Surface Characteristics and Performance Optimization of W-Doped Vanadium Dioxide Thin Films

This study explores the surface characteristics evaluation and performance optimization of tungsten (W)-doped vanadium dioxide (VO<sub>2</sub>) thin films. W-doped vanadium dioxide films were deposited on B270 glass substrates using an electron beam evaporation technique combined with th...

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Main Authors: Chuen-Lin Tien, Chun-Yu Chiang, Jia-Kai Tien, Ching-Chiun Wang, Shih-Chin Lin
Format: Article
Language:English
Published: MDPI AG 2024-12-01
Series:Surfaces
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Online Access:https://www.mdpi.com/2571-9637/7/4/73
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author Chuen-Lin Tien
Chun-Yu Chiang
Jia-Kai Tien
Ching-Chiun Wang
Shih-Chin Lin
author_facet Chuen-Lin Tien
Chun-Yu Chiang
Jia-Kai Tien
Ching-Chiun Wang
Shih-Chin Lin
author_sort Chuen-Lin Tien
collection DOAJ
description This study explores the surface characteristics evaluation and performance optimization of tungsten (W)-doped vanadium dioxide (VO<sub>2</sub>) thin films. W-doped vanadium dioxide films were deposited on B270 glass substrates using an electron beam evaporation technique combined with the ion beam-assisted deposition (IAD) method. The Taguchi method was used to analyze the performance optimization of VO<sub>2</sub> thin films, and L<sub>16</sub> orthogonal array design and Minitab software were used for optimization calculations. The surface roughness, visible light transmittance, infrared transmittance, and residual stress of un-doped and tungsten-doped (3–5%) VO<sub>2</sub> thin films are set as the quality performance indicators of thin films. The goal is to identify the key factors that affect the performance of VO<sub>2</sub> thin films during deposition and optimize their process parameters. The experimental results showed that a VO<sub>2</sub> thin film with 3% tungsten doping, an oxygen flow rate of 60 sccm, a heating temperature of 280 °C, and a film thickness of 60 nm exhibited the lowest surface roughness of 2.12 nm. A VO<sub>2</sub> thin film with 5% tungsten doping, an oxygen flow rate of 0 sccm, a heating temperature of 280 °C, and a film thickness of 60 nm had the highest visible light transmittance at 64.33%. When the oxygen flow rate was 60 sccm, the heating temperature was 295 °C, the film thickness was 150 nm, and the tungsten doping was 5%, the VO<sub>2</sub> thin film showed the lowest infrared transmittance of 31.34%. A thin film with 5% tungsten doping, an oxygen flow rate of 20 sccm, a heating temperature of 265 °C, and a film thickness of 120 nm exhibited the lowest residual stress of −0.195 GPa.
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spelling doaj-art-3f7bfa3c8f4c4f3bac26b885abdeaa342025-08-20T02:57:01ZengMDPI AGSurfaces2571-96372024-12-01741109112410.3390/surfaces7040073Surface Characteristics and Performance Optimization of W-Doped Vanadium Dioxide Thin FilmsChuen-Lin Tien0Chun-Yu Chiang1Jia-Kai Tien2Ching-Chiun Wang3Shih-Chin Lin4Department of Electrical Engineering, Feng Chia University, Taichung 40724, TaiwanPh.D. Program of Electrical and Communications Engineering, Feng Chia University, Taichung 40724, TaiwanGraduate Institute of Library & Information Science, National Chung Hsing University, Taichung 402202, TaiwanMechanical and Systems Research Lab, Industrial Technology Research Institute, Hsinchu 310401, TaiwanMechanical and Systems Research Lab, Industrial Technology Research Institute, Hsinchu 310401, TaiwanThis study explores the surface characteristics evaluation and performance optimization of tungsten (W)-doped vanadium dioxide (VO<sub>2</sub>) thin films. W-doped vanadium dioxide films were deposited on B270 glass substrates using an electron beam evaporation technique combined with the ion beam-assisted deposition (IAD) method. The Taguchi method was used to analyze the performance optimization of VO<sub>2</sub> thin films, and L<sub>16</sub> orthogonal array design and Minitab software were used for optimization calculations. The surface roughness, visible light transmittance, infrared transmittance, and residual stress of un-doped and tungsten-doped (3–5%) VO<sub>2</sub> thin films are set as the quality performance indicators of thin films. The goal is to identify the key factors that affect the performance of VO<sub>2</sub> thin films during deposition and optimize their process parameters. The experimental results showed that a VO<sub>2</sub> thin film with 3% tungsten doping, an oxygen flow rate of 60 sccm, a heating temperature of 280 °C, and a film thickness of 60 nm exhibited the lowest surface roughness of 2.12 nm. A VO<sub>2</sub> thin film with 5% tungsten doping, an oxygen flow rate of 0 sccm, a heating temperature of 280 °C, and a film thickness of 60 nm had the highest visible light transmittance at 64.33%. When the oxygen flow rate was 60 sccm, the heating temperature was 295 °C, the film thickness was 150 nm, and the tungsten doping was 5%, the VO<sub>2</sub> thin film showed the lowest infrared transmittance of 31.34%. A thin film with 5% tungsten doping, an oxygen flow rate of 20 sccm, a heating temperature of 265 °C, and a film thickness of 120 nm exhibited the lowest residual stress of −0.195 GPa.https://www.mdpi.com/2571-9637/7/4/73vanadium dioxidethin filmTaguchi methodsurface roughnessresidual stress
spellingShingle Chuen-Lin Tien
Chun-Yu Chiang
Jia-Kai Tien
Ching-Chiun Wang
Shih-Chin Lin
Surface Characteristics and Performance Optimization of W-Doped Vanadium Dioxide Thin Films
Surfaces
vanadium dioxide
thin film
Taguchi method
surface roughness
residual stress
title Surface Characteristics and Performance Optimization of W-Doped Vanadium Dioxide Thin Films
title_full Surface Characteristics and Performance Optimization of W-Doped Vanadium Dioxide Thin Films
title_fullStr Surface Characteristics and Performance Optimization of W-Doped Vanadium Dioxide Thin Films
title_full_unstemmed Surface Characteristics and Performance Optimization of W-Doped Vanadium Dioxide Thin Films
title_short Surface Characteristics and Performance Optimization of W-Doped Vanadium Dioxide Thin Films
title_sort surface characteristics and performance optimization of w doped vanadium dioxide thin films
topic vanadium dioxide
thin film
Taguchi method
surface roughness
residual stress
url https://www.mdpi.com/2571-9637/7/4/73
work_keys_str_mv AT chuenlintien surfacecharacteristicsandperformanceoptimizationofwdopedvanadiumdioxidethinfilms
AT chunyuchiang surfacecharacteristicsandperformanceoptimizationofwdopedvanadiumdioxidethinfilms
AT jiakaitien surfacecharacteristicsandperformanceoptimizationofwdopedvanadiumdioxidethinfilms
AT chingchiunwang surfacecharacteristicsandperformanceoptimizationofwdopedvanadiumdioxidethinfilms
AT shihchinlin surfacecharacteristicsandperformanceoptimizationofwdopedvanadiumdioxidethinfilms