Regulation of magnetocaloric properties and critical behavior of La0.7Sr0.3MnO3 by high-pressure heat treatment

Summary: La0.7Sr0.3MnO3 polycrystalline samples were prepared using a two-step process (high-temperature solid-phase reaction method and high-pressure heat treatment) under different pressures. The magnetocaloric properties of the samples exhibited a significant dependence on pressure. The nonlinear...

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Main Authors: Xiang Jin, Huaijin Ma, Qi Li, Jiawei Xu, Jianjun Zhao, Tegus O, Jiaohong Huang
Format: Article
Language:English
Published: Elsevier 2025-06-01
Series:iScience
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Online Access:http://www.sciencedirect.com/science/article/pii/S2589004225007941
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author Xiang Jin
Huaijin Ma
Qi Li
Jiawei Xu
Jianjun Zhao
Tegus O
Jiaohong Huang
author_facet Xiang Jin
Huaijin Ma
Qi Li
Jiawei Xu
Jianjun Zhao
Tegus O
Jiaohong Huang
author_sort Xiang Jin
collection DOAJ
description Summary: La0.7Sr0.3MnO3 polycrystalline samples were prepared using a two-step process (high-temperature solid-phase reaction method and high-pressure heat treatment) under different pressures. The magnetocaloric properties of the samples exhibited a significant dependence on pressure. The nonlinear changes in average bond length with pressure were defined in two stages: 0–2 GPa (S1) and 2-4-6 GPa(S2). S1: The double-exchange interaction was weakened and the Curie temperature was decreased from 367 K to 338 K due to negative volume compressibility, while the peaks of magnetic entropy change were reduced. S2: The rate of linear increase in Curie temperature induced by normal cell contraction is 5.6 K·GPa−1. Maximum magnetic entropy change and refrigeration temperature span varied at the rates of 0.29 J·kg−1·K−1·GPa−1 and -5.37 K·GPa−1, respectively. All the samples exhibited a second-order ferromagnetic-paramagnetic transitions with critical behavior evolving from mean-field model adherence (S1) to deviation (S2). The magnetocaloric properties of La0.7Sr0.3MnO3 can be effectively regulated by pressure.
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institution OA Journals
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spelling doaj-art-449a0cf3abc64be686dbfdce596dfcdd2025-08-20T02:23:11ZengElsevieriScience2589-00422025-06-0128611253310.1016/j.isci.2025.112533Regulation of magnetocaloric properties and critical behavior of La0.7Sr0.3MnO3 by high-pressure heat treatmentXiang Jin0Huaijin Ma1Qi Li2Jiawei Xu3Jianjun Zhao4Tegus O5Jiaohong Huang6School of Physics and Electronic Information, Inner Mongolia Normal University, Hohhot 010020, China; School of Vocational and Technical Teachers’ Education, Baotou Teachers’ College, Baotou 014030, China; Key Laboratory of Magnetism and Magnetic Materials for Higher Education in Inner Mongolia Autonomous Region, Baotou 014030, ChinaKey Laboratory of Magnetism and Magnetic Materials for Higher Education in Inner Mongolia Autonomous Region, Baotou 014030, China; School of Physical Science and Technology, Baotou Teachers’ College, Baotou 014030, ChinaKey Laboratory of Magnetism and Magnetic Materials for Higher Education in Inner Mongolia Autonomous Region, Baotou 014030, China; School of Physical Science and Technology, Baotou Teachers’ College, Baotou 014030, ChinaKey Laboratory of Magnetism and Magnetic Materials for Higher Education in Inner Mongolia Autonomous Region, Baotou 014030, China; School of Physical Science and Technology, Baotou Teachers’ College, Baotou 014030, ChinaKey Laboratory of Magnetism and Magnetic Materials for Higher Education in Inner Mongolia Autonomous Region, Baotou 014030, China; School of Physical Science and Technology, Baotou Teachers’ College, Baotou 014030, China; Corresponding authorSchool of Physics and Electronic Information, Inner Mongolia Normal University, Hohhot 010020, China; Corresponding authorNational Key Laboratory of Baiyunobo Rare Earth Resource Research and Comprehensive Utilization, Baotou Research Institute of Rare Earths, Baotou 014030, China; Corresponding authorSummary: La0.7Sr0.3MnO3 polycrystalline samples were prepared using a two-step process (high-temperature solid-phase reaction method and high-pressure heat treatment) under different pressures. The magnetocaloric properties of the samples exhibited a significant dependence on pressure. The nonlinear changes in average bond length with pressure were defined in two stages: 0–2 GPa (S1) and 2-4-6 GPa(S2). S1: The double-exchange interaction was weakened and the Curie temperature was decreased from 367 K to 338 K due to negative volume compressibility, while the peaks of magnetic entropy change were reduced. S2: The rate of linear increase in Curie temperature induced by normal cell contraction is 5.6 K·GPa−1. Maximum magnetic entropy change and refrigeration temperature span varied at the rates of 0.29 J·kg−1·K−1·GPa−1 and -5.37 K·GPa−1, respectively. All the samples exhibited a second-order ferromagnetic-paramagnetic transitions with critical behavior evolving from mean-field model adherence (S1) to deviation (S2). The magnetocaloric properties of La0.7Sr0.3MnO3 can be effectively regulated by pressure.http://www.sciencedirect.com/science/article/pii/S2589004225007941Materials scienceMaterials synthesisMaterials property
spellingShingle Xiang Jin
Huaijin Ma
Qi Li
Jiawei Xu
Jianjun Zhao
Tegus O
Jiaohong Huang
Regulation of magnetocaloric properties and critical behavior of La0.7Sr0.3MnO3 by high-pressure heat treatment
iScience
Materials science
Materials synthesis
Materials property
title Regulation of magnetocaloric properties and critical behavior of La0.7Sr0.3MnO3 by high-pressure heat treatment
title_full Regulation of magnetocaloric properties and critical behavior of La0.7Sr0.3MnO3 by high-pressure heat treatment
title_fullStr Regulation of magnetocaloric properties and critical behavior of La0.7Sr0.3MnO3 by high-pressure heat treatment
title_full_unstemmed Regulation of magnetocaloric properties and critical behavior of La0.7Sr0.3MnO3 by high-pressure heat treatment
title_short Regulation of magnetocaloric properties and critical behavior of La0.7Sr0.3MnO3 by high-pressure heat treatment
title_sort regulation of magnetocaloric properties and critical behavior of la0 7sr0 3mno3 by high pressure heat treatment
topic Materials science
Materials synthesis
Materials property
url http://www.sciencedirect.com/science/article/pii/S2589004225007941
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