Crystal structure and Hirshfeld surface analysis of 4-methyl-N-[2-(5-methylfuran-2-yl)phenyl]-N-[(5-phenylfuran-2-yl)methyl]benzenesulfonamide

In the title compound, C29H25NO4S, the molecular conformation is stable with intramolecular C—H...O and C—H...N interactions being observed. In the crystal, molecules are linked by C—H...O interactions, forming layers parallel to the (100) plane. In addition, π–π [centroid-to-centroid distance = 3.4...

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Main Authors: Selbi Annadurdyyeva, Anastasia E. Levina, Victor N. Khrustalev, Roya Z. Nazarova, Khudayar I. Hasanov, Nurlana D. Sadikhova, Mehmet Akkurt, Gizachew Mulugeta Manahelohe
Format: Article
Language:English
Published: International Union of Crystallography 2025-08-01
Series:Acta Crystallographica Section E: Crystallographic Communications
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Online Access:https://journals.iucr.org/paper?S2056989025006231
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author Selbi Annadurdyyeva
Anastasia E. Levina
Victor N. Khrustalev
Roya Z. Nazarova
Khudayar I. Hasanov
Nurlana D. Sadikhova
Mehmet Akkurt
Gizachew Mulugeta Manahelohe
author_facet Selbi Annadurdyyeva
Anastasia E. Levina
Victor N. Khrustalev
Roya Z. Nazarova
Khudayar I. Hasanov
Nurlana D. Sadikhova
Mehmet Akkurt
Gizachew Mulugeta Manahelohe
author_sort Selbi Annadurdyyeva
collection DOAJ
description In the title compound, C29H25NO4S, the molecular conformation is stable with intramolecular C—H...O and C—H...N interactions being observed. In the crystal, molecules are linked by C—H...O interactions, forming layers parallel to the (100) plane. In addition, π–π [centroid-to-centroid distance = 3.4961 (7) Å] and C—H...π interactions connect the molecules within the layers. The layers are also bound to each other by van der Waals interactions. A Hirshfeld surface analysis of the crystal structure indicates that the most important contributions for the crystal packing are from H...H (53.2%), C...H/H...C (28.9%) and O...H/H...O (13.8%) contacts.
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institution Kabale University
issn 2056-9890
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publishDate 2025-08-01
publisher International Union of Crystallography
record_format Article
series Acta Crystallographica Section E: Crystallographic Communications
spelling doaj-art-447e1263dce44b49836b099123745dd92025-08-20T03:44:29ZengInternational Union of CrystallographyActa Crystallographica Section E: Crystallographic Communications2056-98902025-08-0181870671010.1107/S2056989025006231ee2017Crystal structure and Hirshfeld surface analysis of 4-methyl-N-[2-(5-methylfuran-2-yl)phenyl]-N-[(5-phenylfuran-2-yl)methyl]benzenesulfonamideSelbi Annadurdyyeva0Anastasia E. Levina1Victor N. Khrustalev2Roya Z. Nazarova3Khudayar I. Hasanov4Nurlana D. Sadikhova5Mehmet Akkurt6Gizachew Mulugeta Manahelohe7RUDN University, 6 Miklukho-Maklaya St., Moscow 117198, Russian FederationRUDN University, 6 Miklukho-Maklaya St., Moscow 117198, Russian FederationRUDN University, 6 Miklukho-Maklaya St., Moscow 117198, Russian FederationBaku Engineering University, Khirdalan, Hasan Aliyev str. 120, AZ0101, Absheron, AzerbaijanAzerbaijan Medical University, Scientific Research Centre (SRC), A. Kasumzade St. 14, AZ 1022, Baku, AzerbaijanDepartment of Organic Chemistry, Baku State University, Z. Xalilov Str. 23, AZ 1148 Baku, AzerbaijanDepartment of Physics, Faculty of Sciences, Erciyes University, 38039 Kayseri, TürkiyeDepartment of Chemistry, University of Gondar, PO Box 196, Gondar, EthiopiaIn the title compound, C29H25NO4S, the molecular conformation is stable with intramolecular C—H...O and C—H...N interactions being observed. In the crystal, molecules are linked by C—H...O interactions, forming layers parallel to the (100) plane. In addition, π–π [centroid-to-centroid distance = 3.4961 (7) Å] and C—H...π interactions connect the molecules within the layers. The layers are also bound to each other by van der Waals interactions. A Hirshfeld surface analysis of the crystal structure indicates that the most important contributions for the crystal packing are from H...H (53.2%), C...H/H...C (28.9%) and O...H/H...O (13.8%) contacts.https://journals.iucr.org/paper?S2056989025006231crystal structurehydrogen bondvan der waals interactionshirshfeld surface analysis
spellingShingle Selbi Annadurdyyeva
Anastasia E. Levina
Victor N. Khrustalev
Roya Z. Nazarova
Khudayar I. Hasanov
Nurlana D. Sadikhova
Mehmet Akkurt
Gizachew Mulugeta Manahelohe
Crystal structure and Hirshfeld surface analysis of 4-methyl-N-[2-(5-methylfuran-2-yl)phenyl]-N-[(5-phenylfuran-2-yl)methyl]benzenesulfonamide
Acta Crystallographica Section E: Crystallographic Communications
crystal structure
hydrogen bond
van der waals interactions
hirshfeld surface analysis
title Crystal structure and Hirshfeld surface analysis of 4-methyl-N-[2-(5-methylfuran-2-yl)phenyl]-N-[(5-phenylfuran-2-yl)methyl]benzenesulfonamide
title_full Crystal structure and Hirshfeld surface analysis of 4-methyl-N-[2-(5-methylfuran-2-yl)phenyl]-N-[(5-phenylfuran-2-yl)methyl]benzenesulfonamide
title_fullStr Crystal structure and Hirshfeld surface analysis of 4-methyl-N-[2-(5-methylfuran-2-yl)phenyl]-N-[(5-phenylfuran-2-yl)methyl]benzenesulfonamide
title_full_unstemmed Crystal structure and Hirshfeld surface analysis of 4-methyl-N-[2-(5-methylfuran-2-yl)phenyl]-N-[(5-phenylfuran-2-yl)methyl]benzenesulfonamide
title_short Crystal structure and Hirshfeld surface analysis of 4-methyl-N-[2-(5-methylfuran-2-yl)phenyl]-N-[(5-phenylfuran-2-yl)methyl]benzenesulfonamide
title_sort crystal structure and hirshfeld surface analysis of 4 methyl n 2 5 methylfuran 2 yl phenyl n 5 phenylfuran 2 yl methyl benzenesulfonamide
topic crystal structure
hydrogen bond
van der waals interactions
hirshfeld surface analysis
url https://journals.iucr.org/paper?S2056989025006231
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