Hydrogen isotopes retention studies using laser and microwave induced plasma coupling

Abstract The detection of deuterium and tritium retention in fusion devices via optical emission spectroscopy (OES) faces significant challenges due to experimental limitations, particularly in resolving hydrogen isotope Balmer alpha lines (Hα, Dα, and Tα). In this study, we propose and evaluate the...

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Main Authors: N. Vujadinovic, I. Traparic, B. D. Stankov, D. Rankovic, M. Kuzmanovic, M. Ivkovic
Format: Article
Language:English
Published: Nature Portfolio 2025-04-01
Series:Scientific Reports
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Online Access:https://doi.org/10.1038/s41598-025-96546-x
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author N. Vujadinovic
I. Traparic
B. D. Stankov
D. Rankovic
M. Kuzmanovic
M. Ivkovic
author_facet N. Vujadinovic
I. Traparic
B. D. Stankov
D. Rankovic
M. Kuzmanovic
M. Ivkovic
author_sort N. Vujadinovic
collection DOAJ
description Abstract The detection of deuterium and tritium retention in fusion devices via optical emission spectroscopy (OES) faces significant challenges due to experimental limitations, particularly in resolving hydrogen isotope Balmer alpha lines (Hα, Dα, and Tα). In this study, we propose and evaluate the coupling of laser ablation and laser-induced desorption with microwave-induced plasma (MIP) as an approach to resolve this problem. This approach effectively meets the resolution requirements for Balmer alpha lines, overcoming limitations of standard laser-induced breakdown spectroscopy (LIBS) setups. Optimization of Nd:YAG laser ablation was performed using pure copper and tungsten targets, while desorption, including femtosecond (fs) laser-induced desorption, was studied on graphite powder mixed with heavy water and water. The results demonstrate a significant improvement in spectral resolution and analytical performances, highlighting the potential of this technique for tritium retention studies in plasma-facing components.
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spelling doaj-art-4000b19c3e2e48b0ab9d6c9551f4e5f72025-08-20T02:11:46ZengNature PortfolioScientific Reports2045-23222025-04-0115111410.1038/s41598-025-96546-xHydrogen isotopes retention studies using laser and microwave induced plasma couplingN. Vujadinovic0I. Traparic1B. D. Stankov2D. Rankovic3M. Kuzmanovic4M. Ivkovic5Institute of Physics, University of BelgradeInstitute of Physics, University of BelgradeInstitute of Physics, University of BelgradeFaculty of Physical Chemistry, University of BelgradeFaculty of Physical Chemistry, University of BelgradeInstitute of Physics, University of BelgradeAbstract The detection of deuterium and tritium retention in fusion devices via optical emission spectroscopy (OES) faces significant challenges due to experimental limitations, particularly in resolving hydrogen isotope Balmer alpha lines (Hα, Dα, and Tα). In this study, we propose and evaluate the coupling of laser ablation and laser-induced desorption with microwave-induced plasma (MIP) as an approach to resolve this problem. This approach effectively meets the resolution requirements for Balmer alpha lines, overcoming limitations of standard laser-induced breakdown spectroscopy (LIBS) setups. Optimization of Nd:YAG laser ablation was performed using pure copper and tungsten targets, while desorption, including femtosecond (fs) laser-induced desorption, was studied on graphite powder mixed with heavy water and water. The results demonstrate a significant improvement in spectral resolution and analytical performances, highlighting the potential of this technique for tritium retention studies in plasma-facing components.https://doi.org/10.1038/s41598-025-96546-xHydrogen isotopes retentionLaser ablationLaser induced desorptionMicrowave induced plasmaPlasma-facing componentsLIBS
spellingShingle N. Vujadinovic
I. Traparic
B. D. Stankov
D. Rankovic
M. Kuzmanovic
M. Ivkovic
Hydrogen isotopes retention studies using laser and microwave induced plasma coupling
Scientific Reports
Hydrogen isotopes retention
Laser ablation
Laser induced desorption
Microwave induced plasma
Plasma-facing components
LIBS
title Hydrogen isotopes retention studies using laser and microwave induced plasma coupling
title_full Hydrogen isotopes retention studies using laser and microwave induced plasma coupling
title_fullStr Hydrogen isotopes retention studies using laser and microwave induced plasma coupling
title_full_unstemmed Hydrogen isotopes retention studies using laser and microwave induced plasma coupling
title_short Hydrogen isotopes retention studies using laser and microwave induced plasma coupling
title_sort hydrogen isotopes retention studies using laser and microwave induced plasma coupling
topic Hydrogen isotopes retention
Laser ablation
Laser induced desorption
Microwave induced plasma
Plasma-facing components
LIBS
url https://doi.org/10.1038/s41598-025-96546-x
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AT drankovic hydrogenisotopesretentionstudiesusinglaserandmicrowaveinducedplasmacoupling
AT mkuzmanovic hydrogenisotopesretentionstudiesusinglaserandmicrowaveinducedplasmacoupling
AT mivkovic hydrogenisotopesretentionstudiesusinglaserandmicrowaveinducedplasmacoupling