Microstructure and high-temperature oxidation resistance of wire and arc additively manufactured Si-containing 9Cr oxide dispersion strengthened steel

Three 9Cr oxide dispersion strengthened (ODS) steels with addition of 0.5–2 wt% Si were fabricated by wire and arc additive manufacturing (WAAM) technique in this work. Their microstructures and oxidation behavior at 800 °C were systematically studied. The WAAM-processed steels exhibited refined mar...

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Main Authors: Shengming Yin, Xiaoling Liu, Lihong Xue, Hefei Huang, Youwei Yan
Format: Article
Language:English
Published: Elsevier 2025-05-01
Series:Journal of Materials Research and Technology
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Online Access:http://www.sciencedirect.com/science/article/pii/S2238785425011482
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author Shengming Yin
Xiaoling Liu
Lihong Xue
Hefei Huang
Youwei Yan
author_facet Shengming Yin
Xiaoling Liu
Lihong Xue
Hefei Huang
Youwei Yan
author_sort Shengming Yin
collection DOAJ
description Three 9Cr oxide dispersion strengthened (ODS) steels with addition of 0.5–2 wt% Si were fabricated by wire and arc additive manufacturing (WAAM) technique in this work. Their microstructures and oxidation behavior at 800 °C were systematically studied. The WAAM-processed steels exhibited refined martensite lath bundles due to rapid solidification. Increasing Si content (1–2 wt.%) further refined martensitic laths, enhanced dislocation density, and promoted the formation of high-density (∼6.54 × 1023 m−3) Y2SiO5 nano-oxides (∼3.43 nm) within the matrix. Notably, the 2Si steel demonstrated exceptional oxidation resistance, with a rate of 0.36 × 10−3 mg cm−2 h−1, surpassing most commercial heat-resistant steels. This improvement is attributed to a tri-layered Cr1.5Mn1.5O4/Cr2O3/SiO2(amorphous) oxide scale, which effectively inhibits oxygen inward diffusion.
format Article
id doaj-art-41ab8075b8a749488e56e4736f778f1a
institution OA Journals
issn 2238-7854
language English
publishDate 2025-05-01
publisher Elsevier
record_format Article
series Journal of Materials Research and Technology
spelling doaj-art-41ab8075b8a749488e56e4736f778f1a2025-08-20T02:16:02ZengElsevierJournal of Materials Research and Technology2238-78542025-05-01367069708010.1016/j.jmrt.2025.04.327Microstructure and high-temperature oxidation resistance of wire and arc additively manufactured Si-containing 9Cr oxide dispersion strengthened steelShengming Yin0Xiaoling Liu1Lihong Xue2Hefei Huang3Youwei Yan4State Key Laboratory of Materials Processing and Die & Mould Technology, Department of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan, 430074, ChinaState Key Laboratory of Materials Processing and Die & Mould Technology, Department of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan, 430074, ChinaState Key Laboratory of Materials Processing and Die & Mould Technology, Department of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan, 430074, ChinaShanghai Institute of Applied Physics, Chinese Academy of Sciences, Shanghai, 201800, ChinaState Key Laboratory of Materials Processing and Die & Mould Technology, Department of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan, 430074, China; School of Aerospace Engineering, Huazhong University of Science and Technology, Wuhan, 430074, China; Corresponding author. State Key Laboratory of Materials Processing and Die & Mould Technology, Department of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan, 430074, China.Three 9Cr oxide dispersion strengthened (ODS) steels with addition of 0.5–2 wt% Si were fabricated by wire and arc additive manufacturing (WAAM) technique in this work. Their microstructures and oxidation behavior at 800 °C were systematically studied. The WAAM-processed steels exhibited refined martensite lath bundles due to rapid solidification. Increasing Si content (1–2 wt.%) further refined martensitic laths, enhanced dislocation density, and promoted the formation of high-density (∼6.54 × 1023 m−3) Y2SiO5 nano-oxides (∼3.43 nm) within the matrix. Notably, the 2Si steel demonstrated exceptional oxidation resistance, with a rate of 0.36 × 10−3 mg cm−2 h−1, surpassing most commercial heat-resistant steels. This improvement is attributed to a tri-layered Cr1.5Mn1.5O4/Cr2O3/SiO2(amorphous) oxide scale, which effectively inhibits oxygen inward diffusion.http://www.sciencedirect.com/science/article/pii/S2238785425011482Wire and arc additive manufacturing (WAAM)Oxide dispersion-strengthened steelSilicon alloyingHigh-temperature oxidation
spellingShingle Shengming Yin
Xiaoling Liu
Lihong Xue
Hefei Huang
Youwei Yan
Microstructure and high-temperature oxidation resistance of wire and arc additively manufactured Si-containing 9Cr oxide dispersion strengthened steel
Journal of Materials Research and Technology
Wire and arc additive manufacturing (WAAM)
Oxide dispersion-strengthened steel
Silicon alloying
High-temperature oxidation
title Microstructure and high-temperature oxidation resistance of wire and arc additively manufactured Si-containing 9Cr oxide dispersion strengthened steel
title_full Microstructure and high-temperature oxidation resistance of wire and arc additively manufactured Si-containing 9Cr oxide dispersion strengthened steel
title_fullStr Microstructure and high-temperature oxidation resistance of wire and arc additively manufactured Si-containing 9Cr oxide dispersion strengthened steel
title_full_unstemmed Microstructure and high-temperature oxidation resistance of wire and arc additively manufactured Si-containing 9Cr oxide dispersion strengthened steel
title_short Microstructure and high-temperature oxidation resistance of wire and arc additively manufactured Si-containing 9Cr oxide dispersion strengthened steel
title_sort microstructure and high temperature oxidation resistance of wire and arc additively manufactured si containing 9cr oxide dispersion strengthened steel
topic Wire and arc additive manufacturing (WAAM)
Oxide dispersion-strengthened steel
Silicon alloying
High-temperature oxidation
url http://www.sciencedirect.com/science/article/pii/S2238785425011482
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