Influence of composition of cathodic deposition electrolyte on morphology and capacity properties of MnO2 film

Manganese oxide was obtained by cathodic electrochemical deposition from the electrolyte solutions adding sodium nitrate or sulfate. The structural characteristics and the elemental composition of the MnO2 samples were studied by energy dispersive microanalysis, IR spectroscopy, and transmission ele...

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Main Authors: Chernyavina, Valentina Vladimirovna, Dyshlovaya, Yaroslava Aleksandrovna, Berezhnaya, Aleksandra Grigor'evna
Format: Article
Language:English
Published: Saratov State University 2025-06-01
Series:Электрохимическая энергетика
Subjects:
Online Access:https://energetica.sgu.ru/sites/energetica.sgu.ru/files/text-pdf/2025/06/elektrohimicheskaya_energetika-2025-2-74-86.pdf
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author Chernyavina, Valentina Vladimirovna
Dyshlovaya, Yaroslava Aleksandrovna
Berezhnaya, Aleksandra Grigor'evna
author_facet Chernyavina, Valentina Vladimirovna
Dyshlovaya, Yaroslava Aleksandrovna
Berezhnaya, Aleksandra Grigor'evna
author_sort Chernyavina, Valentina Vladimirovna
collection DOAJ
description Manganese oxide was obtained by cathodic electrochemical deposition from the electrolyte solutions adding sodium nitrate or sulfate. The structural characteristics and the elemental composition of the MnO2 samples were studied by energy dispersive microanalysis, IR spectroscopy, and transmission electron microscopy. The electrochemical characteristics of the electrodes were determined by cyclic voltammetry, galvanostatic charge-discharge and impedance spectroscopy in 0.5M Na2SO4 solution. The dependence of the structural and capacitive properties of the MnO2 electrodes on the anion nature in the electrolyte for electrochemical deposition was determined. High capacitance characteristics were obtained for the MnO2 sample deposited from the electrolyte adding sodium sulfate. Its specific capacity was 215 F/g at the scanning speed of 5 mV/s.
format Article
id doaj-art-3ff974558f1a43d4b24fcacb15075bca
institution Kabale University
issn 1608-4039
1680-9505
language English
publishDate 2025-06-01
publisher Saratov State University
record_format Article
series Электрохимическая энергетика
spelling doaj-art-3ff974558f1a43d4b24fcacb15075bca2025-08-20T03:27:57ZengSaratov State UniversityЭлектрохимическая энергетика1608-40391680-95052025-06-01252748610.18500/1608-4039-2025-25-2-74-86Influence of composition of cathodic deposition electrolyte on morphology and capacity properties of MnO2 filmChernyavina, Valentina Vladimirovna0Dyshlovaya, Yaroslava Aleksandrovna1Berezhnaya, Aleksandra Grigor'evna2Southern Federal University, 7 Zorge St., Rostov-on-Don 344090, RussiaSouthern Federal University, 7 Zorge St., Rostov-on-Don 344090, RussiaSouthern Federal University, 7 Zorge St., Rostov-on-Don 344090, RussiaManganese oxide was obtained by cathodic electrochemical deposition from the electrolyte solutions adding sodium nitrate or sulfate. The structural characteristics and the elemental composition of the MnO2 samples were studied by energy dispersive microanalysis, IR spectroscopy, and transmission electron microscopy. The electrochemical characteristics of the electrodes were determined by cyclic voltammetry, galvanostatic charge-discharge and impedance spectroscopy in 0.5M Na2SO4 solution. The dependence of the structural and capacitive properties of the MnO2 electrodes on the anion nature in the electrolyte for electrochemical deposition was determined. High capacitance characteristics were obtained for the MnO2 sample deposited from the electrolyte adding sodium sulfate. Its specific capacity was 215 F/g at the scanning speed of 5 mV/s.https://energetica.sgu.ru/sites/energetica.sgu.ru/files/text-pdf/2025/06/elektrohimicheskaya_energetika-2025-2-74-86.pdfelectrochemical capacitoraqueous neutral electrolytemanganese dioxidespecific capacity
spellingShingle Chernyavina, Valentina Vladimirovna
Dyshlovaya, Yaroslava Aleksandrovna
Berezhnaya, Aleksandra Grigor'evna
Influence of composition of cathodic deposition electrolyte on morphology and capacity properties of MnO2 film
Электрохимическая энергетика
electrochemical capacitor
aqueous neutral electrolyte
manganese dioxide
specific capacity
title Influence of composition of cathodic deposition electrolyte on morphology and capacity properties of MnO2 film
title_full Influence of composition of cathodic deposition electrolyte on morphology and capacity properties of MnO2 film
title_fullStr Influence of composition of cathodic deposition electrolyte on morphology and capacity properties of MnO2 film
title_full_unstemmed Influence of composition of cathodic deposition electrolyte on morphology and capacity properties of MnO2 film
title_short Influence of composition of cathodic deposition electrolyte on morphology and capacity properties of MnO2 film
title_sort influence of composition of cathodic deposition electrolyte on morphology and capacity properties of mno2 film
topic electrochemical capacitor
aqueous neutral electrolyte
manganese dioxide
specific capacity
url https://energetica.sgu.ru/sites/energetica.sgu.ru/files/text-pdf/2025/06/elektrohimicheskaya_energetika-2025-2-74-86.pdf
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