Ziyuglycoside II in Rat Plasma by UPLC-MS/MS
title_sort pharmacokinetics of ziyuglycoside i and ziyuglycoside ii in rat plasma by uplc ms ms
url http://dx.doi.org/10.1155/2024/7971021
work_keys_str_mv AT xiuweishen pharmacokineticsofziyuglycosideiandziyuglycosideiiinratplasmabyuplcmsms
AT ziyuewang pharmacokineticsofziyuglycosideiandziyuglycosideiiinratplasmabyuplcmsms
AT wentingli pharmacokineticsofziyuglycosideiandziyuglycosideiiinratplasmabyuplcmsms
AT shenshenmei pharmacokineticsofziyuglycosideiandziyuglycosideiiinratplasmabyuplcmsms
AT shunjunma pharmacokineticsofziyuglycosideiandziyuglycosideiiinratplasmabyuplcmsms
AT xianqinwang pharmacokineticsofziyuglycosideiandziyuglycosideiiinratplasmabyuplcmsms
AT congcongwen pharmacokineticsofziyuglycosideiandziyuglycosideiiinratplasmabyuplcmsms
AT fanchen pharmacokineticsofziyuglycosideiandziyuglycosideiiinratplasmabyuplcmsms
AT guojunzheng pharmacokineticsofziyuglycosideiandziyuglycosideiiinratplasmabyuplcmsms